JP3335770B2 - Evaluation method of scale peelability - Google Patents

Evaluation method of scale peelability

Info

Publication number
JP3335770B2
JP3335770B2 JP16076994A JP16076994A JP3335770B2 JP 3335770 B2 JP3335770 B2 JP 3335770B2 JP 16076994 A JP16076994 A JP 16076994A JP 16076994 A JP16076994 A JP 16076994A JP 3335770 B2 JP3335770 B2 JP 3335770B2
Authority
JP
Japan
Prior art keywords
scale
test piece
magnet
amount
steel material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP16076994A
Other languages
Japanese (ja)
Other versions
JPH085544A (en
Inventor
繁夫 古川
博 日坂
正彦 清水
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to JP16076994A priority Critical patent/JP3335770B2/en
Publication of JPH085544A publication Critical patent/JPH085544A/en
Application granted granted Critical
Publication of JP3335770B2 publication Critical patent/JP3335770B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【産業上の利用分野】本発明は、鋼材,特にスケール発
生量の少ない鋼材についても、精度よくかつ効率的にス
ケール剥離性あるいは密着性を評価する方法に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for accurately and efficiently evaluating the scale peelability or adhesion of a steel material, especially a steel material having a small amount of scale.

【0002】[0002]

【従来の技術】鋼材のスケールは、冷間加工時に剥離し
粉塵となって飛散するために作業環境を著しく悪化さ
せ、大きな問題となっている。従って最近では、その対
応策としてスケールの測定方法の必要性が高まってい
る。
2. Description of the Related Art A scale of steel material is a serious problem because it peels off at the time of cold working and is scattered as dust, thereby significantly deteriorating the working environment. Therefore, recently, there is an increasing need for a scale measurement method as a countermeasure.

【0003】また冷間加工は、その対象物により加工度
(加工歪)が大きく異なり、それぞれの条件におけるス
ケール剥離性の定量的な把握も必要であった。従来スケ
ール剥離性の評価方法としては、線材等において実施さ
れているスケールの機械的剥離性(以下、メカデス特性
と称する)を測定する下記のような方法があった。
[0003] In cold working, the degree of working (working strain) varies greatly depending on the object, and it is necessary to quantitatively grasp the scale peelability under each condition. Conventionally, as a method for evaluating scale releasability, there has been the following method for measuring the mechanical releasability (hereinafter, referred to as mekades characteristics) of a scale performed on a wire or the like.

【0004】まず材料を引張試験用試験片と同じ長さに
切断し、引張試験機でメカニカルデスケーラーのベンデ
ィングローラーと同じ伸びを与え、スケールを剥離させ
てそれによる試験片の重量減少量から線材のメカデス特
性を求めていた。
[0004] First, the material is cut to the same length as the tensile test specimen, the tensile tester gives the same elongation as the bending roller of the mechanical descaler, the scale is peeled off, and the weight loss of the test specimen is reduced. Wanted the mechanical death characteristics of

【0005】[0005]

【発明が解決しようとする課題】しかし上記の方法で
は、大きな試験片でスケール剥離による微少な重量変化
を測定するために、重量測定の際の読み取り誤差が大き
く、特に最近ではスケール発生量の少ない鋼材が開発さ
れ、その測定誤差が益々大きな問題であった。
However, in the above-mentioned method, since a small weight change due to scale peeling is measured with a large test piece, a reading error at the time of weight measurement is large. Steel was developed, and its measurement error became an increasingly big problem.

【0006】またこの方法では、上述のように試験片側
の重量を測定するので、例えば引っ張り歪み付与の際の
チャック圧痕による試験片の削れも発生し、これも測定
誤差を大きくし、更に所定の歪みの際の正確なスケール
剥離量の測定を困難にしていた。
Further, in this method, since the weight of the test piece is measured as described above, the test piece may be scraped by, for example, chuck indentation at the time of imparting tensile strain, which also increases the measurement error and further increases the predetermined error. This makes it difficult to accurately measure the amount of scale peeling during distortion.

【0007】本発明は上記課題を解決するもので、例え
ばスケール発生量の少ない鋼材についても、精度よくか
つ効率的にスケール剥離性を評価する方法を提供する。
[0007] The present invention solves the above-mentioned problems, and provides a method for accurately and efficiently evaluating scale peelability even for a steel material having a small amount of scale generation.

【0008】[0008]

【課題を解決するための手段】本発明は、両端をテーピ
ングして被評価材とした試験片を、引張試験機により一
定の歪みになるまで荷重をかけ、この一定歪みに達する
までの前記試験片から剥離落下したスケールをマグネッ
トで吸着し、この吸着したスケール重量を秤量してその
秤量値によって鋼材のスケール剥離性を評価することを
特徴とするスケール剥離性の評価方法である。
SUMMARY OF THE INVENTION According to the present invention, a test piece taped at both ends and used as a material to be evaluated is subjected to a load by a tensile tester until a constant strain is reached, and the test is carried out until the constant strain is reached. This is a method for evaluating scale releasability, in which a scale peeled and dropped from a piece is adsorbed by a magnet, the weight of the adsorbed scale is weighed, and the scale releasability of the steel material is evaluated based on the weighed value.

【0009】[0009]

【実施例】以下本発明の実施例およびその作用を、図面
に基づいて詳細に説明する。
DESCRIPTION OF THE PREFERRED EMBODIMENTS Embodiments of the present invention and the operation thereof will be described below in detail with reference to the drawings.

【0010】図1は本発明の一実施例を示す略側面図で
あり、先ず中央部に被評価面2としての一定の面積を残
し、その両端をビニールテープでテーピング3を施した
試験片1を引張試験機4に装着し、その両端に試験片1
の歪み量を測定する伸び計5をセットしている。
FIG. 1 is a schematic side view showing one embodiment of the present invention. First, a test piece 1 having a fixed area as a surface to be evaluated 2 left in the center and taping 3 with vinyl tape at both ends. Is attached to a tensile tester 4 and a test piece 1
The extensometer 5 for measuring the amount of strain of is set.

【0011】そして試験片1の被評価面2両側の相対し
た位置に固定治具7によりマグネット6を固定し、この
状態で試験片1を引張試験機4で引っ張り、ある一定の
歪みを与えた時点でその歪みを保持し、その時点までに
試験片1から剥離落下しマグネット6に付着したスケー
ル量を秤量し、さらに次の歪みの条件でも同様に、その
秤量値によってスケール剥離性を評価する方法である。
A magnet 6 is fixed by a fixing jig 7 at opposite positions on both sides of the surface 2 to be evaluated of the test piece 1. In this state, the test piece 1 is pulled by a tensile tester 4 to give a certain strain. The strain is held at that time, the scale amount peeled off from the test piece 1 and adhered to the magnet 6 is weighed by that time, and the scale peelability is similarly evaluated by the weighed value under the next strain condition. Is the way.

【0012】ここで試験片1に相対して剥離落下したス
ケールを回収するためのマグネット6は、その上端を試
験片1から離して下端を試験片1に近接させて固定して
いるが、その理由は、マグネット6の上端が試験片1に
近接し過ぎると、上に延びた試験片1から落下してくる
スケールがマグネット6のカバー上に乗ってしまうから
であり、また逆に離し過ぎると、マグネット6の磁力が
弱くなり、スケールの回収率が低下するからである。
Here, the magnet 6 for recovering the scale that has peeled off from the test piece 1 is fixed with the upper end separated from the test piece 1 and the lower end close to the test piece 1. The reason is that if the upper end of the magnet 6 is too close to the test piece 1, the scale falling from the test piece 1 extending upward will ride on the cover of the magnet 6, and if it is too far away from it. This is because the magnetic force of the magnet 6 is weakened and the scale recovery rate is reduced.

【0013】一方下端は、試験片1に接しない程度に近
接してセットするのがスケールの回収率が最もよいから
である。これらマグネット上端および下端と試験片1と
の距離は、そのマグネットの磁力の強さによって随時決
定すればよい。
On the other hand, the lower end is set so as not to be in contact with the test piece 1 because the recovery rate of the scale is the best. The distance between the upper and lower ends of the magnet and the test piece 1 may be determined at any time according to the strength of the magnetic force of the magnet.

【0014】ここでこのマグネット6の固定する際の注
意点は、試験片1としての鋼材が試験中に伸びるので、
その伸びた鋼材露出面を覆うようにセットすることであ
る。またマグネットには、例えば紙等を巻いて用いる
と、マグネットに付着したスケールを効率よく回収する
ことができ、有効なことである。
A point to be noted when fixing the magnet 6 is that the steel material as the test piece 1 is stretched during the test.
That is, it is set so as to cover the elongated exposed surface of the steel material. If the magnet is wound with paper, for example, the scale attached to the magnet can be efficiently collected, which is effective.

【0015】以下本発明の具体的な実施例として、本発
明の方法に基づいてスケールを回収し、そのスケール量
の測定を実施した結果について説明する。
Hereinafter, as a specific example of the present invention, a result of collecting a scale based on the method of the present invention and measuring the amount of the scale will be described.

【0016】まず熱間圧延後の鋼材を、電子天秤(0.
1gまで測定可能)で秤量可能(200g以下)な大き
さ(厚み:7mm,幅:24mm,長さ:150mm)
に切り出し、中央部の長さ30mmを残し、ビニールテ
ープで表面を覆った。
First, the steel material after the hot rolling is applied to an electronic balance (0.
Measurable (up to 200 g) size (thickness: 7 mm, width: 24 mm, length: 150 mm)
, And the surface was covered with a vinyl tape, leaving a length of 30 mm at the center.

【0017】これを引張試験機にセットし、その両端に
伸び計をセットし、試験片の鋼材表面が露出した部分に
相対するように薬包紙で包んだマグネットを固定した。
この時の試験片とマグネットの下端との間隔は1mmに
固定し、試験片とマグネット上端との間隔を変化させ、
その時のスケール回収率(「鋼材の重量減少量=回収ス
ケール量」の場合の回収率を100%とした)を評価し
た。
This was set in a tensile tester, extensometers were set at both ends thereof, and a magnet wrapped with a medicine wrapping paper was fixed so as to face the exposed portion of the steel surface of the test piece.
At this time, the distance between the test piece and the lower end of the magnet was fixed at 1 mm, and the distance between the test piece and the upper end of the magnet was changed.
The scale recovery rate at that time (the recovery rate in the case of “the amount of weight loss of steel material = recovery scale amount” was set to 100%) was evaluated.

【0018】ただし試験片の両端チャック部は、鋼材に
圧痕が残らないように処置した。この結果を図2に示
す。図からも判るように試験片とマグネット上端との間
隔が3〜5mmでは、回収率は、ほぼ100%を示して
いる。
However, the chucks at both ends of the test piece were treated so that no indentation was left on the steel material. The result is shown in FIG. As can be seen from the figure, when the distance between the test piece and the upper end of the magnet is 3 to 5 mm, the recovery rate is almost 100%.

【0019】また図3は、試験片とマグネット上端との
間隔を4mmにセットして、顕微鏡による鋼材表面のス
ケール厚み(引っ張り試験前に測定)と剥離スケール量
との関係を調査した結果を示し、図示のように剥離スケ
ール量と鋼材表面のスケール厚みには明白な相関関係が
あり、剥離スケール量から鋼材のスケール発生量の評価
も可能であり、スケール抑制目的の材料開発の際の定量
的な評価にも貢献できる。
FIG. 3 shows the result of investigating the relationship between the scale thickness of the steel surface (measured before the tensile test) and the amount of peeling scale using a microscope with the distance between the test piece and the upper end of the magnet set to 4 mm. As shown in the figure, there is a clear correlation between the amount of exfoliated scale and the scale thickness of the steel surface, and it is also possible to evaluate the amount of scale generated in steel from the amount of exfoliated scale. It can contribute to a good evaluation.

【0020】このように本発明によれば、微量なスケー
ル剥離量も精度よく測定することができ、このことから
鋼材の高精度なスケール剥離性の評価も可能となった。
As described above, according to the present invention, a very small amount of scale peeling can be measured with high accuracy, and this makes it possible to evaluate the scale peeling property of a steel material with high accuracy.

【0021】[0021]

【発明の効果】以上説明したように本発明の評価方法に
よれば、試験片に荷重をかけてこの試験片から剥離落下
したスケールをマグネットで吸着し、この吸着したスケ
ール重量を秤量して剥離性を評価するようにしているの
で、鋼材試験片から剥離したスケールを効率よく、しか
も高い回収率で回収できるので、鋼材,特に最近開発さ
れつつあるスケール発生量の少ない鋼材のように、発生
スケールが微量な鋼材でも従来のように重量の大きい試
験片の重量変化によって測定せず、直接,剥離したスケ
ールそのものを測定するので、高精度の秤量器を使用で
き、それだけ精度の高いスケール剥離性の評価が可能と
なる。
As described above, according to the evaluation method of the present invention, a scale is peeled off from a test piece by applying a load to the test piece, the scale is attracted by a magnet, and the weight of the attracted scale is weighed and peeled off. The scale that has been peeled off from the steel specimen can be collected efficiently and at a high recovery rate because the steel is evaluated for its properties. However, even a small amount of steel is measured directly by the peeled scale itself instead of measuring the weight change of a heavy test piece as in the past, so a high-precision weighing machine can be used, and the highly accurate scale peelability Evaluation becomes possible.

【0022】また本発明では、従来のように試験片重量
を測定することによる引張り歪み付与の際のチャック圧
痕による誤差もなくなり、さらに精度の高いスケール測
定が可能となり、これにより高精度のスケール剥離性の
評価方法も確立された。
Further, according to the present invention, errors due to chuck indentation when applying tensile strain by measuring the weight of a test piece as in the prior art can be eliminated, and a more accurate scale measurement can be performed. Sex evaluation methods have also been established.

【0023】さらには、引っ張り試験前に測定した鋼材
表面のスケール厚みと、剥離スケール量との関係を調査
した結果より、剥離スケール量と鋼材表面のスケール厚
みには明白な相関関係があり、剥離スケール量から鋼材
のスケール発生量の評価も可能であり、スケール抑制目
的の材料開発の際の定量的な評価にも貢献できる。
Further, from the result of investigation of the relationship between the scale thickness of the steel surface measured before the tensile test and the amount of the peel scale, there is a clear correlation between the amount of the peel scale and the scale thickness of the steel surface. The scale generation amount of the steel material can be evaluated from the scale amount, and it can contribute to the quantitative evaluation at the time of material development for the purpose of scale control.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の一実施例を示し、歪みを与えた試験片
から剥離落下したスケールをマグネットで吸着回収する
要領を示す略側面図である。
FIG. 1 is a schematic side view showing an embodiment of the present invention and showing a procedure for adsorbing and recovering a scale that has peeled and dropped from a strained test piece with a magnet.

【図2】試験片およびマグネット上端とのなす間隔とス
ケール回収率との関係を示す図面である。
FIG. 2 is a drawing showing a relationship between an interval between a test piece and an upper end of a magnet and a scale recovery rate.

【図3】鋼材表面のスケール厚みと剥離スケール量との
関係を示す図面である。
FIG. 3 is a drawing showing a relationship between a scale thickness on a steel material surface and a peeling scale amount.

【符号の説明】[Explanation of symbols]

1 試験片 2 被評価面 3 テーピング 4 引張試験機 5 伸び計 6 マグネット 7 固定治具 DESCRIPTION OF SYMBOLS 1 Test piece 2 Evaluated surface 3 Taping 4 Tensile tester 5 Extensometer 6 Magnet 7 Fixing jig

───────────────────────────────────────────────────── フロントページの続き (56)参考文献 特開 昭57−90141(JP,A) 特開 平5−273115(JP,A) 特開 平5−28417(JP,A) 実開 昭63−2136(JP,U) (58)調査した分野(Int.Cl.7,DB名) G01N 19/04 ──────────────────────────────────────────────────続 き Continuation of the front page (56) References JP-A-57-90141 (JP, A) JP-A-5-273115 (JP, A) JP-A-5-28417 (JP, A) 2136 (JP, U) (58) Field surveyed (Int. Cl. 7 , DB name) G01N 19/04

Claims (1)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 両端をテーピングして被評価材とした試
験片を、引張試験機により一定の歪みになるまで荷重を
かけ、この一定歪みに達するまでの前記試験片から剥離
落下したスケールをマグネットで吸着し、この吸着した
スケール重量を秤量してその秤量値によって鋼材のスケ
ール剥離性を評価することを特徴とするスケール剥離性
の評価方法。
1. A test piece, which is a material to be evaluated with taping at both ends, is subjected to a load by a tensile tester until a certain strain is obtained, and a scale peeled and dropped from the test piece until the test piece reaches the certain strain is magnetized. A method for evaluating scale peelability, comprising weighing the weight of the adsorbed scale and evaluating the scale peelability of the steel material by the weighed value.
JP16076994A 1994-06-21 1994-06-21 Evaluation method of scale peelability Expired - Fee Related JP3335770B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP16076994A JP3335770B2 (en) 1994-06-21 1994-06-21 Evaluation method of scale peelability

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP16076994A JP3335770B2 (en) 1994-06-21 1994-06-21 Evaluation method of scale peelability

Publications (2)

Publication Number Publication Date
JPH085544A JPH085544A (en) 1996-01-12
JP3335770B2 true JP3335770B2 (en) 2002-10-21

Family

ID=15722065

Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Status (1)

Country Link
JP (1) JP3335770B2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102177872B1 (en) * 2019-01-28 2020-11-12 현대제철 주식회사 Method of evaluating peelability of coated steel sheet

Also Published As

Publication number Publication date
JPH085544A (en) 1996-01-12

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