JP4286906B1 - Powdered dentifrice composition based on traditional Korean medicine and its production method - Google Patents

Abstract

The present invention relates to a composition of a powder dentifrice comprising natural herbal medicine ingredients that have an excellent effect on dental health and oral hygiene in conjunction with higher consumer interest and well-being concerns, and its manufacture It is an object to provide a method.
The composition of the powder dentifrice of the present invention heats bamboo salt, flour, dried white mackerel, pine oil, lotus meat, spicy, sesame, peony, bellflower, and enokitake, which are natural ingredients useful for the human body. Alternatively, after drying and pulverizing, the obtained powder is blended and mixed in a certain ratio to produce.
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Description

  TECHNICAL FIELD The present invention relates to a composition of a powder dentifrice mainly containing medicinal materials used in traditional folk remedies and traditional Chinese medicine effective for hygiene management in the oral cavity, and a method for producing the same. More specifically, it is a powdery toothpaste or toothpaste composition, which is different from conventional toothpastes, which are generally composed of chemical substances, and is a traditional ingredient based on natural ingredients beneficial to the human body. The present invention relates to a composition of a powder dentifrice mainly composed of traditional Chinese herbal medicines used in folk remedies and herbal medicines (hereinafter referred to as “Korean medicine” and “Korean medicine materials”, which have become the nominal words of Korea).

  Conventionally, dentifrices that are commercially available are composed of various components in accordance with commercial products. Generally, silicas, calciums, magnesiums, aluminas, and the like are used as dentifrices. These are useful for mechanical cleaning of teeth, but if the particle size, hardness, form, etc. are not appropriate, the dentin surface of the crown portion may be damaged, so the particle size is approximately 1 The base is required to be uniform at ˜20 μm, the form should not have an excessive acute angle, and the hardness should be about 3 degrees of a Mohs hardness meter. Glycerins, sorbitols, xylitols, glycols, etc. are used as wetting agents, fluorides (fluorine) are used to prevent caries, and bactericidal disinfectants are used to kill bacteria in the oral cavity. Cationic surfactants and tartar solubilizers use enzymes to inhibit plaque formation, or use sodium with high osmotic pressure to prevent periodontal disease, hemostasis The active aminocaproic acid, allatoin, vitamins, etc. are used. Occasionally, hydroxyapatites are used that make up the damaged dentin crown, are effective for sensitive teeth, and also have a whitening effect. As the binder for the solid component and the liquid component, celluloses, carrageenans, gums and the like are used. As a foaming agent, anionic surfactant sodium lauryl sulfate, and as a stabilizer, nonionic surfactant polyoxyethylene or a copolymer of propylene (poloxamer), or Additives such as detergents, fragrances, pigments, and neutralizers are mixed with chemicals such as coconut oil and fatty acid esters.

  As a prior art related to the present invention, Patent Document 1 (a composition of a whitening toothpaste containing a Kampo component) is a powder of a Korean medicine material such as Minoko, which is effective for tooth whitening, or its There is a composition of a whitening dentifrice containing an extract and prophosphate and fluorine. Patent Document 2 (a method for producing a powdered Chinese herbal dentifrice) describes a Korean medicine material such as talc powder and oat stone that are pulverized to a powder of 400 mesh or less in 60% by weight of powder salt and bamboo salt mixed 1: 1. A method for producing a powdered Chinese herbal dentifrice comprising: On the other hand, Patent Document 3 (taste protection, mild oral hygiene composition) includes toothpastes, gels, powders, and mouth rinses, protein derivatives derived from collagen, natural emulsifiers Lecithin, highly foaming disodium lauryl sulfosuccinate, flavor oil, anti-cavity fluoride and the like. Further, Patent Document 4 (medicine containing bittern) contains a bitter bite as a main ingredient, and contains a mineral component that tends to be lacking by modern people as an oral treatment drug to be taken percutaneously. Disclosed is an oral therapeutic agent that can be easily prepared and manufactured at low cost by improving the medical condition. Patent Document 5 (Toothpaste and its production method) added shell powder baked at 1,100 to 1,300 ° C. to an aqueous acetic acid solution to obtain a neutral calcium acetate solution having a pH of 6 to 8, which was evaporated to dryness. Toothpaste can suppress the growth of bacteria inside the oral cavity. Patent Document 6 (composition for preparation of oral dentistry with herbs and a method for preparing the same) includes Citrus karna raf., Zantoxylum armatum D.C. and Azadiracta Indica. A medicinal herb powder such as Azadirachta indica A.Juss .: or an extract-containing dental treatment composition for preventing the formation of dental plaque and caries, powder (toothpaste), paste , Gels, dental packs, dental floss, mouth washes and chewing gums. In addition, Patent Document 7 (oral oral composition) is pharmaceutically acceptable as one or more drugs selected from the group consisting of tin ions, zinc ions and copper ions, polyphosphate anticalculus agents, as antibacterial agents. A topical oral composition containing an oral carrier. The above-mentioned patent documents are oral hygiene compositions or dental treatment compositions, which are technical compositions that are completely different from the powdered toothpaste of the pure herbal medicine of the present invention.

  In general, the oral cavity in the human body is a space in the mouth that is connected to the pharynx from the lips at the front of the oral cavity to the back of the mouth, and is related to food and drink such as mastication, oral digestion, and taste. In addition to various functions, it is also involved in the endocrine action and respiration of salivary glands, including the construction of speech sounds. That is, all the nutrients obtained through food and beverage intake, the primary barrier that pathogens in the air enter the human body, and directly related to the mastication function, vocalization function, aesthetic function of the appearance, The gums that support this, the organs like the tongue that feel the taste and are involved in the vocalization function together with the teeth are organically connected to each other and are important organs that ensure the health of the human body. However, the reality is that such important oral hygiene and health management are entrusted to dentifrices made of artificial compounds. In recent years, interest in dental health and oral hygiene has been increasing above all, while pursuing a healthy life and well-being through the extension of human life. Here, when all foods and drinks enter the oral cavity, first feel the taste and eating feeling through mastication with the tongue and teeth inside the oral cavity, stimulate the digestive glands, secrete digestive fluids and promote digestion of food and drink Since it plays a role, in particular, products in which oral hygiene preparations are made of natural products are preferred over chemical products. However, the current situation is that consumers who are familiar with various liquid dentifrices composed of chemical components for dental health and oral hygiene use liquid dentifrices without any sense of resistance.

Korean open patent 10-2004-0066313 Korean Registered Patent No. 10-0659915 Japanese Published Patent No. 5-170632 Japanese Patent Publication No. 2004-300043 Japanese Published Patent No. 2007-31286 Japanese published patent 2007-527849 Japanese Patent Publication No. 2008-143910

  Recently, interest in dental hygiene and health management has been increasing, but commercially available dentifrices are generally Chinese herbal medicine extracts in addition to toothpastes, binders, whitening agents, wetting agents and additives, or Most of the preparations are liquid-phase toothpastes in a gel state, which are chemically prepared from extracts that are effective for whitening teeth. However, the main component of these dentifrices used for the prevention of caries, plaque and plaque, tartar, bad breath is often left in the oral cavity after use, and if this residue accumulates, It weakens the teeth and tongue, gums and oral wall, causing inflammation in the oral mucosa and causing exfoliative gingivitis. Moreover, not only does the oral cavity be strongly stimulated during use to numb the taste, but the chemical components of the preparation still remain after use and the food and drink residue cannot be completely removed. That is, it can be said that various dentifrices used for oral health management may adversely affect the oral cavity and teeth.

  In view of the above circumstances, the present inventor of the present application is prominent in dental health and oral care based on the knowledge gained through multi-year experiments and intensive studies. An object of the present invention is to provide a powder dentifrice composition and a method for producing the same, in which natural ingredients and herbal medicine ingredients having various effects are blended at a fixed rate.

  The composition of the powder dentifrice of the present invention is bamboo salt (bamboo salt), wheat flour, dried white salmon (baked alum), pine oil (matsuya ni), lotus meat (lotus meat), natural ingredients useful for the human body, After heating or drying the fine spicy, sesame, sandalwood, kikyo and enokitake mushrooms and pulverizing them with a predetermined mesh, the resulting powder is mixed at a certain ratio. Formulated composition. This is mixed to produce a powder dentifrice.

  The composition of the powder dentifrice of the present invention can prevent the formation of plaque by a powerful antibacterial action, prevent the accumulation of tartar and tongue coating, remove bad breath by the cleaning effect and anti-inflammatory action and In addition to preventing various internal inflammations, it also provides tooth whitening effect by preventing tooth discoloration. In addition, the present invention is a powder dentifrice produced by a process in which natural chemicals are heated, dried, and pulverized, regardless of the chemicals and production methods that are harmful to the human body. Since it is easily dissolved by saliva in the mouth, a brushing effect similar to that of a toothbrush can be obtained by simple gargle alone. In addition, the same effect as drinking a Chinese medicine can be obtained even if swallowed without being exhaled while rinsing with water. In addition, although it cannot be said that it is a common routine, according to a plurality of experimenters who customarily swallowed after gargle, there is a report that there was also an improvement effect of the visceral system.

  Moreover, when it is used together with an existing liquid phase dentifrice, the liquid phase dentifrice is decomposed and no residue remains in the mouth or in the gargling water discharged.

  The present invention provides a powder dentifrice composition comprising bamboo salt, wheat flour, dried white potato, pine oil, lotus meat, fine spicy, sesame, peony, bellflower and enokitake as ingredients.

  In the present invention, the blending ratio of the powder dentifrice composition is 25 to 28% by mass of bamboo salt, 23 to 28% by mass of wheat flour, 10 to 12% by mass of dried white potatoes, and 10 to 12% of pine resin per unit mass of the whole. %, Lotus meat 10-12% by weight, spicy 1-3% by weight, hemp 2-4% by weight, peony 2-4% by weight, bellflower 1-3% by weight, enokitake mushroom 1-3% by weight. It is preferable.

  In the present invention, the powder dentifrice composition preferably has a particle size of 150 to 180 mesh.

  More specifically, the composition of the powder dentifrice contains 0.1 to 150 μm bamboo salt, 0.1 to 25 μm flour, 0.001 to 3 μm dried white rice, 0.1 to 50 μm pine resin, 0.1 lotus meat It is preferable to have a particle size of ˜55 μm, fine spicy 0.1-10 μm, urn 0.1-10 μm, peony 0.1-25 μm, bellflower 0.1-70 μm, enokitake 0.1-80 μm.

  In the present invention, the bamboo salt, dried white mackerel, and pine oil are powders obtained through a heat treatment and pulverization process, and lotus meat, fine spicy, sesame, peony, bellflower, and enokitake are dried and crushed in a shaded background. Provided is a method for producing a powder dentifrice composition, wherein the powder is produced through a blending step and a mixing step at a certain blending ratio together with wheat flour.

  Moreover, in the manufacturing method of the powder dentifrice composition of this invention, the composition of the said powder dentifrice WHEREIN: The blending ratio per unit mass of the whole is 25-28 mass% of bamboo salt, 23-28 mass% of wheat flour, withering, respectively. White potato 10-12% by weight, pine resin 10-12% by weight, lotus meat 10-12% by weight, fine spicy 1-3% by weight, ramie 2-4% by weight, peony 2-4% by weight, bellflower 1-3% by weight %, Enokitake mushrooms are blended at 1 to 3% by mass, and are preferably produced by mixing them.

  Hereinafter, the composition of the powder dentifrice of this invention and this manufacturing method are demonstrated in detail.

  The present invention is composed of the above-mentioned 10 kinds of natural medicines or foods, among which the bamboo salts (Takeshio) and dried white potatoes (baked alum) are heated and solidified at high temperature. Use with post-ground powder. Wheat flour, which is a cereal food, is used by pulverizing organically grown wheat that has been sufficiently dried and maintained at a moisture content of 14% or less into a powder of 150 to 180 mesh. Further, pine resin, which is a natural resin, is obtained by pulverizing a purified rosin obtained by boiling the matsuya at a high temperature. The other 6 kinds of lotus meat, spicy, cinnamon, peony, bellflower, enokitake, etc. are used after being crushed to a powder of 150-180 mesh while keeping the moisture content below 12% by drying in the shade. .

  Next, the respective purification methods and the effects in the oral cavity and human body will be individually described in detail for the ten types of compositions.

  (1) Bamboo salt is a toxin that is harmful to the human body by heating with bamboo cylinders at a high temperature of 1,300 to 2,000 ° C. once to 9 times by the traditional bamboo salt extraction method. It is a salt made by removing the ingredients from the process (processed by a preparation method established by traditional Korean medicine). In this embodiment, the raw bamboo cylinder grown for 3 to 5 years is filled with mineral-rich sun salt (produced on the west coast of Korea) for about 7 to 8 minutes. Bake 8 times repeatedly at 800 ° C. using fire. After that, at the time of the last 9th baking, after pine oil is sown in the firewood of dried pine, it is heated to 1,300 ° C. or more by the bonfire. At this time, the salt is completely dissolved and flows down in a mud. At this time, when the liquid obtained by synthesizing the moisture of the bamboo, that is, the bamboo shoot liquid and the dissolved salt and the sulfur component of the sealed ocher, is cooled overnight, it solidifies like a stone block. This is pulverized to 150-180 mesh to produce a powder. This is so-called bamboo salt. In addition, when reliable, it is also possible to use a commercially available preparation as described above. Bamboo salt is preferably used in an overall unit mass ratio of 25 to 28% by mass, preferably 26.6% by mass. Moreover, it is preferable to use the particle size of the bamboo salt of 0.1 to 150 μm, preferably 5 to 130 μm (FE-SEM [scanning electron microscope manufactured by Hitachi High-Tech Co., Ltd.] was used for particle size analysis). This powdered bamboo salt from which various impurities in the sun salt have been removed has a salty taste, but its aftertaste is unsatisfactory and has a sweet taste and contains various components useful to the human body. Bamboo salt is effective for tooth gum disease, and also has special effects on tonsils, esophagus and stomatitis, as well as brushing of teeth, as well as simple gargle. In addition, it has special effects on prevention of dental caries and periodontitis, soreness of the oral cavity, and tooth pain. There are also reports of detoxification of nicotine in the body when taken with soup soaked in kelp. In the manufacturing process of bamboo salt, bamboo and sulfur spirit, pine pine oil components, soil soil molecules, iron and firepower are synthesized in the salt that promotes metabolism, and the so-called five elements The strength of extinguishing and cleansing is further strengthened. Therefore, bamboo salt is a healthy salt that can be widely used for any disease, regardless of humanity. Bamboo salt that alkalizes acidic foods and supplies minerals that are beneficial to the human body is attracting attention as a valuable health food that is irreplaceable for modern people who are exposed to various types of pollution.

  (2) Wheat flour is flour (product of Toago Flour Milling Co., Ltd.) produced by milling wheat cultivated by organic farming into fine particles, and 150 grams of well-dried organic farming wheat having a water content of 14% or less. It is preferable to use it after pulverizing to ~ 180 mesh and blending this flour with 23 to 28% by mass, preferably 25% by mass. Moreover, it is preferable that the particle size of this wheat flour is 0.1-25 μm, preferably 5-8 μm. Wheat flour has warm properties and sweetness, and when used for food, it makes the intestines and stomach strong, strengthens the energy, and promotes the activities of the intestines. According to the East Medical Treasure Book (Korean Traditional Chinese Medicine), wheat flour is also used as a therapeutic agent for tetanus, jaundice and swelling, enhancing immune function, preventing aging and degrading harmful cells. Are listed. Furthermore, at the same time as it is put into the mouth, it has an excellent cleaning effect that it melts softly and rinses out various impurities, removing impurities such as animal fat remaining in the mouth of modern people who prefer meat eating and residues in internal organs. It is also known to serve as a lubricant that prevents damage to the dentin of the tooth due to brushing such as a toothbrush, and to perform a particularly excellent function for the whitening effect of the tooth.

  (3) Boiled alum (burnt alum) is a white powder that has been baked alum and has been freed of water of crystallization, and is also called dry. A lighter powder has a lower solubility in water than alum, so it dissolves gradually and becomes an almost transparent solution. In the method for producing a dried white leopard, first, the white birch is heated to 120 ° C. or more and boiled, and the white birch raised in a liquid state is further solidified when cooled at room temperature. When this is pulverized to 180 mesh or less, it becomes milk-colored powder like flour. It is preferable to use 10-1 to 12% by mass, preferably 11.7% by mass, of this dried white potato. Moreover, it is preferable to use a grain size of dried white cocoons of 0.001 to 3 μm, preferably 0.003 to 1 μm. Baked white potatoes are effective in inhibiting and preserving bacteria due to their acidity, and are particularly effective in treating inflammation of the gums, tongue and palate. That is, it is also effective in preventing inflammation of the oral respiratory system such as sore throat, tonsillitis, and sore throat. In particular, it binds with pine resin in the composition and well harmonizes the beneficial components of the present powder composition, and adsorbs the composition to each part of the oral cavity, particularly strengthening the gums and symptoms of tooth shaking It is also effective in preventing periodontitis by improving and treating

  (4) Pine resin is a pine sap, the first of which is a colorless and transparent liquid, but it becomes a white solid that comes out of resin acid as it becomes cloudy and becomes cloudy over time Are deposited. After collecting pine resin and solidifying it naturally, it is boiled in kuwa (mulberry tree) lye (combustion liquid) or boiled in sake (alcohol) and then immersed in cold water to repeat the process of pine oil. The impurities are completely removed and the center of the sap becomes solidified like a transparent brown cocoon. When the solidified pine resin is placed in a stainless steel container and heated with high heat, the water remaining in the interior is further evaporated to become a transparent coconut (liquid). The liquid is cooled to form a lump and then pulverized to 180 mesh or less to form a powder.

  The pine resin purified as described above is preferably used in an amount of 10 to 12% by mass, preferably 11.7% by mass. Moreover, it is preferable to use a pine resin particle size of 0.1 to 50 μm, preferably 5 to 44 μm. The rosin has a warm sweetness and bitterness, is non-toxic, calms the fever and the viscera, is effective in gingivation, and has the effect of stopping pain and the like. In addition, since it has an anti-inflammatory action, it is effective for dental caries treatment. In addition, it has excellent bactericidal properties, removes various harmful bacteria remaining on the gums and tongue, and removes calculus sandwiched between teeth and tongue coating deposited on the tongue.

  (5) After the lotus flower is collected and the seed coat of the lotus seed is removed, it is dried in the shade to a moisture content of 15% or less, into a powder of 180 mesh or less. Make it. The lotus meat is used in a blend of 10 to 12% by mass, preferably 11.7% by mass. Also, it is preferable to use a lotus meat having a particle size of 0.1 to 55 μm, preferably 5 to 51 μm. In addition, the lotus meat has a warm and sweet taste and astringency, supplements the blood and qi of human twelve meridians, replenishes the viscera and strengthens the heart to calm the heart. . It is rich in vitamins B1 and minerals such as calcium, phosphorus, iron, and potassium, and provides beneficial nutrients in the oral cavity. In particular, lecithin contained in lotus meat regenerates damaged hepatocytes and performs functions such as improving cholesterol levels, supplying nutrients to the brain, antioxidants, and improving blood circulation. In addition, since it has the softness to dissolve water and oil well, it is effective for removing animal fat remaining in blood vessels and oral cavity. Therefore, it is particularly effective for removing fine contaminants remaining in the mouth. It also cleans the gums and tongue, smoothes blood circulation, and maintains various tissues in the oral cavity. In particular, the salivary gland is stimulated during brushing and the saliva is secreted to make the mouth moist, so that the cleaning effect is excellent and the saliva becomes clear after use. It also combines with other various compositions to remove tongue tongue and bad breath.

  (6) As for the spicy (saicin), it is a rind of the roots of Aristolochiaceae (Asiasarum heterotropoides F. Maekawa var. Mandshuricum F. Maekawa) or water. After that, it is dried in the shade to a moisture content of 15% or less to produce a fine powder of 180 mesh or less. This powder is used by blending 1 to 3% by mass, preferably 2.5% by mass. The fine particle size is preferably 0.1 to 10 μm, preferably 5 to 8 μm. Spicy spicy food is warm and spicy and non-toxic, so it mainly treats wind numbness, warming the internal air (warming the internal organs and lowering the air), and sore throat ( Symptoms of throat irritation and throat narrowing or clogging) and nasal congestion are resolved. Add bile to relieve head wind (chronic headache and scalp symptom) and help improve vision. It also eliminates wrinkles and is used as a sweating agent. It is effective for pain relief and gingivitis caused by wind-cooled toothache and caries. It is effective for removing bad breath and moisturizing and whitening teeth.

  (7) Cimicifuga heracleifolia is a root of a perennial plant (rhizocarp) obtained from a perennial plant (Ranunculaceae) of a dicotyledonous plant (Dicotyledoneae), Ranunculaceae. After that, it is dried in the shade to a moisture content of 15% or less to produce a powder of 180 mesh or less. This powder is used in an amount of 2 to 4% by mass, preferably 3.3% by mass. Moreover, it is preferable to use a sesame particle size of 0.1 to 10 μm, preferably 2 to 8 μm. The nature of urn is sweet and bitter, but it is not toxic, so it can be used as a treatment for sores due to inflammation in the mouth and bacterial infections even when raw. Also, when used with bamboo salt, there is a synergistic effect. It is also effective for treatment when periodontitis causes swelling of the gums and severe toothache, or when bloody pus develops from the gums while shaking the back teeth. According to the above-mentioned east medicine treasure book, it can detoxify 100 kinds of poisons, and cures sore throat and inflammation in the mouth by removing waste products of hundreds of energy, energy, energy, semen and spirit It is recorded.

  (8) Juniper (Rhizome rhizome) is prepared by washing the roots of Angelica Dahurica with water and then drying in the shade to a moisture content of 15% or less to obtain a powder of 180 mesh or less. It is preferable to blend 2 to 4% by mass, preferably 3.3% by mass of this powder. In addition, it is preferable to use particles having a particle size of 0.1 to 25 μm, preferably 6 to 21 μm. Beaky is warm and pungent and non-toxic, so it can cause wind fever (various symptoms due to heat, such as chills caused by high fever and yellow tongue coating on the tongue) and vertigo (dizziness due to cold, stiff neck) ) Can be treated. It is effective in removing various stains on the face and also has antibacterial and anti-inflammatory effects. In addition, it is effective for swelling and bleeding of gums caused by periodontitis, but it is particularly effective for treating inflammation of the back teeth, and also effective for whitening teeth.

  (9) Kikyo (Korean: Korean folk name Doraji) (Platycodon Grandiflorus) dried a certain amount of Doraji in natural wind and dried it like ginseng, and then the water content was 15% or less. To a powder of 180 mesh or less. It is preferable to use this powder in an amount of 1 to 3% by mass, preferably 2.1% by mass. The particle size of the powdered bellflower is 0.1 to 70 μm, preferably 5 to 52 μm. Kikyo has a low temperature, has a pungent taste and a bitter taste, can clarify the lungs in particular and can eliminate depression, and can eliminate coldness in the abdomen. Its main component is saponin, and the pharmacological effects of the saponin component are well-known, and the premise of the East Medical Treasure Book includes tonsillitis, abdominal pain, hemostasis, cough (cough), expectoration, asthma, pharyngitis, etc. Recorded to be used as a therapeutic agent.

  (10) Enokitake (Flamulina velutipes) is a white mushroom of Trichomataceae of the basidiomycete Agaricales, and after washing a certain amount with water, it is dried in the shade for about a month, It looks like brown fallen leaves. This is dried to a moisture content of 15% or less to produce a powder of 180 mesh or less. The powdered enokitake mushroom can be used as a commercial product because its method is simple. It is preferable that enokitake is blended in an amount of 1 to 3% by mass, preferably 2.1% by mass. The particle size of the powdered enokitake is 0.1-80 μm, preferably 18-68 μm. Enokitake mushrooms are warm and effective as medical products for reducing blood cholesterol, liver and gastrointestinal diseases. In particular, the white stem part activates the functions of the respiratory system and is rich in high-protein, low-calorie and natural vitamins, so it promotes the growth of bones and teeth, so it is especially useful for growing children Good food. Guanylic acid contained in enoki mushrooms is known to be effective in reducing cholesterol levels and facilitating blood circulation, arteriosclerosis, heart disease, and hyperlipidemia. In addition, it stimulates the immune system, protects the body from infection with various viruses, suppresses the occurrence of cancer, and has good components for brain development. In addition, the abundant dietary fiber in mushrooms cleans the tooth surface to prevent tartar and contains a strong antibacterial component called enokipodins, which also prevents caries fungus growth and prevents tooth decay There is a special effect. Moreover, coloring of teeth by green tea or coffee can be prevented.

  As described above, the effects and effects of each component are described in the composition of the present application with reference to the traditional Chinese medicine documents such as “Hong Kong” and “Eastern Medical Treasure Book” and the records of traditional Korean medicines from Korea. The method for preparing each traditional Chinese medicine described above is a preferred example. Of course, as long as the original function of each chemical material is not impaired, a chemical material prepared by a method other than the above-described preparation method can also be used for the composition of the present application. The present invention is a new dentifrice composition in which these herbal medicines are made to exhibit a new effect by a unique formulation. In particular, each of the above ingredients has a distinctive taste (five tastes: acid, bitter, sweet, spicy, mochi), and these tastes are mixed to create a unique taste created by agitation and synergy. Yes.

Examples 1-6
Ten kinds of chemicals constituting the above-described powder dentifrice of the present invention were prepared by blending as follows according to each use amount. As described above, the minerals bamboo salt and dried white cocoon were powders manufactured by the method, which were heated at a high temperature and then solidified and pulverized. For cereal flour, commercially available products are used, and for pine resin, powder obtained by crushing lumps of rosin that has been boiled at high temperature and pulverized, and other lotus meat, spicy, sesame, peony, bellflower For enokitake, etc., commercial products manufactured by law were used. As described above, 10 kinds of chemicals were weighed and blended in respective amounts, and then further mixed and pulverized by a pulverizer. In particular, bamboo salt, dried white mackerel, and pine resin having a high molecular weight were used as fine powders of 150 to 180 mesh in order to completely mix with other Korean medicine materials (see Table 1 below).

Comparative Examples 1-3
Comparative Example 1 is a general salt instead of bamboo salt, white birch (commercial product) instead of dried white birch, Comparative Example 2 is white birch instead of dried white birch, and Comparative Example 3 is larger than wheat flour. Except using each flour, it mix | blended and manufactured by the same method as Examples 1-6. The compounding ratios of the components of Examples 1 to 6 and Comparative Examples 1 to 3 are summarized in Table 1 below.

  For reference, the dentifrice of the present invention provided in Example 1 of Table 1 above was used as a sample, and the water content of each was analyzed by the Korea Food Research Institute, a subsidiary of the Ministry of Knowledge Economy of the Korean government. As a result, the following test report on January 13, 2009 (file No. AO2009-01-13-010) was received and is shown in Table 2.

  Various effects on the powder dentifrice composed at the same mixing ratio as in Table 1 will be described in detail through the following test examples.

Test Example 1 Measurement of whitening effect on teeth To compare the whitening effect on the powdered toothpastes of Examples 1 to 6 and Comparative Examples 1 to 3 in Table 1 above, the following measurement was performed. First, a mixture of tobacco, coffee, tea, sugar, calcium, and the like is made into a gel, and then this gel-like product is fixedly mounted on a rotating plate mounted on a rotatable device. After moving into the tooth specimen extracted from a healthy person in their 20s to 30s, the exposed area is horizontal x vertical = 2 mm x 2 mm, and the remaining part is covered with epoxy resin, and this is a specimen. As above, it was fixed in the bottomed container with an epoxy resin. In this state, the stain on the specimen was dried while rotating the bottomed container for 3 days. At this time, an incandescent lamp was installed in the central upper space of the rotating plate in order to promote the drying of the stain. Measure the whiteness of the stain-formed specimen using a color difference meter (SZ, Nippon Denshoku), fix the specimen on a reciprocating kneading force measuring instrument, and then move the soft toothbrush bristles to the axis of motion. It was fixed so that it would rub against the specimen. 0.5 g of each of the compositions of Examples 1 to 6 and Comparative Examples 1 to 3 was simultaneously placed on the ends of the toothbrush bristles and rotated so as to reciprocate 180 times per minute. The color difference was measured again, the degree of improvement in whiteness was converted as a percentage, and the results are shown in Table 3.

  On the other hand, as a control group, pine salt dentifrice (Amore Pacific product: control group 1) and bamboo salt dentifrice (LG Life Health Co., Ltd. product: control group 2) on the market are used to improve whiteness. After measuring the rate, it was compared with the examples of the present invention.

  From the above results, in Comparative Example 3 in which no flour was added and in Examples 1, 2, 3 and Examples 4, 5, 6 and Comparative Examples 1 and 2 in which a little amount of flour was added, the whiteness improvement rate was considerable. It showed a meaningful difference.

Test Example 2: Measurement of Detergency and Whitening Effect Detergency was measured for Examples 3 to 6 and Comparative Example 2 (see Table 3), which were judged to have a whitening effect in Test Example 1. After the petri dish is soaked in a mixed solution of 10% coffee and 5% caramel for 2 days to completely change the color of the surface, the petri dish is taken out and dried, then a color difference meter (colorimeter, CR-241, Minolta, Japan) ) To measure the whiteness. A Petri dish was placed in a solution diluted by mixing powder dentifrice and purified water 5: 5 and brushed 1,000 times with a nylon toothbrush in a horizontal reciprocation stroke. Thereafter, water was completely removed and the whiteness was measured by a color difference meter to evaluate the cleaning power of the powder dentifrice. The results are shown in Table 4. The control group 1 on the market and the control group 2 described above as a control group were used to measure the improvement in detergency and whiteness, and then compared with the composition of the present invention.

  As described above, the detergency and whitening effect were measured through the brushing test. As a result, comparatively meaningful detergency and whiteness improvement rate were shown in Examples 4, 5, and 6 and Comparative Example 2 in which a relatively large amount of flour was added. It was done. In particular, the improvement rate of Example 6 and Comparative Example 2 with the highest content of bamboo salt and flour is high.

Test Example 3 Measurement of whitening effect on human subjects Among the blending ratios of the present invention, Examples 4, 5, 6 and Comparative Examples 1 and 2 having relatively good whitening effect were used directly for 3 months. The whitening effect was measured. After selecting 100 healthy individuals with relatively yellow teeth and measuring the color tone with a colorimeter (Trubyte Bioform) in advance, the average color tone values were classified into 4 groups of 25 people each having almost the same color tone. A powder dentifrice composition was dispensed for use. In order to confirm the increase in the brightness of the teeth, 10 types that are easily sensibly discriminated out of 24 standard standards according to the lightness in the Truebyte Bioform colorimeter are selected, and the lightness value is set to at least one point for each. An evaluation score of up to 10 points was given. Before using the test dentifrice, evaluate the brightness value of each group of teeth based on the above criteria to one decimal place, evaluate the brightness value after brushing for 3 months, and then the brightness value before the test The increase rate of the average brightness value with respect to was calculated. The improvement rate of whiteness was measured using the above-mentioned control group 2 on the market as a control group, and then compared with the examples of the present invention.

  The lightness value increase rate showed significant lightness value improvement rate in Examples 4, 5, and 6 and Comparative Example 2 in which a relatively large amount of flour was blended.

Test Example 4 Bactericidal power test In order to compare the bactericidal power effect on the powder dentifrices of Examples 1 to 6 and Comparative Examples 1 to 3, measurements were made as follows. Streptococcus mutant ATCC 27607, 6735 which causes oral diseases such as dental caries by putting the composition of the powder dentifrice of this Example into BHI (Brain Heart Infusion) broth by 0.02% to 0.5% by concentration. After inoculating the bacterial solution and culturing at 37 ° C. for 48 hours, each medium is smeared on agar with 1 platinum loop and further cultured for 48 hours, after which the minimum concentration at which the test bacteria do not grow further is minimized. The growth inhibitory concentration (MIC) was taken as the MIC (minimum inhibiting concentration), and the results are shown in Table 6. The improvement rate of bactericidal activity was measured using the above-mentioned control group 1 and the above-mentioned control group 2 on the market as the control group, and then compared with the composition of the present invention. The results are shown in Table 6.

  As a result of measuring the inhibitory effect on oral inflammation through the bactericidal power test as described above, the comparatively significant increase in bactericidal power was shown in Examples 3 to 6 and Comparative Example 3 in which a relatively large amount of bamboo salt and dried white straw was added. It was.

Test Example 5 Specimen teeth processed as in Test Example 1 for the composition of the present invention having a relatively high whitening effect, cleaning effect and bactericidal effect as in Examples 3 to 6 and Comparative Example 3 The bottom of was ground using sandpaper and 1 μm diamond paste. Before grinding, the thickness was measured (Pioneer calipers) and adhered to a test plaque for evaluation of the degree of polishing using an adhesive, and then subjected to a load of 500 g. A 200 mm disc with a soft scouring blanket attached to a general kneader was prepared, and powder toothpaste and water were diluted 50:50, and 10 ml was put into the scouring blanket every 10 minutes on a rotating disc. . The grinding was performed at a speed of 100 rpm for 5 hours. The thickness of the specimen after the grinding was measured, and the difference is shown in Table 7. As the subject group, the pine salt dentifrice (supra control group 1) and the bamboo salt dentifrice (previously control group 2) were measured and the degree of grinding was measured, and then compared with the composition of the present invention. The results are shown in Table 7 below.

  As a result of measuring the degree of grinding from the above results, Examples 3 to 6 and Comparative Example 3 were not different in surface condition compared to the control group, and there was no decrease in thickness, or a slight decrease compared to the control group. I was able to confirm that.

  The powder dentifrice of the present invention shows much better results than the conventional commercial products of liquid dentifrice, as confirmed by the measurement of whitening effect, cleaning power, bactericidal power, degree of grinding, etc. Because it has an excellent effect on whitening of the skin, it is highly available in the manufacturing industry for health and hygiene products.

Claims (5)

  A composition of a powder dentifrice comprising powders of bamboo salt, wheat flour, dried white mackerel, pine oil, lotus meat, fine spicy, hemp, peony, bellflower, and enokitake.   The composition of the above-mentioned powder dentifrice has a composition ratio per unit mass of 25-28% by mass of bamboo salt, 23-28% by mass of flour, 10-12% by mass of dried white rice, 10-12% by mass of pine resin, lotus meat 10 to 12% by mass, 1 to 3% by mass spicy, 2 to 4% by mass of cannabis, 2 to 4% by mass of peony, 1 to 3% by mass of bellflower, and 1 to 3% by mass of enokitake mushroom, respectively. The composition of the powder dentifrice of Claim 1 characterized by the above-mentioned.   The powder dentifrice composition according to claim 1, wherein the powder dentifrice composition is composed of powder having a particle size of 150 to 180 mesh. Bamboo salt, dried white mackerel, and pine oil are powders obtained through heat treatment and pulverization process. Bamboo salt, flour, dried white mackerel, pine oil, lotus meat, fine spicy, hemp, peony, bellflower, and enokitake , characterized by being mixed and manufactured through a mixing process at a certain mixing ratio with wheat flour. A method for producing a powder dentifrice composition comprising the above powder as a component .   The composition of the above-mentioned powder dentifrice has a composition ratio per unit mass of 25-28% by mass of bamboo salt, 23-28% by mass of flour, 10-12% by mass of dried white rice, 10-12% by mass of pine resin, lotus meat 10 to 12% by mass, 1 to 3% by mass spicy, 2 to 4% by mass of cannabis, 2 to 4% by mass of peony, 1 to 3% by mass of bellflower, and 1 to 3% by mass of enokitake mushroom, respectively. The method for producing a powder dentifrice composition according to claim 4.