JP2892217B2 - Method and apparatus for manufacturing glass material - Google Patents

Method and apparatus for manufacturing glass material

Info

Publication number
JP2892217B2
JP2892217B2 JP4143926A JP14392692A JP2892217B2 JP 2892217 B2 JP2892217 B2 JP 2892217B2 JP 4143926 A JP4143926 A JP 4143926A JP 14392692 A JP14392692 A JP 14392692A JP 2892217 B2 JP2892217 B2 JP 2892217B2
Authority
JP
Japan
Prior art keywords
glass
molten glass
lump
molten
glass material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP4143926A
Other languages
Japanese (ja)
Other versions
JPH06127955A (en
Inventor
忠孝 米本
義之 清水
孝志 井上
寿彦 室井
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SUMITA KOGAKU GARASU KK
Panasonic Holdings Corp
Original Assignee
SUMITA KOGAKU GARASU KK
Matsushita Electric Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SUMITA KOGAKU GARASU KK, Matsushita Electric Industrial Co Ltd filed Critical SUMITA KOGAKU GARASU KK
Priority to JP4143926A priority Critical patent/JP2892217B2/en
Publication of JPH06127955A publication Critical patent/JPH06127955A/en
Application granted granted Critical
Publication of JP2892217B2 publication Critical patent/JP2892217B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B11/00Pressing molten glass or performed glass reheated to equivalent low viscosity without blowing
    • C03B11/06Construction of plunger or mould
    • C03B11/08Construction of plunger or mould for making solid articles, e.g. lenses
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2215/00Press-moulding glass
    • C03B2215/02Press-mould materials
    • C03B2215/03Press-mould materials defined by material properties or parameters, e.g. relative CTE of mould parts
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【産業上の利用分野】本発明は、レンズやプリズム等の
高精度な光学ガラス素子のリヒ−トプレス用のガラス素
材の製造方法と製造装置に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method and an apparatus for producing a glass material for use in a high-precision optical glass element such as a lens or a prism for a repetitive press.

【0002】[0002]

【従来の技術】近年、光学ガラスレンズは光学機器のレ
ンズ構成の簡略化とレンズ部分の軽量化の両方を同時に
達成し得る非球面化の方向にある。この非球面レンズの
製造にあたっては、従来の光学レンズの製造方法である
ガラスのブロック、ロッド、板等から素材を切り出した
後、研削、研磨する方法、あるいは、製造しようとする
レンズに近い形状の型で溶融ガラス塊を予めプレスし、
このガラス成形体を研削、研磨する方法といった研磨法
では、加工及び量産化が困難であり金型を用いた成形法
が有望視されている。
2. Description of the Related Art In recent years, optical glass lenses have become more aspherical so that both the simplification of the lens structure of an optical device and the reduction of the weight of the lens portion can be achieved simultaneously. In manufacturing this aspheric lens, a method of manufacturing a conventional optical lens is to cut out a material from a glass block, a rod, a plate, or the like, and then grind and polish the material, or a method similar to the lens to be manufactured. Press the molten glass lump in advance with a mold,
In a polishing method such as a method of grinding and polishing this glass formed body, it is difficult to process and mass-produce, and a forming method using a mold is expected to be promising.

【0003】金型を用いた成形方法には、溶融ガラス塊
を直接プレスし高精度の光学ガラス素子を得るダイレク
トプレス方法と成形に用いる予備成形体のガラス素材を
プレスし高精度の光学ガラス素子を得るリヒートプレス
方法がある。
[0003] A molding method using a mold includes a direct pressing method of directly pressing a molten glass lump to obtain a high-precision optical glass element and a high-precision optical glass element by pressing a glass material of a preform used for molding. There is a reheat press method for obtaining

【0004】前者の方法によれば、非常に安価な光学ガ
ラス素子を製造することが可能であるが、高温の溶融ガ
ラス塊を取り扱うことから成形ガラスの高精度化が困難
なことやプレス型のライフが短くなる等の技術的な問題
も多く実用化が困難である。
According to the former method, it is possible to manufacture a very inexpensive optical glass element. There are also many technical problems such as a shortened life and it is difficult to put it to practical use.

【0005】後者の方法によれば、ダイレクトプレス方
法による課題は改善されるが、ガラス素材を製造するた
めの工程が増えるためコストは割高となる。このリヒー
トプレス用のガラス素材を製造する工程の簡略化が光学
ガラス素子を製造するにあたって重要な課題である。
According to the latter method, the problem of the direct press method is improved, but the cost is relatively high because the number of steps for manufacturing the glass material is increased. The simplification of the process of manufacturing a glass material for reheat pressing is an important issue in manufacturing an optical glass element.

【0006】ガラス素材を簡単に形成する有効な方法と
して、溶融ガラス塊を、受け皿上に落し込みその状態で
放置して形状を成す方法によれば、非常に安価なリヒー
トプレス用のガラス素材を製造できる(例えば、特開平
2−34525号公報)。
As an effective method for easily forming a glass material, according to a method of dropping a molten glass lump on a saucer and leaving it in that state to form a shape, a very inexpensive glass material for reheat press can be obtained. It can be manufactured (for example, JP-A-2-34525).

【0007】[0007]

【発明が解決しようとする課題】溶融ガラスを、溶融炉
のガラス流出口より流下させる方法は、流出口温度を1
000度以上の高温にしガラスの粘度を低くしてから、
自然滴下させることによって、あるいは切断刃で切断す
ることによって、溶融ガラス塊を落下させる。
The method of causing molten glass to flow down from the glass outlet of a melting furnace involves the following steps.
After lowering the viscosity of the glass to a high temperature of 000 degrees or more,
The molten glass block is dropped by natural dropping or cutting by a cutting blade.

【0008】この溶融ガラス塊を受ける為の受け皿は、
平滑な面に磨かれたもので、溶融ガラスとの濡れ性が良
い材質にするか、あるいは溶融ガラスが前記受け皿に濡
れる温度まで加熱することにより受け皿の面をガラスに
転写させることが重要である。
A tray for receiving the molten glass lump is
It is important that the surface of the saucer be transferred to glass by polishing the surface to a smooth surface and having good wettability with the molten glass, or by heating the molten glass to a temperature at which the saucer gets wet with the saucer. .

【0009】たとえば、従来例を示した図7(a)のよ
うに溶融ガラスと濡れ性の悪い材質2aの受け皿では、
溶融ガラス塊1の受け皿との接触面1bに濡れの悪さに
よるしわが発生してしまう。
For example, as shown in FIG. 7A showing a conventional example, in a saucer made of a material 2a having poor wettability with molten glass,
Wrinkles due to poor wetting occur on the contact surface 1b of the molten glass lump 1 with the tray.

【0010】このような濡れの悪さによるしわが発生
し、受け皿の平滑面をガラス素材1’に転写できなけれ
ば、リヒートプレス後にもレンズに気泡あるいは穴とし
て残留するため光学ガラス素子の性能が低下するという
問題がある。
If wrinkles due to such poor wetting occur and the smooth surface of the saucer cannot be transferred to the glass material 1 ', the performance of the optical glass element deteriorates because it remains as bubbles or holes in the lens even after reheat pressing. There is a problem of doing.

【0011】図7(b)のように、粘度の低い高温の溶
融ガラス塊を落下し、平滑な面に磨かれた、溶融ガラス
との濡れ性が良い材料2bの受け皿で受けた場合は、し
わ状の欠陥の発生はないが、受け皿が単一材料であるた
め、溶融ガラス塊1と受け皿の濡れ角度が大きくなり、
ガラス素材外周が鋭角に突起した形状になり、割れ、チ
ッピングが発生しやすい形状になる。また、受け皿に落
ちた時の溶融ガラス塊の変形が濡れの影響でそのまま形
に現れ形状ばらつきが生じることや、溶融ガラス塊と受
け型との濡れる面積(転写面積)の制御が困難で、自由
な厚みのガラス素材が得られない等、所望の形状にガラ
ス素材1’を作製しにくいという課題もあった。
As shown in FIG. 7 (b), when a molten glass mass having a low viscosity and a high temperature is dropped and received by a saucer of a material 2b polished to a smooth surface and having good wettability with the molten glass, No wrinkle-like defects are generated, but since the pan is a single material, the wet angle between the molten glass lump 1 and the pan becomes large,
The outer periphery of the glass material has a shape protruding at an acute angle, and has a shape in which cracking and chipping easily occur. In addition, the deformation of the molten glass lump when it is dropped on the pan is reflected in the shape as it is under the influence of wetting, causing shape variations, and it is difficult to control the wetted area (transfer area) between the molten glass lump and the receiving mold. There is also a problem that it is difficult to produce a glass material 1 ′ in a desired shape, for example, a glass material having a large thickness cannot be obtained.

【0012】本発明は上記課題に鑑み、低コストで高精
度なガラス素材が製造できるガラス素材の製造方法とそ
の製造装置を提供することを目的とする。
The present invention has been made in view of the above problems, and has as its object to provide a method of manufacturing a glass material capable of manufacturing a high-precision glass material at low cost and an apparatus for manufacturing the same.

【0013】[0013]

【課題を解決するための手段】前記目的を達成するた
め、本発明は、光学ガラス素子のリヒートプレス用のガ
ラス素材を次のようにして製造する。先ず、必要量の溶
融ガラス塊を精度よく平滑な面に磨かれた受け皿で受け
る。溶融ガラス塊を受ける受け皿には、溶融ガラスとの
濡れ性の異なる少なくとも2種類以上の材料により構成
された受け皿を使用する。例えば、その受け皿の材料の
構成方法を、溶融ガラス塊の移載中心部に濡れ性の良い
材料を構成し、溶融ガラス塊の移載外周部に濡れ性の悪
い材料を構成した受け皿とする。この様な受け皿上で冷
却してガラス素材を作製する。あるいは、前記受け皿で
溶融ガラス塊を受けた後、溶融ガラス塊を押圧型で冷却
加圧し、受け皿上で取り出し温度まで冷却しガラス素材
を作製する。
According to the present invention, a glass material for reheat pressing an optical glass element is manufactured as follows. First, a required amount of molten glass lump is accurately received in a saucer polished to a smooth surface. As the tray for receiving the molten glass block, a tray composed of at least two or more types of materials having different wettability with the molten glass is used. For example, the material of the tray is configured such that a material having good wettability is formed at the transfer center of the molten glass lump and a material having poor wettability is formed at the outer periphery of the transfer of the molten glass lump. A glass material is produced by cooling on such a tray. Alternatively, after receiving the molten glass lump in the tray, the molten glass lump is cooled and pressurized with a pressing die, and cooled to a removal temperature on the tray to produce a glass material.

【0014】[0014]

【作用】前記本発明の構成によれば、受け皿で受けた溶
融ガラス塊には、表面張力により形成された自由面と受
け皿に接する接触面が形成される。
According to the structure of the present invention, a free surface formed by surface tension and a contact surface in contact with the tray are formed in the molten glass mass received by the tray.

【0015】この内、溶融ガラス塊の自由面は、表面張
力の作用によって極めて滑らかな鏡面に形成される。溶
融ガラス塊の受け皿との接触面は、例えば、濡れ性の良
い材料と接する中心部は、面精度のよい受け皿の面が溶
融ガラス塊に転写されるため自由面と同等の鏡面がなさ
れ、濡れ性の悪い材料と接する外周部は溶融ガラス塊が
濡れないために、所望の面積だけ受け皿の平滑面をガラ
ス素材に転写することが可能になった。また、溶融ガラ
ス塊と受け皿の濡れる面積が制御できるため、できるガ
ラス素材の形状も非常に安定する。
Of these, the free surface of the molten glass lump is formed into an extremely smooth mirror surface by the action of surface tension. The contact surface of the molten glass mass with the saucer is, for example, a central portion in contact with a material having good wettability, the surface of the saucer having good surface accuracy is transferred to the molten glass mass, so that a mirror surface equivalent to the free surface is made, and Since the molten glass lump does not wet the outer peripheral portion in contact with the material having poor properties, the smooth surface of the receiving tray can be transferred to the glass material by a desired area. Further, since the wetted area of the molten glass lump and the saucer can be controlled, the shape of the glass material can be very stable.

【0016】溶融ガラスと濡れ性の良い材料は、例えば
オーステナイト鋼、ニクロム、グラッシーカーボンや光
学ガラスと反応あるいはわずかに付着する貴金属、タン
グステン、タンタル、レニウム、ハフニウムの単体ある
いはそれらの合金であることが望ましい。溶融ガラスと
濡れ性の悪く、離型性が優れている材料は、例えばカー
ボン、ボロンナイトライド、炭化珪素、窒化珪素、窒化
アルミ、窒化クロム等が適している。
The material having good wettability with the molten glass is, for example, a simple substance of a noble metal, tungsten, tantalum, rhenium, hafnium which reacts with or slightly adheres to austenitic steel, nichrome, glassy carbon or optical glass, or an alloy thereof. desirable. As a material having poor wettability with the molten glass and excellent releasability, for example, carbon, boron nitride, silicon carbide, silicon nitride, aluminum nitride, chromium nitride, and the like are suitable.

【0017】溶融ガラス塊と受け皿の濡れ面積を制御す
る場合、溶融ガラス塊のもつ表面張力の影響により、受
け皿で受けただけでは、所望の濡れ面積を得られないこ
とがある。この場合、溶融ガラス塊を受け皿に移載し
て、直ちに自由面を押圧型で冷却加圧すれば所望の転写
面積と所望の厚み形状を持つガラス素材が得られる。
When controlling the wet area of the molten glass lump and the pan, the desired wet area may not be obtained only by receiving the molten glass lump with the pan due to the surface tension of the molten glass lump. In this case, a glass material having a desired transfer area and a desired thickness shape can be obtained by transferring the molten glass lump to a receiving tray and immediately cooling and pressing the free surface with a pressing die.

【0018】こうして得られたガラス素材をガラス素子
の成形に用いれば、極めて高精度のガラス素子をプレス
のみの加工で得ることができるのである。
If the glass material thus obtained is used for forming a glass element, an extremely high-precision glass element can be obtained only by pressing.

【0019】[0019]

【実施例】以下、本発明のガラス素材の製造方法及び製
造装置の一実施例について図1〜図6の図面を参照しな
がら詳細に説明する。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS One embodiment of the method and apparatus for manufacturing a glass material according to the present invention will be described below in detail with reference to FIGS.

【0020】(実施例1)図1は、本発明の一実施例の
ガラス素材の製造方法を表わす断面図である。
(Embodiment 1) FIG. 1 is a sectional view showing a method of manufacturing a glass material according to an embodiment of the present invention.

【0021】図1では、溶融ガラス塊1を濡れ性の異な
る2種類の構成材料2a、2bでできた受け皿2で受け
た時の状態を示す。この受け皿2の材料構成は、溶融ガ
ラス塊が受け皿2上に落し込まれる中心部(面精度の必
要な部分)に溶融ガラスと濡れ性の良い構成材料2bを
構成し、溶融ガラス塊1の外周が接する面に中心部の構
成材料2bより濡れ性の悪い構成材料2aを構成したも
のである。
FIG. 1 shows a state in which a molten glass lump 1 is received by a tray 2 made of two kinds of constituent materials 2a and 2b having different wettability. The material composition of the tray 2 is such that the molten glass lump is dropped on the tray 2 (a part requiring surface accuracy), and the molten glass and the constituent material 2b having good wettability are formed. Is made of a constituent material 2a having a lower wettability than the constituent material 2b at the center.

【0022】本発明の一実施例のガラス素材の製造方法
を工程順に説明する。まず、溶融ガラス塊を受ける前
に、受け皿2を加熱すれば溶融ガラス塊と受け皿の濡れ
性が向上し表面転写性が良くなるため、ガラスの種類と
濡れ性の良い材料2aに合ったガラスの軟化点以下の温
度に受け皿2を予備加熱する。
A method for manufacturing a glass material according to one embodiment of the present invention will be described in the order of steps. First, if the pan 2 is heated before receiving the molten glass lump, the wettability of the molten glass lump and the pan is improved, and the surface transfer property is improved. The pan 2 is preheated to a temperature below the softening point.

【0023】そして、ガラス溶融炉で溶融されたガラス
を、所定量だけ受け皿2上に供給する。この時、受け皿
2により、溶融ガラス塊1の中心部は、濡れ性の良い構
成材料2b上に載置されるため、受け皿2の平滑な面が
転写され、溶融ガラス塊の外周部は、濡れ性の悪い構成
材料2aにより、溶融ガラスとの離型性が良く付着しな
いため、必要な転写面が得られると共に形状の安定した
溶融ガラス塊が形成される。自由面1aは、溶融ガラス
塊の表面張力により形成される極めて良好な鏡面とな
る。
Then, a predetermined amount of the glass melted in the glass melting furnace is supplied onto the tray 2. At this time, the center of the molten glass lump 1 is placed on the constituent material 2b having good wettability by the tray 2, so that the smooth surface of the tray 2 is transferred, and the outer periphery of the molten glass lump is wetted. Due to the poor material 2a, the releasability from the molten glass does not adhere well, so that a necessary transfer surface is obtained and a molten glass lump having a stable shape is formed. The free surface 1a is a very good mirror surface formed by the surface tension of the molten glass lump.

【0024】この溶融ガラス塊を受け皿上で、ガラスの
軟化点以下の温度まで冷却し取り出す。
The molten glass lump is cooled on a plate to a temperature lower than the softening point of the glass and is taken out.

【0025】本実施例では、極めて滑らかな鏡面と、良
好な面粗度に管理された所望の形状のガラス素材1’が
得られ、このガラス素材を成形することで優れた光学素
子を得ることができた。
In this embodiment, an extremely smooth mirror surface and a glass material 1 'having a desired shape controlled to a good surface roughness can be obtained, and an excellent optical element can be obtained by molding this glass material. Was completed.

【0026】なお、受け皿2の形状は、例えば図2
(a)、(b)に示すように、濡れ性の良い材料2bを
凸凹形状に加工すれば各種ガラス素子の形状にあったガ
ラス素材1’を作製することも可能である。また、図2
(c)のように、濡れ性の悪い材料2aを母材とし、濡
れ性の良い材料2bの薄膜を形成した受け皿2を作製し
て使用しても前記実施例同様に、所望のガラス素材1’
が得られる。
The shape of the tray 2 is, for example, as shown in FIG.
As shown in (a) and (b), if the material 2b having good wettability is processed into an uneven shape, it is also possible to produce a glass material 1 'that matches the shape of various glass elements. FIG.
As shown in (c), the desired glass material 1 can be obtained by using the material 2a having poor wettability as a base material and forming and using the saucer 2 on which a thin film of the material 2b having good wettability is formed. '
Is obtained.

【0027】(実施例2)図5は、第1の実施例のガラ
ス素材の製造方法を用いた製造装置の基本構成を示す断
面図である。
(Embodiment 2) FIG. 5 is a sectional view showing a basic configuration of a manufacturing apparatus using the method for manufacturing a glass material of the first embodiment.

【0028】11はガラス溶融炉、12は溶融ガラスの
流出口、13、15、17は加熱ヒータ、14は切断
刃、2は溶融ガラス塊の受け皿、16は搬送チェーンコ
ンベアを示す。また、18は冷却ガス、19は冷却ガス
管、20は取り出しロボットである。
11 is a glass melting furnace, 12 is a molten glass outlet, 13, 15 and 17 are heaters, 14 is a cutting blade, 2 is a tray for molten glass lump, and 16 is a conveyor chain conveyor. Reference numeral 18 denotes a cooling gas, 19 denotes a cooling gas pipe, and 20 denotes a take-out robot.

【0029】受け型2の中心部φ6の大きさを転写面と
し構成材料にオーステナイト鋼(SUS316)を、外
周部の構成材料にカーボンを選定し平型に加工した。
The size of the central portion φ6 of the receiving mold 2 was used as a transfer surface, and austenitic steel (SUS316) was selected as a constituent material, and carbon was selected as a constituent material of an outer peripheral portion, and processed into a flat shape.

【0030】溶融ガラスは、ジルコニア(ZrO2)8
重量パ−セント、酸化ランタン(La23)30重量パ
−セント、酸化ホウ素(B23)42重量パ−セント、
酸化カルシウム(CaO)10重量パ−セント、残部が
微量成分からなるランタン系ガラスを用いた。
The molten glass is zirconia (ZrO 2 ) 8
Weight percent, lanthanum oxide (La 2 O 3 ) 30 weight percent, boron oxide (B 2 O 3 ) 42 weight percent,
A lanthanum-based glass comprising 10% by weight of calcium oxide (CaO) and the balance being trace components was used.

【0031】このガラスを1400℃で溶融したあと、
加熱ヒータ13により950℃に保持した流出口12か
ら、約1グラムの溶融ガラス塊10を流出し、切断刃1
4により切断することにより、予め400℃に加熱され
た受け皿2に供給する。その後、冷却ステージにおいて
加熱ヒータ17により温調された冷却ガス18を溶融ガ
ラス塊1上面に吹き付けてガラスの軟化点より低い温度
に冷却し、100℃以下に徐冷してからてからガラス素
材1’を取り出しロボット20により装置内から取り出
した。
After melting this glass at 1400 ° C.,
Approximately 1 gram of molten glass lump 10 flows out of outlet 12 maintained at 950 ° C. by heater 13,
By cutting at 4, it is supplied to the tray 2 which has been heated to 400 ° C. in advance. Thereafter, in a cooling stage, a cooling gas 18 whose temperature is controlled by a heater 17 is sprayed on the upper surface of the molten glass lump 1 to cool the glass to a temperature lower than the softening point of the glass, and gradually cooled to 100 ° C. or lower. 'Was taken out of the apparatus by the take-out robot 20.

【0032】本実施例によって得られたガラス素材1’
において、中心点平均粗さは1. 0μm以下の鏡面状態
で、形状安定性は0.1mm以下であり光学顕微鏡観察
した結果、表面に異物付着、傷、といった欠陥は認めら
れなかった。
Glass material 1 'obtained by this embodiment
Of the sample, the center point average roughness was 1.0 μm or less, and the shape stability was 0.1 mm or less. As a result of observation with an optical microscope, no defects such as adhesion of foreign matter and scratches were found on the surface.

【0033】なお、装置内は受け皿の酸化による劣化を
防止するために、適当な非酸化性雰囲気となされるのが
通常であるが、本実施例では、装置内を窒素ガス20リ
ットル/分、トリクロロトリフルオロエタン(C2Cl3
3)ガス1リットル/分の割合で混合したハロゲン化
炭化水素雰囲気とした。
The inside of the apparatus is usually provided with an appropriate non-oxidizing atmosphere in order to prevent the tray from being deteriorated by oxidation. Trichlorotrifluoroethane (C 2 Cl 3
F 3 ) A halogenated hydrocarbon atmosphere mixed at a rate of 1 liter / minute of gas was used.

【0034】(実施例3)図5と同一機能の製造装置を
用いて異なるガラス組成のガラス素材を作製した。図2
(c)の形状の受け型2の母材に炭化珪素(SiC)を
選定し、中心部φ5の大きさを転写面とし材料に白金ー
イリジウムーオスミウム(Pt−Ir−Os)の薄膜を
成膜した。溶融ガラスは、酸化珪素(SiO2)65重
量パ−セント、酸化カリウム(K2O)9重量パ−セン
ト、酸化ホウ素(B23)10重量パ−セント、酸化ナ
トリウム(Na2O)10重量パ−セント、残部が微量
成分からなるホウケイ酸ガラスを用いた。
Example 3 Glass materials having different glass compositions were produced using a production apparatus having the same function as that shown in FIG. FIG.
Silicon carbide (SiC) was selected as the base material of the receiving die 2 having the shape of (c), and a platinum-iridium-osmium (Pt-Ir-Os) thin film was formed as the material using the size of the center part φ5 as a transfer surface. Filmed. The molten glass is 65% by weight of silicon oxide (SiO 2 ), 9% by weight of potassium oxide (K 2 O), 10% by weight of boron oxide (B 2 O 3 ), and sodium oxide (Na 2 O). Borosilicate glass consisting of 10% by weight and the balance of trace components was used.

【0035】このガラスを1350℃で溶融したあと、
920℃に保持した流出口12から約1グラムの溶融ガ
ラス10を予め350℃に加熱された受け皿2に供給す
る。その後、冷却ステージにおいて加熱ヒータ17によ
り温調された冷却ガス18を溶融ガラス塊1の上面に吹
き付けてガラスの軟化点より低い温度に冷却し、100
℃以下に徐冷してからガラス素材1’を取り出しロボッ
ト20により装置内から取り出した。
After melting this glass at 1350 ° C.,
About 1 gram of the molten glass 10 is supplied from the outlet 12 maintained at 920 ° C. to the pan 2 which has been heated to 350 ° C. in advance. Thereafter, in a cooling stage, a cooling gas 18 whose temperature is controlled by the heater 17 is sprayed on the upper surface of the molten glass lump 1 to cool the glass to a temperature lower than the softening point of the glass,
The glass material 1 ′ was gradually cooled to a temperature of not more than 0 ° C. and was taken out of the apparatus by the robot 20.

【0036】本実施例によって得られたガラス素材1’
において、中心点平均粗さは1. 0μm以下の鏡面状態
で、形状安定性は0.1mm以下であり光学顕微鏡観察
した結果、表面に異物付着、傷、といった欠陥は認めら
れなかった。
Glass material 1 'obtained according to this embodiment
Of the sample, the center point average roughness was 1.0 μm or less, and the shape stability was 0.1 mm or less. As a result of observation with an optical microscope, no defects such as adhesion of foreign matter and scratches were found on the surface.

【0037】なお、本実施例では装置内の雰囲気はアル
ゴンガス20リットル/分、エチレン(C24)1リットル/分
の割合で混合した炭化水素雰囲気とした。
In this embodiment, the atmosphere in the apparatus was a hydrocarbon atmosphere in which argon gas was mixed at a rate of 20 L / min and ethylene (C 2 H 4 ) at a rate of 1 L / min.

【0038】(実施例4)図3は、本発明の一実施例の
ガラス素材の製造方法を表わす断面図である。
(Embodiment 4) FIG. 3 is a sectional view showing a method of manufacturing a glass material according to an embodiment of the present invention.

【0039】本発明の一実施例のガラス素材の製造方法
を工程順に説明する。図3(a)では、第1の実施例に
おける図1に示すと同様の構成の受け皿2に、溶融ガラ
ス塊1を受けた時の状態を示す。図3(a)のように、
溶融ガラス塊の重量や溶融ガラス塊の表面張力の違い、
あるいは所望の転写面の大きさの違いにより、濡れ性の
良い構成材料2bの転写面に溶融ガラス塊1が充分広が
らない場合が生じる。
A method for manufacturing a glass material according to one embodiment of the present invention will be described in the order of steps. FIG. 3A shows a state where the molten glass lump 1 is received in the tray 2 having the same configuration as that shown in FIG. 1 in the first embodiment. As shown in FIG.
Difference in weight of molten glass mass and surface tension of molten glass mass,
Alternatively, depending on the size of the desired transfer surface, the molten glass lump 1 may not sufficiently spread on the transfer surface of the constituent material 2b having good wettability.

【0040】図3(b)では、ガラス素材に所望の受け
皿の転写面を形成するために、押圧型を用い高温の溶融
ガラス塊1を冷却加圧し、濡れ性の良い材料2の面に溶
融ガラス塊1を押し広げている状態を示す。
In FIG. 3B, in order to form a transfer surface of a desired tray on a glass material, a high-temperature molten glass lump 1 is cooled and pressurized using a pressing die, and is melted on a surface of a material 2 having good wettability. The state where the glass lump 1 is being spread is shown.

【0041】図3(c)では、所望の転写面(濡れ性の
良い材料2bの面)以上に押し広げられた状態で、溶融
ガラス塊1がガラスの軟化点以下の温度に冷却される前
に押圧型を開放し、溶融ガラス塊の表面張力により溶融
ガラス塊を形状復帰させる。形状復帰した溶融ガラス塊
1の自由面1aは、極めて良好な鏡面に戻る。溶融ガラ
ス塊が形状復帰後も、濡れ性のよい材料2bに接した面
は、そのままの状態を保持し冷却されるため、所望の面
積だけ高精度の受け皿の転写面を持つガラス素材1’を
容易に作製できる。
In FIG. 3 (c), the molten glass lump 1 is cooled to a temperature lower than the softening point of the glass in a state where the molten glass lump 1 is spread over a desired transfer surface (the surface of the material 2b having good wettability). Then, the pressing die is opened, and the molten glass lump is returned to the shape by the surface tension of the molten glass lump. The free surface 1a of the molten glass lump 1 whose shape has been restored returns to a very good mirror surface. Even after the molten glass lump recovers its shape, the surface in contact with the material 2b having good wettability is kept as it is and is cooled, so that the glass material 1 'having a highly accurate transfer surface of a saucer by a desired area is used. It can be easily manufactured.

【0042】本実施例では、極めて滑らかな鏡面と、良
好な面粗度に管理された所望の形状のガラス素材1’が
得られ、このガラス素材を成形することで優れた光学素
子を得ることができる。
In this embodiment, an extremely smooth mirror surface and a glass material 1 'having a desired shape controlled to a good surface roughness can be obtained, and an excellent optical element can be obtained by molding this glass material. Can be.

【0043】また、例えば図4のように、受け皿と同様
に所望の形状と所望の転写面積を必要とする面の材料に
溶融ガラスと濡れ性のよい材料3bを構成した押圧型3
を使用すれば、平板、凹、メニスカスといった各種光学
ガラス素子の形状に対応したガラス素材を作製すること
ができる。前記、作製方法を用いたとき、ガラスの表面
張力による溶融ガラス塊1の形状復帰を防ぎ、所望の形
状を維持することができるように、冷却加圧の開放のタ
イミングは、溶融ガラス塊1がガラスの軟化点以下の温
度に冷却されてから押圧型3を開放する。
Further, as shown in FIG. 4, for example, similarly to the tray, a pressing die 3 having a material 3b having a desired shape and a desired transfer area is formed of a material 3b having good wettability with molten glass.
By using, a glass material corresponding to the shape of various optical glass elements such as a flat plate, a concave, and a meniscus can be produced. When the above-described manufacturing method is used, the timing of releasing the cooling and pressurizing is set such that the molten glass lump 1 is released so as to prevent the molten glass lump 1 from returning to the shape due to the surface tension of the glass and maintain a desired shape. After being cooled to a temperature lower than the softening point of the glass, the pressing mold 3 is opened.

【0044】(実施例5)図6は、第4の実施例のガラ
ス素材の製造方法を用いた製造装置の基本構成を示す断
面図である。
(Embodiment 5) FIG. 6 is a sectional view showing the basic structure of a manufacturing apparatus using the method for manufacturing a glass material of the fourth embodiment.

【0045】受け型2の中心部φ10の構成材料にオー
ステナイト鋼(SUS316)を、外周部の構成材料に
カーボンを選定し平型に加工した。また、押圧型3の構
成材料に溶融ガラスと濡れ性の悪い炭化珪素を選定し平
型に加工した。
Austenitic steel (SUS316) was selected as the constituent material of the center part φ10 of the receiving mold 2 and carbon was selected as the constituent material of the outer peripheral part, and processed into a flat mold. Further, silicon carbide having poor wettability with molten glass was selected as a constituent material of the pressing die 3 and processed into a flat die.

【0046】溶融ガラスは、ジルコニア(ZrO2)8
重量パ−セント、酸化ランタン(La23)30重量パ
−セント、酸化ホウ素(B23)42重量パ−セント、
酸化カルシウム(CaO)10重量パ−セント、残部が
微量成分からなるランタン系ガラスを用いた。このガラ
スを1400℃で溶融したあと、加熱ヒータ13により
950℃に保持した流出口12から、約1グラムの溶融
ガラス10を流出し、自然滴下により、予め400℃に
加熱された受け皿2に供給する。
The molten glass is made of zirconia (ZrO 2 ) 8
Weight percent, lanthanum oxide (La 2 O 3 ) 30 weight percent, boron oxide (B 2 O 3 ) 42 weight percent,
A lanthanum-based glass comprising 10% by weight of calcium oxide (CaO) and the balance being trace components was used. After melting the glass at 1400 ° C., about 1 gram of the molten glass 10 flows out of the outlet 12 maintained at 950 ° C. by the heater 13 and supplied to the pan 2 previously heated to 400 ° C. by natural dropping. I do.

【0047】次に、受け皿2を搬送用チェーンコンベア
16により押圧型3の下に移動する。移動時に溶融ガラ
ス塊が急冷され、ガラス軟化点以下になるのを防ぐた
め、受け皿2は移動時も加熱ヒータ15にて加熱する。
図3(b)のように受け皿2が押圧型3の真下に移動さ
れると同時に、250℃に温度コントロールされた押圧
型3は、押圧シリンダ21で溶融ガラス塊を加圧する。
溶融ガラス塊1は、冷却されるが、図3(c)のように
押圧型3と溶融ガラス塊1の接触面がガラスの軟化点以
下になる前に、加圧を開放し再び自由面とする。
Next, the receiving tray 2 is moved below the pressing die 3 by the transport chain conveyor 16. In order to prevent the molten glass lump from being rapidly cooled during the movement and becoming lower than the glass softening point, the saucer 2 is also heated by the heater 15 during the movement.
As shown in FIG. 3B, the tray 2 is moved directly below the pressing die 3, and at the same time, the pressing die 3, the temperature of which is controlled at 250 ° C., presses the molten glass block by the pressing cylinder 21.
The molten glass lump 1 is cooled, but before the contact surface between the pressing die 3 and the molten glass lump 1 becomes lower than the softening point of the glass as shown in FIG. I do.

【0048】その後、溶融ガラス塊は自然冷却される
が、図3(c)のように、溶融ガラス塊と受け皿の接触
面1bは、極めて良好な鏡面に磨かれた濡れ性の良い材
料2bと密着したままガラスの軟化点以下に冷却され
る。100℃以下の温度に徐冷してからガラス素材1’
を取り出しロボット20により装置内から取り出した。
Thereafter, the molten glass lump is naturally cooled, and as shown in FIG. 3 (c), the contact surface 1b between the molten glass lump and the saucer is made of a very wet mirror-polished material 2b. The glass is cooled to a temperature below the softening point of the glass while keeping the glass in close contact. Glass material 1 'after gradually cooling to a temperature of 100 ° C or less
Was taken out of the apparatus by the take-out robot 20.

【0049】本実施例によって得られたガラス素材1’
において、中心点平均粗さは1. 0μm以下の鏡面状態
で所望の転写面を有し、形状安定性は0.1mm以下で
あり光学顕微鏡観察した結果、表面に異物付着、傷、と
いった欠陥は認められなかった。
The glass material 1 'obtained according to this embodiment
Has a desired transfer surface in a mirror state having a center point average roughness of 1.0 μm or less, and has a shape stability of 0.1 mm or less. As a result of observation with an optical microscope, defects such as adhesion of foreign matter and scratches on the surface are I was not able to admit.

【0050】本実施例では、装置内を窒素ガス20リットル
/分、トリクロロトリフルオロエタン(C2Cl33
ガス1リットル/分の割合で混合したハロゲン化炭化水素雰
囲気とした。
In this embodiment, the inside of the apparatus is filled with 20 liters / minute of nitrogen gas and trichlorotrifluoroethane (C 2 Cl 3 F 3 ).
The atmosphere was a halogenated hydrocarbon atmosphere mixed at a rate of 1 liter / minute of gas.

【0051】(実施例6)図6と同一機能の製造装置を
用いて異なるガラス組成のガラス素材を作製した。受け
型2の中心部φ8の構成材料にグラッシーカーボンを、
外周部の構成材料にボロンナイトライドを選定し図2
(a)のように凹型に鏡面加工した。また、押圧型3の
中心部φ8の濡れ性の良い構成材料3bにグラッシーカ
ボンを、外周部の濡れ性の悪い構成材料3aに炭化珪素
を選定し図2(b)のように凸型に鏡面加工した。
Example 6 Glass materials having different glass compositions were produced using a production apparatus having the same functions as in FIG. Glassy carbon as the constituent material of the center part φ8 of the receiving mold 2,
Boron nitride was selected as the material of the outer periphery and Fig. 2
As shown in (a), it was mirror-finished into a concave shape. In addition, glassy carbon is selected as the material 3b having good wettability at the center portion φ8 of the pressing mold 3, and silicon carbide is selected as the material 3a having poor wettability at the outer periphery, and a convex mirror surface is formed as shown in FIG. processed.

【0052】溶融ガラスは、酸化珪素(SiO2)65
重量パ−セント、酸化カリウム(K2O)9重量パ−セ
ント、酸化ホウ素(B23)10重量パ−セント、酸化
ナトリウム(Na2O)10重量パ−セント、残部が微
量成分からなるホウケイ酸ガラスを用いた。このガラス
を1350℃で溶融したあと、920℃に保持した流出
口12から約1グラムの溶融ガラス10を予め350℃
に加熱された受け皿2に供給する。
The molten glass is made of silicon oxide (SiO 2 ) 65
Weight percent, potassium oxide (K 2 O) 9 weight percent, boron oxide (B 2 O 3 ) 10 weight percent, sodium oxide (Na 2 O) 10 weight percent, balance from trace components Borosilicate glass was used. After melting this glass at 1350 ° C., about 1 gram of molten glass 10 was introduced at 350 ° C. from outlet 12 kept at 920 ° C.
Is supplied to the tray 2 which has been heated.

【0053】次に、受け皿2を搬送用チェーンコンベア
16により押圧型3の下に移動する。移動時に溶融ガラ
ス塊が急冷され、ガラス軟化点以下になるのを防ぐた
め、受け皿2は移動時も加熱ヒータ15にて加熱する。
図4(b)のように受け皿2が押圧型3の真下に移動さ
れると同時に、300℃に温度コントロールされた押圧
型3は、押圧シリンダ21で溶融ガラス塊を加圧する。
溶融ガラス塊1が、ガラスの軟化点以下の温度に冷却さ
れるまでは、図4(b)のように溶融ガラス塊1を押圧
型3で加圧した状態を保持する。溶融ガラス塊1が冷却
され、ガラスの軟化点以下の温度になってから、加圧を
開放し次のステージへと搬送する。この時の、溶融ガラ
ス塊の押圧型との接触面1aは、押圧型3の良好な鏡面
が所望の大きさに転写され溶融ガラス塊が軟化点以下の
温度に冷却されているため、その形状が維持される。
Next, the receiving tray 2 is moved below the pressing die 3 by the transport chain conveyor 16. In order to prevent the molten glass lump from being rapidly cooled during the movement and becoming lower than the glass softening point, the saucer 2 is also heated by the heater 15 during the movement.
As shown in FIG. 4B, the tray 2 is moved directly below the pressing die 3, and at the same time, the pressing die 3, the temperature of which is controlled at 300 ° C., presses the molten glass block by the pressing cylinder 21.
Until the molten glass lump 1 is cooled to a temperature lower than the softening point of the glass, the state in which the molten glass lump 1 is pressed by the pressing mold 3 as shown in FIG. After the molten glass lump 1 is cooled to a temperature below the softening point of the glass, the pressure is released and the molten glass lump 1 is conveyed to the next stage. At this time, the contact surface 1a of the molten glass lump with the pressing die has a good mirror surface of the pressing die 3 transferred to a desired size and the molten glass lump is cooled to a temperature below the softening point. Is maintained.

【0054】その後、ガラス素材1’は自然冷却される
が、図4(c)のように、ガラス素材と受け皿の接触面
1bは、極めて良好な鏡面に磨かれた濡れ性の良い材料
2bと密着したまま100℃以下まで冷却し、ガラス素
材1’を取り出しロボット20により装置内から取り出
した。
Thereafter, the glass material 1 'is naturally cooled, but as shown in FIG. 4 (c), the contact surface 1b between the glass material and the saucer is made of a very wet mirror-polished material 2b. The glass material 1 ′ was cooled down to 100 ° C. or less while keeping the contact, and the glass material 1 ′ was taken out from the apparatus by the robot 20.

【0055】本実施例によって得られたガラス素材1’
において、中心点平均粗さは1. 0μm以下の鏡面状態
で所望の転写面を有し、形状安定性は0.1mm以下で
あり光学顕微鏡観察した結果、表面に異物付着、傷、と
いった欠陥は認められなかった。
Glass material 1 'obtained according to this embodiment
Has a desired transfer surface in a mirror state having a center point average roughness of 1.0 μm or less, and has a shape stability of 0.1 mm or less. As a result of observation with an optical microscope, defects such as adhesion of foreign matter and scratches on the surface are I was not able to admit.

【0056】以上、本発明の実施例を詳細に説明した
が、各実施例記載の受け皿の材質・形状は、溶融ガラス
の温度、ガラス組成、あるいはガラス素材の形状を考慮
し決められるもので限定するものではない。例えば、溶
融ガラスを直接受ける受け皿は、セラミック、アルミ
ナ、ジルコニア等の各種材料の組合せでも使用できる。
Although the embodiments of the present invention have been described in detail above, the material and shape of the saucer described in each embodiment are limited in consideration of the temperature of the molten glass, the glass composition, or the shape of the glass material. It does not do. For example, a saucer for directly receiving molten glass can be used in a combination of various materials such as ceramic, alumina, and zirconia.

【0057】非酸化性雰囲気は、窒素、アルゴン、ヘリ
ウム等の不活性ガス、およびこれらの不活性ガスに水
素、あるいは一酸化炭素、二酸化炭素の炭素酸化物、メ
タン、エタン、エチレン、トルエン等の炭化水素類、ト
リクロロエチレン、トリクロロトリフルオロエタン等の
ハロゲン化炭化水素類、エチレングリコ−ル、グリセリ
ン等のアルコ−ル類、F−113、F−11等のフルオ
ロカ−ボン類を適宜混合したものである。
The non-oxidizing atmosphere may be an inert gas such as nitrogen, argon or helium, or hydrogen or carbon monoxide, carbon oxides of carbon dioxide, methane, ethane, ethylene, toluene or the like. A mixture of hydrocarbons, halogenated hydrocarbons such as trichloroethylene and trichlorotrifluoroethane, alcohols such as ethylene glycol and glycerin, and fluorocarbons such as F-113 and F-11. is there.

【0058】なお、本発明は、各実施例に記載の光学ガ
ラスの組成、ガラス素材の形状、ガラス溶融炉や受け皿
の加熱の方法・条件等に限定されるものではない。
The present invention is not limited to the composition of the optical glass, the shape of the glass material, the method and conditions for heating the glass melting furnace and the saucer described in each embodiment.

【0059】[0059]

【発明の効果】本発明によれば、表面に欠陥がなく、所
望の形状のリヒートプレス用のガラス素材をエッチング
及び研磨工程無しに大量生産することが可能となり、生
産性の向上と製造コストの低減に著しい効果がある。
According to the present invention, it is possible to mass-produce a glass material for a reheat press having a desired shape without defects on the surface without etching and polishing steps, thereby improving productivity and reducing production costs. It has a remarkable effect on reduction.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の一実施例のガラス素材の製造方法を説
明するための断面図
FIG. 1 is a cross-sectional view for explaining a method of manufacturing a glass material according to one embodiment of the present invention.

【図2】同実施例において使用される受け皿の構成を示
す断面図
FIG. 2 is a sectional view showing a configuration of a tray used in the embodiment.

【図3】本発明の一実施例のガラス素材の製造方法の工
程を示す断面図
FIG. 3 is a sectional view showing steps of a method for manufacturing a glass material according to one embodiment of the present invention.

【図4】本発明の一実施例のガラス素材の製造方法を示
す断面図
FIG. 4 is a sectional view showing a method for manufacturing a glass material according to one embodiment of the present invention.

【図5】本発明の一実施例のガラス素材の製造装置の構
成を示す断面図
FIG. 5 is a sectional view showing a configuration of a glass material manufacturing apparatus according to one embodiment of the present invention.

【図6】本発明の一実施例のガラス素材の製造装置の構
成を示す断面図
FIG. 6 is a cross-sectional view showing a configuration of an apparatus for manufacturing a glass material according to one embodiment of the present invention.

【図7】従来例のガラス素材の製造方法を説明するため
の断面図
FIG. 7 is a cross-sectional view for explaining a conventional method for manufacturing a glass material.

【符号の説明】[Explanation of symbols]

1 溶融ガラス塊 1’ ガラス素材 1a 自由面 1b 接触面 2 受け皿 2a、3a 濡れ性の悪い材料 2b、3b 濡れ性の良い材料 3 押圧型 10 溶融ガラス 11 ガラス溶融炉 12 溶融ガラスの流出口 13、15、17 加熱ヒ−タ 14 切断刃 16 コンベア 18 冷却ガス 19 冷却ガス管 20 取り出しロボット 21 押圧シリンダ Reference Signs List 1 molten glass lump 1 'glass material 1a free surface 1b contact surface 2 saucer 2a, 3a material with poor wettability 2b, 3b material with good wettability 3 pressing mold 10 molten glass 11 glass melting furnace 12 outlet for molten glass 13, 15, 17 Heating heater 14 Cutting blade 16 Conveyor 18 Cooling gas 19 Cooling gas pipe 20 Take-out robot 21 Press cylinder

フロントページの続き (72)発明者 井上 孝志 大阪府門真市大字門真1006番地 松下電 器産業株式会社内 (72)発明者 室井 寿彦 東京都千代田区神田須田町1丁目28番地 株式会社住田光学ガラス内 (56)参考文献 特開 平3−60435(JP,A) 特開 平6−40730(JP,A) (58)調査した分野(Int.Cl.6,DB名) C03B 11/00 C03B 40/00 Continued on the front page (72) Inventor Takashi Inoue 1006 Kadoma, Kazuma, Osaka Prefecture Matsushita Electric Industrial Co., Ltd. (72) Inventor Toshihiko Muroi 1-28 Kandasudacho, Chiyoda-ku, Tokyo Sumita Optical Glass Co., Ltd. (56) References JP-A-3-60435 (JP, A) JP-A-6-40730 (JP, A) (58) Fields investigated (Int. Cl. 6 , DB name) C03B 11/00 C03B 40 / 00

Claims (25)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】溶融ガラスとの濡れ性の異なる少なくとも
2種類以上の材料により構成された受け皿で溶融ガラス
塊を受け、前記受け皿上で取り出し温度まで冷却しガラ
ス素材を作製することを特徴とするガラス素材の製造方
法。
The present invention is characterized in that a molten glass lump is received in a tray made of at least two or more kinds of materials having different wettability with the molten glass, and cooled to a take-out temperature on the tray to produce a glass material. Manufacturing method of glass material.
【請求項2】溶融ガラスとの濡れ性の異なる少なくとも
2種類以上の材料により構成された受け皿で溶融ガラス
塊を受け、前記溶融ガラス塊を押圧型で冷却加圧し、前
記受け皿上で取り出し温度まで冷却しガラス素材を作製
することを特徴とするガラス素材の製造方法。
2. A molten glass lump is received in a tray made of at least two or more types of materials having different wettability with the molten glass, and the molten glass lump is cooled and pressed by a pressing mold, and the temperature of the molten glass lump is reduced to a take-out temperature on the pan. A method for producing a glass material, comprising cooling the glass material.
【請求項3】溶融ガラスとの濡れ性の異なる少なくとも
2種類以上の材料により構成された受け皿で溶融ガラス
塊を受ける手段と、前記受け皿上で取り出し温度まで冷
却しガラス素材を作製する手段とを少なくとも備えたこ
とを特徴とするガラス素材の製造装置。
3. A means for receiving a lump of molten glass in a tray made of at least two or more materials having different wettability with the molten glass, and means for producing a glass material by cooling to a take-out temperature on the pan. An apparatus for manufacturing a glass material, at least comprising:
【請求項4】溶融ガラスとの濡れ性の異なる少なくとも
2種類以上の材料により構成された受け皿で溶融ガラス
塊を受ける手段と、前記溶融ガラス塊を押圧型で冷却加
圧する手段と、前記受け皿上で取り出し温度まで冷却し
ガラス素材を作製する手段とを少なくとも備えたことを
特徴とするガラス素材の製造装置。
4. A means for receiving a molten glass lump in a tray made of at least two or more materials having different wettability with the molten glass, a means for cooling and pressing the molten glass lump with a pressing die, and At least means for producing a glass material by cooling to a take-out temperature.
【請求項5】溶融ガラス塊の移載中心部に溶融ガラスと
濡れ性の良い材料を構成し、溶融ガラス塊の移載外周部
に溶融ガラスと濡れ性の悪い材料を構成した受け皿を使
用する請求項1または2記載のガラス素材の製造方法。
5. A saucer in which a material having good wettability with molten glass is formed at the center of the transfer of the molten glass lump, and a saucer having a material having poor wettability with the molten glass is used at the outer periphery of the transfer of the molten glass lump. The method for producing a glass material according to claim 1.
【請求項6】ガラス素材は、溶融ガラスと濡れ性の良い
材料と溶融ガラス塊との接触面積の増減により、所望の
転写面と形状を得る請求項1または2記載のガラス素材
の製造方法。
6. The method according to claim 1, wherein the glass material has a desired transfer surface and shape by increasing or decreasing the contact area between the material having good wettability with the molten glass and the molten glass lump.
【請求項7】溶融ガラス塊の移載中心部に溶融ガラスと
濡れ性の良い材料を構成し、溶融ガラス塊の移載外周部
に溶融ガラスと濡れ性の悪い材料を構成した受け皿を使
用する請求項3または4記載のガラス素材の製造装置。
7. A saucer in which a material having good wettability with molten glass is formed at the transfer center of the molten glass lump and a material which is formed of a material having poor wettability with the molten glass is used at the outer periphery of the transfer of the molten glass lump. An apparatus for producing a glass material according to claim 3.
【請求項8】溶融ガラス塊を予備加熱された受け皿で受
ける請求項1または2記載のガラス素材の製造方法。
8. The method for producing a glass material according to claim 1, wherein the molten glass lump is received in a preheated pan.
【請求項9】溶融ガラス塊を受ける受け皿は、溶融ガラ
ス塊が接するまでにガラス軟化点以下に加熱されている
請求項1または2記載のガラス素材の製造方法。
9. The method for producing a glass material according to claim 1, wherein the tray for receiving the molten glass mass is heated to a temperature lower than the glass softening point before the molten glass mass contacts.
【請求項10】溶融ガラス塊を受ける前に、受け皿を予
備加熱する手段を備えた請求項3または4記載のガラス
素材の製造装置。
10. An apparatus for manufacturing a glass material according to claim 3, further comprising means for preheating the tray before receiving the molten glass lump.
【請求項11】溶融ガラス塊を受ける受け皿は、所望の
ガラス素材の形状に近似した光学面を有する請求項1ま
たは2記載のガラス素材の製造方法。
11. The method according to claim 1, wherein the tray for receiving the molten glass mass has an optical surface approximate to a desired shape of the glass material.
【請求項12】溶融ガラス塊が受け皿に移載された後、
温度制御されたガスを溶融ガラス塊に吹き付け冷却する
請求項2記載のガラス素材の製造方法。
12. After the molten glass mass has been transferred to a saucer,
3. The method for producing a glass material according to claim 2, wherein a gas whose temperature is controlled is blown onto the molten glass lump and cooled.
【請求項13】溶融ガラス塊が受け皿に移載された後、
温度制御されたガスを溶融ガラス塊に吹き付け冷却する
手段を備えた請求項4記載のガラス素材の製造装置。
13. After the molten glass mass is transferred to a saucer,
The apparatus for producing a glass material according to claim 4, further comprising means for spraying a gas whose temperature is controlled to the molten glass lump to cool it.
【請求項14】所望のガラス素材の形状と近似した押圧
型を使用する請求項2記載のガラス素材の製造方法。
14. The method for producing a glass material according to claim 2, wherein a pressing die having a shape approximate to a desired shape of the glass material is used.
【請求項15】溶融ガラスと濡れ性の異なる少なくとも
2種類以上の材料により構成された押圧型を使用する請
求項2記載のガラス素材の製造方法。
15. The method for producing a glass material according to claim 2, wherein a pressing die made of at least two or more materials having different wettability from the molten glass is used.
【請求項16】溶融ガラス塊の中心部に接する面にガラ
スと濡れ性の良い材料を構成し、溶融ガラス塊の外周部
に接する面にガラスと濡れ性の悪い材料を構成した押圧
型を使用する請求項2記載のガラス素材の製造方法。
16. A pressing die comprising a material having good wettability with glass on a surface in contact with the center of the molten glass lump and a material having poor wettability with glass on a surface in contact with the outer periphery of the molten glass lump. The method for producing a glass material according to claim 2.
【請求項17】溶融ガラスと濡れ性の異なる少なくとも
2種類以上の材料により構成された押圧型を使用する請
求項4記載のガラス素材の製造装置。
17. The apparatus for manufacturing a glass material according to claim 4, wherein a pressing die made of at least two or more materials having different wettability from the molten glass is used.
【請求項18】溶融ガラス塊の中心部に接する面にガラ
スと濡れ性の良い材料を構成し、溶融ガラス塊の外周部
に接する面にガラスと濡れ性の悪い材料を構成した押圧
型を使用する請求項4記載のガラス素材の製造装置。
18. A pressing die comprising a material having good wettability with glass on a surface in contact with the center of the molten glass lump and a material having poor wettability with glass on a surface in contact with the outer periphery of the molten glass lump. The apparatus for manufacturing a glass material according to claim 4.
【請求項19】溶融ガラス塊が受け皿に移載された後、
ガラス軟化点以下に冷却される前に冷却加圧する請求項
2記載のガラス素材の製造方法。
19. After the molten glass mass is transferred to a saucer,
3. The method for producing a glass material according to claim 2, wherein cooling and pressurizing are performed before cooling to a temperature lower than the glass softening point.
【請求項20】溶融ガラス塊が受け皿に移載された後、
ガラス軟化点以下に冷却される前に冷却加圧する手段を
備えた請求項4記載のガラス素材の製造装置。
20. After the molten glass mass is transferred to a saucer,
The apparatus for producing a glass material according to claim 4, further comprising means for cooling and pressurizing before cooling to a temperature lower than the glass softening point.
【請求項21】ガラス素材は、受け皿に移載された溶融
ガラス塊を押圧型で冷却加圧し、ガラスの温度が軟化点
以下になる前に押圧型をガラスより開放することで、所
望の形状を得る請求項2記載のガラス素材の製造方法。
21. A glass material having a desired shape is obtained by cooling and pressurizing a molten glass mass transferred to a tray with a pressing die and releasing the pressing die from the glass before the temperature of the glass becomes lower than the softening point. 3. The method for producing a glass material according to claim 2, wherein
【請求項22】ガラス素材は、受け皿に移載された溶融
ガラス塊を押圧型で冷却加圧し、ガラスの温度を軟化点
以下に冷却してから押圧型をガラスより開放すること
で、所望の形状を得る請求項2記載のガラス素材の製造
方法。
22. The glass material is cooled and pressurized with a pressing mold on the molten glass mass transferred to the tray, and the temperature of the glass is cooled to a softening point or lower, and then the pressing mold is released from the glass to obtain a desired glass material. 3. The method for producing a glass material according to claim 2, wherein the shape is obtained.
【請求項23】押圧型は、ガラス軟化点以下に温度制御
されている請求項4記載のガラス素材の製造装置。
23. The apparatus for manufacturing a glass material according to claim 4, wherein the temperature of the pressing die is controlled to be equal to or lower than the glass softening point.
【請求項24】押圧型を、温度制御する手段を備えた請
求項4記載のガラス素材の製造装置。
24. The apparatus according to claim 4, further comprising means for controlling the temperature of the pressing die.
【請求項25】ガラス素材の取り出し温度が、ガラスの
軟化点以下である請求項1または2記載のガラス素材の
製造方法。
25. The method according to claim 1, wherein the temperature at which the glass material is taken out is equal to or lower than the softening point of the glass.
JP4143926A 1992-06-04 1992-06-04 Method and apparatus for manufacturing glass material Expired - Lifetime JP2892217B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP4143926A JP2892217B2 (en) 1992-06-04 1992-06-04 Method and apparatus for manufacturing glass material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP4143926A JP2892217B2 (en) 1992-06-04 1992-06-04 Method and apparatus for manufacturing glass material

Publications (2)

Publication Number Publication Date
JPH06127955A JPH06127955A (en) 1994-05-10
JP2892217B2 true JP2892217B2 (en) 1999-05-17

Family

ID=15350307

Family Applications (1)

Application Number Title Priority Date Filing Date
JP4143926A Expired - Lifetime JP2892217B2 (en) 1992-06-04 1992-06-04 Method and apparatus for manufacturing glass material

Country Status (1)

Country Link
JP (1) JP2892217B2 (en)

Also Published As

Publication number Publication date
JPH06127955A (en) 1994-05-10

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