JP2023002842A - Machine component for automobiles made of steel material for carburization excellent in static torsional strength and torsional fatigue strength - Google Patents

Machine component for automobiles made of steel material for carburization excellent in static torsional strength and torsional fatigue strength Download PDF

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JP2023002842A
JP2023002842A JP2022177732A JP2022177732A JP2023002842A JP 2023002842 A JP2023002842 A JP 2023002842A JP 2022177732 A JP2022177732 A JP 2022177732A JP 2022177732 A JP2022177732 A JP 2022177732A JP 2023002842 A JP2023002842 A JP 2023002842A
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武 宮▲崎▼
Takeshi Miyazaki
清志 田島
Kiyoshi Tajima
雅裕 石川
Masahiro Ishikawa
直生 ▲高▼林
Sunao Takabayashi
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Sanyo Special Steel Co Ltd
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Abstract

PROBLEM TO BE SOLVED: To provide a machine component for automobiles having a shot-peening layer in the induction hardened/tempered state of the machine component for automobiles made of a steel material for carburization hardening, and excellent in static torsional strength and torsional fatigue strength.
SOLUTION: Provided is a machine component for automobiles that contains, by mass%, C:0.33 to 0.43%, Si:0.45 to 0.65%, Mn:0.20 to 0.40%, P:0.030% or less, S:0.030% or less, Ni:0.25% or less, Cr:1.70 to 2.00%, Al:0.010 to 0.040% and N:0.0200% or less, and the balance Fe with inevitable impurities. In the case of a torsional test specimen of Fig. 1 for the machine component for automobiles in a carburization hardened/tempered state, the surface hardness is 650 Hv or more, the core hardness is 450 Hv or more, the hardened layer depth is 1.0 to 2.6 mm, the cross-sectional average hardness is 550 Hv or more, the grain size number of the surface is 7.0 or more, and the surface C concentration is 0.60 to 1.00%.
SELECTED DRAWING: Figure 1
COPYRIGHT: (C)2023,JPO&INPIT

Description

本発明は、静捩り強度ならびに捩り疲労強度に優れた浸炭用鋼材に関し、特に自動車のシャフト部材などの自動車用機械部品に関する。 TECHNICAL FIELD The present invention relates to a carburizing steel material excellent in static torsional strength and torsional fatigue strength, and more particularly to mechanical parts for automobiles such as automobile shaft members.

近年、自動車のエンジンにおいて高トルク化や高出力化が進んでいる。これに伴い、エンジンからの入力トルクを出力する軸物部品であるシャフト部材の高強度化の要請がある。さらに、シャフト部材は捩り応力が負荷されることから、静捩り強度や捩り疲労強度が要求される。
シャフト部材には、従来から、肌焼鋼として例えばSCr420やSCM420が用いられており、浸炭焼入れ・焼戻し材として浸炭処理がなされる場合がある。しかし前述のような自動車の高トルク化や高出力化の背景に伴い、さらなる静捩り強度、捩り疲労強度に優れたシャフト部材の自動車用機械部品の開発が求められている。
2. Description of the Related Art In recent years, there has been a trend toward higher torque and higher output in automobile engines. Along with this, there is a demand for increasing the strength of the shaft member, which is a shaft component that outputs the input torque from the engine. Furthermore, since the shaft member is subjected to torsional stress, static torsional strength and torsional fatigue strength are required.
Conventionally, SCr420 and SCM420, for example, are used as case hardening steels for shaft members, and carburizing treatment is sometimes performed as a carburizing, quenching and tempering material. However, with the increasing torque and output of automobiles as described above, there is a demand for the development of mechanical parts for automobiles, such as shaft members, which are even more excellent in static torsional strength and torsional fatigue strength.

そこで、肌焼鋼に浸炭処理を施して製造されるシャフト部材の高強度化に関する技術が提案されている。
たとえば、鋼の化学成分としてTeやCa、Zr、Mg、Y、希土類元素のうち1種または2種以上を含有させ、MnSの形態形成や圧延組織の制御によって、捩り疲労強度を向上させる方法が提案されている(例えば、特許文献1参照。)。
しかし、製鋼や圧延工程において操業条件に制約が出てしまう問題がある。
Accordingly, techniques have been proposed for increasing the strength of shaft members manufactured by carburizing case-hardened steel.
For example, one or more of Te, Ca, Zr, Mg, Y, and rare earth elements are included as chemical components of steel, and the torsional fatigue strength is improved by controlling the morphology of MnS and the rolling structure. It has been proposed (see Patent Document 1, for example).
However, there is a problem that operating conditions are restricted in the steelmaking and rolling processes.

また、浸炭用鋼において炭化物生成を抑制するCo、Ni、Cu、また炭化物を生成するCrを適正量添加することで、捩り疲労特性に優れた浸炭用鋼が提案されている(例えば、特許文献2参照。)。
しかし、さらなる静捩り強度、捩り疲労強度が望まれている。
In addition, a carburizing steel having excellent torsional fatigue properties has been proposed by adding an appropriate amount of Co, Ni, and Cu, which suppress the formation of carbides, and Cr, which forms carbides, in the carburizing steel (see, for example, Patent Document 2).
However, further static torsional strength and torsional fatigue strength are desired.

そして、部品コストの大幅な増加がなく、しかも捩り衝撃強度や捩り疲労強度に優れた浸炭用鋼が提案されている(例えば、特許文献3参照。)。
しかし、これは浸炭焼入れ時に、T(℃)=40×[Mn%]+75の式により算出される温度Tよりも低い温度の焼入れ油中に焼入れする必要があるなど、操業条件に制約が出てしまう。
Further, there has been proposed a carburizing steel that is excellent in torsional impact strength and torsional fatigue strength without a significant increase in part cost (see, for example, Patent Document 3).
However, this imposes restrictions on operating conditions, such as the need for quenching in quenching oil at a temperature lower than the temperature T calculated by the formula T (°C) = 40 x [Mn%] + 75 during carburizing and quenching. end up

また、鋼材鋳造時の冷却速度や熱間圧延時の操業条件の制約によって、長径が3μm以上の介在物粒子の平均アスペクト比を6.0以上、かつ介在物粒子の面積率を0.6%以下とすることで、捩り疲労強度に優れた浸炭用鋼材が提案されている(例えば、特許文献4参照。)。
しかし、製鋼や圧延工程において操業条件に制約が出てしまう問題がある。
In addition, due to restrictions on the cooling rate during steel casting and the operating conditions during hot rolling, the average aspect ratio of inclusion particles with a major axis of 3 μm or more is 6.0 or more, and the area ratio of inclusion particles is 0.6%. A carburizing steel material having excellent torsional fatigue strength has been proposed (see, for example, Patent Document 4).
However, there is a problem that operating conditions are restricted in the steelmaking and rolling processes.

さらに、B以外にMoを必須元素とし、浸炭焼入れ・焼戻し後の浸炭層深さを最適化することによって、部品コストの大幅な増加がなく、製造性に優れ、捩り疲労強度に優れた部材およびシャフトが提案されている(例えば、特許文献5参照。)。
しかし、さらなる静捩り強度、捩り疲労強度が望まれている。
Furthermore, by using Mo as an essential element in addition to B and optimizing the depth of the carburized layer after carburizing, quenching and tempering, there is no significant increase in the cost of parts, excellent manufacturability, and excellent torsional fatigue strength. A shaft has been proposed (see Patent Document 5, for example).
However, further static torsional strength and torsional fatigue strength are desired.

その他、化学成分と鋼材のジョミニー一端焼入れ法による硬さのみを規定することで、低サイクルねじり疲労強度に優れたシャフト用肌焼鋼が提案されている(例えば、特許文献6参照。)。もっともさらなる静捩り強度、捩り疲労強度が望まれている。 In addition, there has been proposed a case-hardening steel for shafts that is excellent in low-cycle torsional fatigue strength by specifying only the chemical composition and the hardness obtained by the Jominy single-end quenching method (see, for example, Patent Document 6). However, further static torsional strength and torsional fatigue strength are desired.

また、化学成分を6.0%≧2C+5Si+Cr-3Mn≧2.0%に規定することで、捩り疲労特性に優れた浸炭用鋼からなる鋼材とする提案がなされている(例えば特許文献7参照。)。しかし、化学成分のみでは機械部品としての特性を発揮させるには十分とはいいきれず、さらなる静捩り強度、捩り疲労強度が望まれている。 In addition, a steel material made of carburizing steel with excellent torsional fatigue properties has been proposed by specifying the chemical composition to be 6.0%≧2C+5Si+Cr-3Mn≧2.0% (see, for example, Patent Document 7). ). However, the chemical composition alone is not sufficient to exhibit the characteristics as a machine part, and further static torsional strength and torsional fatigue strength are desired.

特開2002-069573号公報JP-A-2002-069573 特開2003-183772号公報Japanese Patent Application Laid-Open No. 2003-183772 特開2003-239039号公報Japanese Patent Application Laid-Open No. 2003-239039 特開2004-107694号公報JP 2004-107694 A 特開2006-152330号公報JP 2006-152330 A 特開2009-293070号公報JP 2009-293070 A 特開2013-028860号公報JP 2013-028860 A

さて、浸炭処理以外にも、高周波焼入れによる機械部品の製造がなされている。もっとも、焼入れ処理前に所望の形状に加工する必要があるところ、高周波焼入れ用鋼のC含有量は一般に高いことが多いので、被削性に劣るところがある。また、高周波焼入れによる機械部品は一般的に曲げ疲労強度が高いとは限らない。そこで、捩り疲労強度の向上のみから高周波焼入れと同列に対比することはできないものであり、浸炭処理における機械部品についての捩り疲労特性等の向上が望まれている。 In addition to carburizing, induction hardening is also used to manufacture machine parts. However, since it is necessary to work the steel into a desired shape before the quenching treatment, the C content of the steel for induction hardening is generally high in many cases, so the machinability is sometimes inferior. In addition, mechanical parts made by induction hardening generally do not necessarily have high bending fatigue strength. Therefore, it cannot be compared with induction hardening only in terms of improvement in torsional fatigue strength, and it is desired to improve torsional fatigue characteristics of machine parts in carburizing treatment.

そこで、本発明が解決しようとする課題は、鋼材の化学成分の適正化をはかり、また浸炭焼入れ・焼戻し状態における鋼部品の硬さや硬化層の深さや、鋼部品の表面のC濃度を規定することで、従来から使用されてきた自動車用機械部品に比べて、より静捩り強度ならびに捩り疲労強度に優れた、シャフト部材の自動車用機械部品を提供することである。 Therefore, the problem to be solved by the present invention is to optimize the chemical composition of steel materials, and to define the hardness of steel parts in the carburized, quenched and tempered state, the depth of the hardened layer, and the C concentration on the surface of the steel parts. Thus, it is an object of the present invention to provide an automotive mechanical part of a shaft member which is superior in static torsional strength and torsional fatigue strength as compared with conventionally used automotive mechanical parts.

上記の課題を解決するための手段は、第1の手段では、化学成分として、質量%で、C:0.33~0.43%、Si:0.45~0.65%、Mn:0.20~0.40%、P:0.030%以下、S:0.030%以下、Ni:0.25%以下、Cr:1.70~2.00%、Al:0.010~0.040%、N:0.0200%以下を含有し、残部Feおよび不可避不純物からなり、浸炭焼入れ・焼戻し状態における鋼部品の、表面硬さが650Hv以上、芯部硬さが450Hv以上、全硬化層の深さが1.0~2.6mm、かつ下記式で表される断面平均硬さが550Hv以上、表面の結晶粒度番号が7.0以上、表面のC濃度が0.60~1.00%であることを特徴とする自動車用機械部品である。

Figure 2023002842000002
a:試験片の半径、Hv(r):ビッカース硬さ、r:中心からの距離 Means for solving the above problems are, in the first means, as chemical components, in mass%, C: 0.33 to 0.43%, Si: 0.45 to 0.65%, Mn: 0 .20-0.40%, P: 0.030% or less, S: 0.030% or less, Ni: 0.25% or less, Cr: 1.70-2.00%, Al: 0.010-0 .040%, N: 0.0200% or less, the balance being Fe and unavoidable impurities, and the surface hardness of the steel part in the carburized, quenched and tempered state is 650 Hv or more, the core hardness is 450 Hv or more, and the full hardening The layer depth is 1.0 to 2.6 mm, the average cross-sectional hardness represented by the following formula is 550 Hv or more, the surface grain size number is 7.0 or more, and the surface C concentration is 0.60 to 1.0. 00%.
Figure 2023002842000002
a: radius of test piece, Hv (r): Vickers hardness, r: distance from center

第2の手段では、第1の手段の化学成分に加えて、質量%で、Mo:0.10~0.30%、Nb:0.02~0.07%を含有し、残部Feおよび不可避不純物からなり、浸炭焼入れ・焼戻し状態における鋼部品の、表面硬さが650Hv以上、芯部硬さが450Hv以上、全硬化層の深さが1.0~2.6mm、かつ下記式で表される断面平均硬さが550Hv以上、表面の結晶粒度番号が7.0以上、表面のC濃度が0.60~1.00%であることを特徴とする自動車用機械部品である。

Figure 2023002842000003
a:試験片の半径、Hv(r):ビッカース硬さ、r:中心からの距離 In the second means, in addition to the chemical components of the first means, in mass%, Mo: 0.10 to 0.30%, Nb: 0.02 to 0.07%, the balance Fe and unavoidable The surface hardness of the steel part in the carburized, quenched and tempered state is 650 Hv or more, the core hardness is 450 Hv or more, the depth of the fully hardened layer is 1.0 to 2.6 mm, and is expressed by the following formula: An automotive mechanical part characterized by having an average cross-sectional hardness of 550 Hv or more, a surface grain size number of 7.0 or more, and a surface C concentration of 0.60 to 1.00%.
Figure 2023002842000003
a: radius of test piece, Hv (r): Vickers hardness, r: distance from center

第3の手段では、第1または第2の手段の化学成分に加えて、質量%で、Ti:0.010~0.050%、B:0.0003~0.0030%を含有し、残部Feおよび不可避不純物からなり、浸炭焼入れ・焼戻し状態における鋼部品の、表面硬さが650Hv以上、芯部硬さが450Hv以上、全硬化層の深さが1.0~2.6mm、かつ下記式で表される断面平均硬さが550Hv以上、表面の結晶粒度番号が7.0以上、表面のC濃度が0.60~1.00%であることを特徴とする自動車用機械部品である。

Figure 2023002842000004
a:試験片の半径、Hv(r):ビッカース硬さ、r:中心からの距離 In the third means, in addition to the chemical components of the first or second means, in mass%, Ti: 0.010 to 0.050%, B: 0.0003 to 0.0030%, the balance The surface hardness of the steel part in the carburized, quenched and tempered state, which is composed of Fe and inevitable impurities, is 650 Hv or more, the core hardness is 450 Hv or more, the depth of the hardened layer is 1.0 to 2.6 mm, and the following formula 550 Hv or more, a surface grain size number of 7.0 or more, and a surface C concentration of 0.60 to 1.00%.
Figure 2023002842000004
a: radius of test piece, Hv (r): Vickers hardness, r: distance from center

第4の手段では、自動車用機械部品は、浸炭焼入れ・焼戻しされた状態の自動車用機械部品にショットピーニング層を有し、このショットピーニング層の表面硬さが700Hv以上、かつ表面の圧縮残留応力が1000MPa以上の値を有していることを特徴とする第1~第3の手段のいずれか1の手段における自動車用機械部品である。 In the fourth means, the automotive mechanical part has a shot peening layer in the carburized, quenched and tempered automotive mechanical part, the surface hardness of the shot peening layer is 700 Hv or more, and the compressive residual stress on the surface is is a mechanical part for automobiles according to any one of the first to third means, characterized in that has a value of 1000 MPa or more.

第5の手段では、自動車用機械部品は、シャフト部材を有していることを特徴とする第1~第4の手段のいずれか1の手段における自動車用機械部品である。 A fifth means is the automobile mechanical part according to any one of the first to fourth means, characterized in that the automobile mechanical part has a shaft member.

本発明によると、本発明に規定する成分組成の浸炭焼入れ用鋼に対して、自動車、その他の産業用機械において、浸炭焼入れ・焼戻し処理すると、その自動車用機械部品は、その表面硬さが650Hv以上、芯部硬さが450Hv以上、硬化層深さが1.0~2.6mm、断面平均硬さが550Hv以上、表面の結晶粒度番号が7.0以上、かつ表面C濃度が0.60~1.00%である鋼部品とすることができるので、優れた静捩り強度および優れた捩り疲労強度を備えた自動車用機械部品が得られる。
また、上記の浸炭焼入れ・焼戻し後の鋼部品にショットピーニングをした鋼部品は、表面硬さが700Hv以上で、かつ表面の圧縮残留応力が1000MPa以上となることから、静捩り強度および捩り疲労強度において、より一層に優れた鋼部品となっている。
このように本発明は、自動車用機械部品のなかでも、とりわけ軸部を有するシャフト部材に好適な静捩り強度と捩り疲労特性を備えたものとなっている。
According to the present invention, carburizing, quenching, and tempering the steel for carburizing and quenching, which has the chemical composition specified in the present invention, in automobiles and other industrial machinery, the mechanical parts for automobiles have a surface hardness of 650 Hv. Above, the core hardness is 450 Hv or more, the hardened layer depth is 1.0 to 2.6 mm, the cross-sectional average hardness is 550 Hv or more, the surface grain size number is 7.0 or more, and the surface C concentration is 0.60. ∼1.00%, resulting in automotive mechanical parts with excellent static torsional strength and excellent torsional fatigue strength.
In addition, the steel parts obtained by shot peening after carburizing, quenching and tempering have a surface hardness of 700 Hv or more and a compressive residual stress on the surface of 1000 MPa or more, so static torsional strength and torsional fatigue strength , it has become a much more excellent steel part.
As described above, the present invention has static torsional strength and torsional fatigue characteristics suitable for a shaft member having a shaft portion, among mechanical parts for automobiles.

捩り試験片の形状を示す図である。It is a figure which shows the shape of a torsion test piece. 焼入れ・焼戻し条件を示す図で、(a)は焼入れ条件を示す図で、(b)は焼戻し条件を示す図である。It is a figure which shows hardening and tempering conditions, (a) is a figure which shows hardening conditions, (b) is a figure which shows tempering conditions.

本発明の実施の形態を詳述する前に、まず本発明における浸炭焼入れ用鋼の化学成分の限定理由について説明し、次いで、本発明における浸炭焼入れ用鋼材からなる自動車用機械部品の浸炭焼入れ・焼戻し状態における、表面硬さ、芯部硬さ、硬化層深さ、断面平均硬さ、表面の結晶粒度番号および表面のC濃度の各値の範囲の限定理由について説明する。 Before describing the embodiments of the present invention in detail, first, the reasons for limiting the chemical composition of the steel for carburizing and quenching in the present invention will be explained. The reasons for limiting the ranges of the surface hardness, core hardness, hardened layer depth, cross-sectional average hardness, surface grain size number, and surface C concentration in the tempered state will be explained.

先ず、本発明における浸炭焼入れ用鋼の化学成分の限定理由について以下に説明する。なお、これらの限定理由における%は、全て、質量%である。 First, the reason for limiting the chemical composition of the steel for carburizing and quenching in the present invention will be explained below. In addition, % in these reasons for limitation is all % by mass.

C:0.33~0.43%
Cは、浸炭焼入れ・焼戻し状態における、鋼部品の断面平均硬さ550Hv以上を確保するためには、Cは0.33%以上が必要である。
しかし、Cが0.43%を超えると、鋼材の被削性や冷間鍛造性を劣化させ、捩り試験時の鋼材の破壊が脆性破壊になり、かえって捩り強度が低下する。
そこで、Cは0.33~0.43%とする。
C: 0.33-0.43%
C needs to be 0.33% or more in order to secure a cross-sectional average hardness of 550 Hv or more of the steel part in the carburized, quenched and tempered state.
However, when C exceeds 0.43%, the machinability and cold forgeability of the steel material deteriorate, and the fracture of the steel material during the torsion test becomes brittle fracture, which rather reduces the torsional strength.
Therefore, C is set to 0.33 to 0.43%.

Si:0.45~0.65%
Siは、脱酸に必要な元素であり、また鋼材の焼入性や強度向上に有効な元素であり、粒界を強化する元素であり、捩り強度向上に有効な元素である。このためには、Siは0.45%以上が必要である。
しかし、Siが0.65%を超えると、焼なまし後のフェライト基地の硬さを上げ、冷間鍛造時に割れが発生しやすくなり、さらに被削性が低下する。
そこで、Siは0.45~0.65%とする。
Si: 0.45-0.65%
Si is an element necessary for deoxidation, an element effective for improving the hardenability and strength of steel materials, an element for strengthening grain boundaries, and an element effective for improving torsional strength. For this purpose, Si needs to be 0.45% or more.
However, when Si exceeds 0.65%, the hardness of the ferrite matrix after annealing is increased, cracks are likely to occur during cold forging, and machinability is further reduced.
Therefore, Si should be 0.45 to 0.65%.

Mn:0.20~0.40%
Mnは、脱酸に必要な元素で、さらに鋼の焼入性や強度向上に有効な元素である。このためには、Mnは0.20%以上が必要である。
しかし、Mnが0.40%を超えると、焼なまし後のフェライト基地の硬さを上げ、冷間鍛造時に割れを発生しやすくし、被削性が低下する。さらに、Pなどの脆化元素の粒界偏析を助長することで、鋼部品の捩り強度を低下させる。
そこで、Mnは0.20~0.40%とする。
Mn: 0.20-0.40%
Mn is an element necessary for deoxidation and is an element effective for improving the hardenability and strength of steel. For this purpose, Mn must be 0.20% or more.
However, when Mn exceeds 0.40%, the hardness of the ferrite matrix after annealing is increased, cracks are likely to occur during cold forging, and machinability is reduced. Furthermore, it reduces the torsional strength of steel parts by promoting grain boundary segregation of embrittlement elements such as P.
Therefore, Mn is set to 0.20 to 0.40%.

P:0.030%以下
Pは、粒界に偏析して捩り疲労強度を低下し、焼なまし後のフェライト基地の硬さを上げ、さらに冷間鍛造時に割れを発生しやすくする元素である。そこで、Pは0.030%以下とする。
P: 0.030% or less P is an element that segregates at grain boundaries to lower the torsional fatigue strength, increases the hardness of the ferrite matrix after annealing, and makes cracks more likely to occur during cold forging. . Therefore, P is set to 0.030% or less.

S:0.030%以下
Sは、被削性を向上させる元素であるが、Mnと結合してMnSを多く生成すると、冷間鍛造性や捩り強度を低下させる元素である。そこで、Sは0.030%以下とする。
S: 0.030% or less S is an element that improves machinability, but if it combines with Mn to form a large amount of MnS, it is an element that reduces cold forgeability and torsional strength. Therefore, S is set to 0.030% or less.

Ni:0.25%以下
Niは、焼なまし後のフェライト基地の硬さを上げ、冷間鍛造時に割れが発生しやすくし、被削性を低下させる作用のある元素である。そこで、Niは0.25%以下とする。
Ni: 0.25% or less Ni is an element that increases the hardness of the ferrite matrix after annealing, makes cracks more likely to occur during cold forging, and reduces machinability. Therefore, Ni should be 0.25% or less.

Cr:1.70~2.00%
Crは、鋼の焼入性向上に有効な元素である。このためには、Crは1.70%以上が必要である。
しかし、Crは、2.00%より多く含有されると、鋼部材の浸炭時に粗大炭化物や網状炭化物を生成して捩り強度を低下させる。
そこで、Crは1.70~2.00%とする。
Cr: 1.70-2.00%
Cr is an element effective in improving the hardenability of steel. For this purpose, Cr must be 1.70% or more.
However, when the Cr content exceeds 2.00%, coarse carbides and reticulated carbides are formed during carburizing of the steel member, which reduces the torsional strength.
Therefore, Cr is set to 1.70 to 2.00%.

Al:0.010~0.040%
Alは、脱酸に必要な元素である。さらに、Alは固溶Nと結合してAlNを形成することで浸炭時の結晶粒粗大化を抑制する元素である。このためには、Alは0.010%以上含有する必要がある。
さらに、Alは、鋼中にアルミナ系酸化物を増加し、鋼部品の捩り疲労強度を低下する。そこで、Alは0.040%以下にする必要がある。
そこで、Alは0.010~0.040%とする。
Al: 0.010-0.040%
Al is an element necessary for deoxidation. Furthermore, Al is an element that suppresses coarsening of crystal grains during carburizing by forming AlN in combination with solute N. For this purpose, it is necessary to contain 0.010% or more of Al.
In addition, Al increases alumina-based oxides in steel and reduces the torsional fatigue strength of steel parts. Therefore, Al needs to be 0.040% or less.
Therefore, Al is set to 0.010 to 0.040%.

N:0.0200%以下
Nは、鋼中でAlやNbと結合してAlNやNbCNを形成することで結晶粒粗大化を抑制する元素である。しかし、Nは、0.0200%より多く含有されると、鋼材の熱間加工性を劣化させてしまい、さらに、鋼材中に窒化物を形成することで、鋼部品の捩り疲労強度に対して悪影響を及ぼす。そこで、Nは0.0200%以下とする。
N: 0.0200% or less N is an element that suppresses grain coarsening by combining with Al and Nb in steel to form AlN and NbCN. However, if the N content exceeds 0.0200%, the hot workability of the steel material deteriorates, and furthermore, by forming nitrides in the steel material, the torsional fatigue strength of the steel parts is reduced. Adversely affect. Therefore, N is set to 0.0200% or less.

Mo:0.10~0.30%
Moは、鋼の焼入性や強度向上に有効であり、粒界を強化し、脆性破面を減少させる元素であり、さらに鋼部材の捩り強度向上に有効な元素である。このためには、Moは0.10%以上とする必要がある。
しかし、Moは、0.30%より多いと、焼なまし後のフェライト基地の硬さを上げ、冷間鍛造時に割れを発生し、被削性を低下し、さらに、鋼のコストを高める。
そこで、Moは0.10~0.30%とする。
Mo: 0.10-0.30%
Mo is an element that is effective for improving the hardenability and strength of steel, strengthens grain boundaries and reduces brittle fracture surfaces, and is an element that is effective for improving the torsional strength of steel members. For this purpose, Mo should be 0.10% or more.
However, when Mo is more than 0.30%, the hardness of the ferrite matrix after annealing increases, cracking occurs during cold forging, machinability decreases, and the cost of steel increases.
Therefore, Mo is set to 0.10 to 0.30%.

Nb:0.02~0.07%
Nbは、ナノオーダーの炭窒化物を形成することで結晶粒粗大化を抑制する元素であるが、Nbが0.02%未満ではその効果が得られない。
しかし、Nb0.07%より多いと、鋼材中にNb炭窒化物の量が過剰となって鋼材の加工性を低下させ、さらに浸炭時にCが表面に拡散侵入しにくくなる。
そこで、Nbは0.02~0.07%とする。
Nb: 0.02-0.07%
Nb is an element that suppresses grain coarsening by forming nano-order carbonitrides, but this effect cannot be obtained if the Nb content is less than 0.02%.
However, when Nb is more than 0.07%, the amount of Nb carbonitride in the steel material becomes excessive and the workability of the steel material is lowered, and furthermore, it becomes difficult for C to diffuse into the surface during carburizing.
Therefore, Nb is set to 0.02 to 0.07%.

Ti:0.010~0.050%
Tiは、Cと結合してTiCを形成することで、浸炭加熱時の結晶粒の粗大化を抑制する元素で、さらに、TiはNと結合することで、BがBNになることを防ぐ働きをする。そのためには、Tiは0.010%以上とする必要がある。
一方、Tiが0.050%より多いと、過剰なTiCやTiNの形成によって被削性や冷間鍛造性を低下させる。
そこで、Tiは0.010~0.050%とする。
Ti: 0.010-0.050%
Ti is an element that suppresses the coarsening of crystal grains during carburizing heating by combining with C to form TiC. Furthermore, Ti combines with N to prevent B from becoming BN. do. For that purpose, Ti needs to be 0.010% or more.
On the other hand, when Ti is more than 0.050%, the machinability and cold forgeability are deteriorated due to excessive formation of TiC and TiN.
Therefore, Ti should be 0.010 to 0.050%.

B:0.0003~0.0030%
Bは、少量の添加によって鋼の焼入性を著しく向上させる元素で、Bの添加によって他の合金元素の添加量を減らすことができる。さらに、Bは粒界を強化し、脆性破面を減少させる元素であり、さらに、鋼材のねじり強度向上に有効な元素である。これらのためには、Bは0.0003%以上とする必要がある。
しかし、Bが0.0030%より多く含有されても、焼入性や強度の向上効果は飽和する。
そこで、Bは0.0003~0.0030%とする。
B: 0.0003 to 0.0030%
B is an element that significantly improves the hardenability of steel when added in a small amount, and the addition of B can reduce the amount of other alloying elements added. Furthermore, B is an element that strengthens grain boundaries and reduces brittle fracture surfaces, and is an element that is effective in improving the torsional strength of steel materials. For these, B needs to be 0.0003% or more.
However, even if the B content exceeds 0.0030%, the effect of improving hardenability and strength is saturated.
Therefore, B is set to 0.0003 to 0.0030%.

本発明の自動車用機械部品は、本発明に規定する化学成分の浸炭焼入れ用鋼材を冷間鍛造、熱間鍛造、切削加工等によって所定の形状のシャフト部材や自動車用機械部品の形状へと成形、適宜の熱処理等をした後、部品表面に浸炭焼入れ・焼戻しすること、さらに必要に応じてショットピーニングを付与することで得られる。そこで、本発明における浸炭焼入れ用鋼材からなる自動車用機械部品を、浸炭焼入れ・焼戻し後の、浸炭焼入れ・焼戻し状態における鋼部品の、表面硬さ、芯部硬さ、硬化層深さ、断面平均硬さ、表面の結晶粒度番号および表面のC濃度の各値の範囲の限定理由について説明する。 The mechanical parts for automobiles of the present invention are formed by cold forging, hot forging, cutting, etc., of carburizing and quenching steel materials having the chemical composition specified in the present invention, into shaft members of predetermined shapes and mechanical parts for automobiles. It can be obtained by subjecting the surface of the component to carburizing, quenching, tempering, and, if necessary, subjecting it to shot peening. Therefore, the surface hardness, core hardness, hardening layer depth, cross-sectional average The reasons for limiting the ranges of the hardness, surface grain size number, and surface C concentration will be explained.

表面硬さ:650Hv以上
表面硬さは、断面平均硬さを増加させて鋼部材の捩り強度を向上させる。このためには、表面硬さは650Hv以上が必要である。
Surface hardness: 650 Hv or more Surface hardness increases the cross-sectional average hardness and improves the torsional strength of the steel member. For this purpose, a surface hardness of 650 Hv or more is required.

芯部硬さ(すなわち非硬化層):450Hv以上
芯部硬さ(すなわち非硬化層)は、断面平均硬さを増加させて、鋼部材の捩り強度を向上させる。このためには、芯部硬さ(すなわち非硬化層)は450Hv以上が必要である。
Core Hardness (ie, Non-Hardened Layer): 450 Hv or More The core hardness (that is, non-hardened layer) increases the cross-sectional average hardness and improves the torsional strength of the steel member. For this purpose, the hardness of the core (that is, the non-hardened layer) must be 450 Hv or more.

硬化層深さ:1.0~2.6mm
硬化層深さは、断面平均硬さを上昇させて、鋼部材の捩り強度を向上させる。このためには、硬化層深さは1.0mm以上が必要である。
しかし、硬化層深さが2.6mmより深いと、長時間の浸炭が必要になることで、粗大炭化物や網状炭化物を形成しやすくなり、鋼部材の捩り強度が低下する。
そこで、全硬化層深さは1.0~2.6mmとする。
Hardened layer depth: 1.0 to 2.6 mm
The hardened layer depth increases the cross-sectional average hardness and improves the torsional strength of the steel member. For this purpose, the hardened layer depth must be 1.0 mm or more.
However, if the hardening layer depth is greater than 2.6 mm, long carburization is required, and coarse carbides and reticulated carbides are likely to be formed, and the torsional strength of the steel member is reduced.
Therefore, the total hardened layer depth is set to 1.0 to 2.6 mm.

断面平均硬さ:550Hv以上
断面平均硬さは、鋼部材の捩り強度を向上させる。このためには、断面平均硬さは550Hv以上が必要である。
Cross-sectional average hardness: 550 Hv or more The cross-sectional average hardness improves the torsional strength of the steel member. For this purpose, a cross-sectional average hardness of 550 Hv or more is required.

表面の結晶粒度番号:7.0以上
表面の結晶粒度番号は、その番号が大きい方が鋼部材の捩り強度向上に有効であり、また、粒界脆化元素であるP、Sの粒界偏析量を減少させる働きをする。このためには、表面の結晶粒度番号は7.0以上が必要である。
Surface grain size number: 7.0 or more The larger the surface grain size number, the more effective it is in improving the torsional strength of the steel member. Acts as a volume reducer. For this purpose, the crystal grain size number of the surface must be 7.0 or more.

表面C濃度:0.60~1.00%
表面C濃度は、鋼部材の表面硬さに影響する。したがって、表面C濃度が0.60%より少ないと表面硬さが650Hv以下となる。
しかし、表面C濃度が1.00%を超えると、粗大炭化物や網状炭化物を形成することで鋼部材の捩り強度が低下し、さらに、軟質な残留オーステナイトが多く形成されることで、表面硬さの低下を招くこととなる。そこで、表面C濃度は0.60~1.00%とする。
Surface C concentration: 0.60 to 1.00%
The surface C concentration affects the surface hardness of the steel member. Therefore, if the surface C concentration is less than 0.60%, the surface hardness will be 650 Hv or less.
However, when the surface C concentration exceeds 1.00%, the torsional strength of the steel member decreases due to the formation of coarse carbides and network carbides. will lead to a decline in Therefore, the surface C concentration is set to 0.60 to 1.00%.

次いで、浸炭焼入れ・焼戻した鋼部材にショットピーニングした鋼部材の各表面硬さおよび圧縮残留応力の限定理由について以下に説明する。 Next, the reasons for limiting each surface hardness and compressive residual stress of a steel member which is shot peened to a carburized, quenched and tempered steel member will be explained below.

表面硬さ:700Hv以上
表面硬さは、700Hvより少ないと、鋼部材の断面平均硬さが低く、鋼部材の捩り強度を低くする。そこで、鋼部材の断面平均硬さを増加し、鋼部材の捩り強度を向上させるために、表面硬さは700Hv以上とする
Surface hardness: 700 Hv or more If the surface hardness is less than 700 Hv, the average cross-sectional hardness of the steel member is low, and the torsional strength of the steel member is low. Therefore, in order to increase the cross-sectional average hardness of the steel member and improve the torsional strength of the steel member, the surface hardness is set to 700 Hv or more.

圧縮残留応力:1000MPa以上
表面の圧縮残留応力は、鋼部材の捩り強度を向上させて、圧縮残留応力によってき裂の生成・伝播が遅延される。そのためには、表面の圧縮残留応力は1000MPa以上とする必要がある。
Compressive residual stress: 1000 MPa or more The compressive residual stress on the surface improves the torsional strength of the steel member, and the compressive residual stress delays the generation and propagation of cracks. For that purpose, the compressive residual stress on the surface needs to be 1000 MPa or more.

ここで、本発明の浸炭焼入れ・焼戻し用鋼を用いる実施の形態について説明するため、鋼材の化学成分について、本願発明の規定範囲に相当する供試材のNo.1~8と、規定する成分範囲から外れる供試材のNo.9~12を示す。なお、表1の化学成分の含有量は質量%であり、表1の記載からは、Feおよび不可避不純物は除かれている。
また、供試材No.10はJIS(日本工業規格)のSCr420、供試材No.11はJISのSCM420、供試材No.12はJISのSNCM420である。
Here, in order to describe an embodiment using the steel for carburizing, quenching and tempering of the present invention, the chemical composition of the steel material will be described with reference to the No. of the test material corresponding to the specified range of the present invention. 1 to 8, and No. of the test material outside the specified range of components. 9-12 are shown. The content of the chemical components in Table 1 is in mass %, and Fe and unavoidable impurities are excluded from Table 1.
Moreover, test material No. 10 is SCr420 of JIS (Japanese Industrial Standards), test material No. 11 is SCM420 of JIS, test material No. 12 is JIS SNCM420.

Figure 2023002842000005
Figure 2023002842000005

次に、表2及び表3に、浸炭処理等された試験片による実施例、比較例の特性が記載されている。なお、表中の実施例及び比較例の「No.」の値は、試験片に用いた供試材の「No.」に対応しており、その化学成分を示すものであり、試験片の鋼材が表1の供試材No.1~12のいずれであったかを示している。
さらに表2には、各供試材が(a)浸炭焼入れ・焼戻し処理(浸炭処理)された場合の、
表3には、各供試材に(b)浸炭処理が加えられてショットピーニングを付してショットピーニング層が形成された場合の、浸炭焼入れ・焼戻し状態における表面硬さ、芯部硬さ、硬化層深さ、断面平均硬さ、表面の結晶粒度番号、表面C濃度、浸炭焼入れ鋼およびショットピーニング層の表面硬さ、浸炭焼入れ鋼およびショットピーニング層の圧縮残留応力、静捩り強度比、捩り疲労強度比を記載して示している。
Next, Tables 2 and 3 describe the characteristics of Examples and Comparative Examples using test pieces subjected to carburizing treatment or the like. The "No." values of the examples and comparative examples in the table correspond to the "No." The test material No. in Table 1 is used as the steel material. It shows which of 1 to 12 it was.
Furthermore, in Table 2, when each test material is (a) carburized, quenched and tempered (carburized),
Table 3 shows the surface hardness, core hardness, Hardened layer depth, cross-sectional average hardness, surface grain size number, surface C concentration, surface hardness of carburized hardened steel and shot peening layer, compressive residual stress of carburized hardened steel and shot peened layer, static torsional strength ratio, torsion Fatigue strength ratios are listed and shown.

表2および表3に実施例として示すものは、供試材No.1~No.3、供試材No.5~No.7を用いた実施例No.1(a)、実施例No.1(b)、実施例No.2(a)、実施例No.2(b)、実施例No.3(a)、実施例No.3(b)、実施例No.5(a)、実施例No.5(b)、実施例No.6(a)、実施例No.6(b)、実施例7No.(a)、実施例No.7(b)である。
また、表2及び表3には、比較例として、供試材No.4、供試材No.8~No.12を用いた比較例No.4(a)、比較例No.4(b)、比較例No.8(a)、比較例No.8(b)、比較例No.9(a)、比較例No.9(b)、比較例No.10(a)、比較例No.10(b)、比較例No.11(a)、比較例No.11(b)、比較例No.12(b)を示す。
なお、表2、表3における静捩り強度比と、捩り疲労強度比は、いずれも、表2の比較例No.10(a)の浸炭焼入れ焼戻しされた場合の鋼部品の強度を1.00とした場合の、これに対する比を示したものである。
Examples shown in Tables 2 and 3 are test material Nos. 1 to No. 3, test material No. 5 to No. Example no. 1(a), Example No. 1(b), Example No. 2(a), Example No. 2(b), Example No. 3(a), Example No. 3(b), Example No. 5(a), Example No. 5(b), Example No. 6(a), Example No. 6(b), Example 7 No. (a), Example No. 7(b).
Tables 2 and 3 also show test material No. 1 as a comparative example. 4, test material No. 8 to No. Comparative Example No. 12 using 4(a), Comparative Example No. 4(b), Comparative Example No. 8(a), Comparative Example No. 8(b), Comparative Example No. 9(a), Comparative Example No. 9(b), Comparative Example No. 10(a), Comparative Example No. 10(b), Comparative Example No. 11(a), Comparative Example No. 11(b), Comparative Example No. 12(b).
Note that the static torsional strength ratio and the torsional fatigue strength ratio in Tables 2 and 3 are both for Comparative Example No. 2 in Table 2. 10(a) shows the ratio to 1.00, the strength of the carburized, quenched and tempered steel part of 10(a).

Figure 2023002842000006
Figure 2023002842000006

Figure 2023002842000007
Figure 2023002842000007

(表2、表3に関する手順について)
さて、表1に示された化学成分を有し残部がFe及び不可避不純物からなる供試材を、100kg真空溶解炉で溶製し、直径45mmに熱間鍛伸した後に放冷し、次いで、焼ならしを行ない、さらに、低温焼なましとして720℃に4時間保持した後、空冷して、図1に示す捩り試験片1に加工した。
そして、この捩り試験片1は、図2に示す、浸炭焼入れ・焼戻し条件で、浸炭焼入れ・焼戻し処理を行なった。すなわち、930℃まで加熱し0.5時間予熱として保持し、その後930℃で3時間浸炭し、引き続き930℃に2.5時間保持して拡散、その後850℃に0.5時間保持した後、60℃の油に油焼入れした。その後焼戻しとして、180℃まで昇温して1.5時間保持後、空冷した。
また、上記の浸炭処理工程に続いてショットピーニングを施して、ショットピーニング層を付与した。
さらに、この捩り試験片1に、表2、表3に示す、静捩り強度および捩り疲労強度の試験を実施した。
(Regarding procedures for Tables 2 and 3)
Now, a test material having the chemical composition shown in Table 1 and having the balance of Fe and unavoidable impurities is melted in a 100 kg vacuum melting furnace, hot forged to a diameter of 45 mm, and then allowed to cool. After normalizing and holding at 720° C. for 4 hours as low temperature annealing, it was air-cooled and processed into a torsion test piece 1 shown in FIG.
Then, this torsion test piece 1 was subjected to carburizing, quenching, and tempering treatment under the carburizing, quenching, and tempering conditions shown in FIG. That is, it is heated to 930°C and held as preheat for 0.5 hours, then carburized at 930°C for 3 hours, subsequently held at 930°C for 2.5 hours for diffusion, and then held at 850°C for 0.5 hours, followed by It was oil quenched in oil at 60°C. After that, as tempering, the temperature was raised to 180° C., held for 1.5 hours, and then air-cooled.
Shot peening was applied following the above carburizing treatment step to provide a shot peening layer.
Furthermore, this torsional test piece 1 was tested for static torsional strength and torsional fatigue strength shown in Tables 2 and 3.

図1に、捩り試験片1の形状を示す。捩り試験片1は、長さ150mmで、30mm角であり、軸方向に沿ってφ7mmの貫通穴を、長手中央部に軸方向に垂直な縦方向にφ4mmの貫通穴をそれぞれ有している。 The shape of the torsion test piece 1 is shown in FIG. The torsion test piece 1 has a length of 150 mm and a size of 30 mm square, and has a through hole of φ7 mm along the axial direction and a through hole of φ4 mm in the vertical direction perpendicular to the axial direction in the center of the longitudinal direction.

表2、表3の静捩り強度は、油圧サーボ式捩り疲労試験機によって、負荷トルク-試験角度のデータから得た比例限度の値による。
また、捩り疲労強度は、両振り、周波数5Hzの条件で、105サイクル疲労強度の値による。
なお、これらにおける比の値は、比較例No.10(a)の浸炭焼入れ焼戻しされた場合の値を1.00としたときの、これに対する比の値である。
The static torsional strengths in Tables 2 and 3 are based on proportional limit values obtained from load torque-test angle data by a hydraulic servo type torsional fatigue tester.
Also, the torsional fatigue strength is based on the value of 10 5 cycle fatigue strength under the conditions of both swings and a frequency of 5 Hz.
In addition, the value of the ratio in these is comparative example No. 10(a) carburized, quenched and tempered to 1.00.

表2と表3に示す静捩り強度比は、比較例No.10(a)の浸炭焼入れ焼戻しされた場合の値を1.00としたときの比であるところ、表2の静捩り強度比は実施例No.1(a)が1.69、実施例No.2(a)では1.79、実施例No.3(a)の静捩り強度比が1.81で、実施例No.5(a)が1.67、実施例No.6(a)が1.74、実施例No.7(a)が1.83であることから、本発明の実施例では、浸炭焼入れ焼戻しされた状態の鋼部材でも優れた特性を備えているといえる。 The static torsional strength ratios shown in Tables 2 and 3 are the same as those of Comparative Example No. 10(a) after carburizing, quenching and tempering is taken as 1.00. 1(a) is 1.69, Example No. 2(a) is 1.79, Example No. 3(a) has a static torsional strength ratio of 1.81, and Example No. 5(a) is 1.67, Example No. 6(a) is 1.74, Example No. Since 7(a) is 1.83, it can be said that the steel member in the carburized, quenched and tempered state has excellent properties in the example of the present invention.

また、表3に示すように、実施例のうち(b)のように浸炭処理後にショットピーニングを付して、ショットピーニング層を形成させたものでは、その静捩り強度比は、実施例No.1(b)が1.90、実施例No.2(b)が1.99、実施例No.3(b)が2.05、実施例No.5(b)が2.16、実施例No.6(b)が2.07、実施例No.7(b)が2.31であり、これらはショットピーニングに付されたことで(a)の場合よりもさらに優れる結果になった。 Further, as shown in Table 3, in the example (b) in which shot peening was applied after the carburizing treatment to form a shot peening layer, the static torsional strength ratio was lower than that of Example No. 3. 1(b) is 1.90, Example No. 2(b) is 1.99, Example No. 3(b) is 2.05, Example No. 5(b) is 2.16, Example No. 6(b) is 2.07, Example No. 7(b) was 2.31, and these were shot peened even better than (a).

表2と表3に示す捩り疲労強度比は、比較例No.10(a)の浸炭焼入れ焼戻しされた場合の値を1.00としたときの比であるところ、表2の捩り疲労強度比は、実施例No.1(a)が1.05、実施例No.2(a)では1.06、実施例No.3(a)の静捩り強度比が1.07で、実施例No.5(a)が1.05、実施例No.6(a)が1.07、実施例No.7(a)が1.10であり、表2の比較例よりも良好である。 The torsional fatigue strength ratios shown in Tables 2 and 3 are for Comparative Example No. The torsional fatigue strength ratio in Table 2 is the ratio when the value in the case of carburizing, quenching and tempering of 10(a) is taken as 1.00. 1(a) is 1.05, Example No. 2(a) is 1.06, Example No. 3(a) has a static torsional strength ratio of 1.07, and Example No. 5(a) is 1.05, Example No. 6(a) is 1.07, Example No. 7(a) is 1.10, which is better than the comparative examples in Table 2.

また、表3に示すように、実施例のうち(b)のように浸炭処理後にショットピーニングを付してショットピーニング層を形成させたものでは、その捩り疲労強度比は、実施例No.1(b)が1.52、実施例No.2(b)が1.54、実施例No.3(b)が1.65、実施例No.5(b)が1.62、実施例No.6(b)が1.63、実施例No.7(b)が1.73であり、いずれも高強度のSNCM420からなる比較例No.12(b)の捩り疲労強度比1.47と比しても、より高強度である。また、比較例No.4(b)、比較例No.8(b)、比較例No.9(b)、比較例No.10(b)、比較例No.11(b)に比しても、捩り疲労強度比に優れている。 Further, as shown in Table 3, in Example (b), shot peening was applied after carburizing treatment to form a shot peening layer, and the torsional fatigue strength ratio was lower than that of Example No. 3. 1(b) is 1.52, Example No. 2(b) is 1.54, Example No. 3(b) is 1.65, Example No. 5(b) is 1.62, Example No. 6(b) is 1.63, Example No. 7(b) is 1.73, and Comparative Example No. 7 (b) is all made of high-strength SNCM420. Even compared with the torsional fatigue strength ratio of 1.47 in 12(b), the strength is higher. Also, Comparative Example No. 4(b), Comparative Example No. 8(b), Comparative Example No. 9(b), Comparative Example No. 10(b), Comparative Example No. Compared to 11(b), it is excellent in torsional fatigue strength ratio.

このように、実施例の静捩り強度、捩り疲労強度が優れている理由としては、鋼の化学成分、浸炭焼入れ・焼戻し後の熱処理品質が最適化され、破断後の表面の脆性破面率が低減されたことが、挙げられる。 Thus, the reason why the static torsional strength and torsional fatigue strength of the examples are excellent is that the chemical composition of the steel and the heat treatment quality after carburizing, quenching and tempering are optimized, and the brittle fracture surface ratio of the surface after fracture is reduced. It is mentioned that it was reduced.

さて、供試材No.4を用いた比較例No.4(a)および比較例No.4(b)は、浸炭時の平衡炭素濃度を他条件に比べて2/3に低減し、表面C濃度が0.55%(なお、本発明の手段では表面C濃度が0.60~1.00%である。)で低かったため、表面硬さ、断面平均硬さが低くなり、ほぼ同じ化学成分である供試材No.3(表面C濃度は0.85%である。)の実施例No.3(a)およびNo.3(b)に比して、捩り強度が低くなっている。 By the way, test material No. Comparative example no. 4(a) and comparative example no. 4(b) reduces the equilibrium carbon concentration at the time of carburizing to 2/3 compared to other conditions, and the surface C concentration is 0.55% (in the means of the present invention, the surface C concentration is 0.60 to 1 .00%), the surface hardness and cross-sectional average hardness are low, and the test material No. 1, which has almost the same chemical composition, has a low surface hardness and a low cross-sectional average hardness. Example No. 3 (surface C concentration is 0.85%). 3(a) and no. Compared to 3(b), the torsional strength is low.

さて、供試材No.8を用いた比較例No.8(a)および比較例No.8(b)は、浸炭時の平衡炭素濃度を他条件に比べて2/3に低減し、表面C濃度が0.55%(なお、本発明の手段では表面C濃度が0.60~1.00%である。)で低かったため、表面硬さ、断面平均硬さが低くなり、ほぼ同じ化学成分である供試材No.7(表面C濃度は0.90%である。)の実施例No.3(a)およびNo.3(b)に比して、捩り強度が低くなっている。 By the way, test material No. Comparative example no. 8(a) and comparative example no. 8(b) reduces the equilibrium carbon concentration at the time of carburizing to 2/3 compared to other conditions, and the surface C concentration is 0.55% (in the means of the present invention, the surface C concentration is 0.60 to 1 .00%), the surface hardness and cross-sectional average hardness are low, and the test material No. 1, which has almost the same chemical composition, has a low surface hardness and a low cross-sectional average hardness. Example No. 7 (surface C concentration is 0.90%). 3(a) and no. Compared to 3(b), the torsional strength is low.

また、供試材No.9を用いた比較例No.9(a)および比較例No.9(b)は、表面の結晶粒度番号が6.8であり、本発明の7.0を下回るため、静捩り強度、捩り疲労強度が低くなった。
これは、供試材No.9では、Moが0.32%(なお、本発明の手段ではMoは0.10~0.30%である。)であったことから、浸炭前組織が粒度特性に不利なベイナイト+マルテンサイト組織になったこと、またピンニング粒子として寄与するNbが添加されなかったために、結晶粒度番号が本発明の規定する7.0を下回ることになったためである。
Moreover, test material No. Comparative example no. 9(a) and comparative example no. 9(b) had a surface crystal grain size number of 6.8, which was lower than 7.0 of the present invention, and therefore had low static torsional strength and low torsional fatigue strength.
This is the test material No. In No. 9, Mo was 0.32% (In the means of the present invention, Mo is 0.10 to 0.30%.), so the structure before carburization is bainite + martensite, which is disadvantageous in grain size characteristics. This is because the crystal grain size number fell below 7.0 specified in the present invention due to the formation of a texture and the absence of Nb that contributes as pinning particles.

次に、断面平均硬さは、表面から芯部までの硬さ分布を求めた後、面積に対応させて重み付き積分を行ない、全断面積で割ることにより求めた値であり、Hvで示している。次の段落に、この重み付き積分の式を示す。 Next, the average cross-sectional hardness is a value obtained by determining the hardness distribution from the surface to the core, performing weighted integration corresponding to the area, and dividing by the total cross-sectional area, and is expressed in Hv. ing. The next paragraph gives the formula for this weighted integral.

Figure 2023002842000008
a:捩り試験片1の半径、Hv(r):ビッカース硬さ、r:中心からの距離
Figure 2023002842000008
a: radius of torsion test piece 1, Hv (r): Vickers hardness, r: distance from center

表2に示す、表面の結晶粒度番号は光学顕微鏡400倍または1000倍で撮影した2視野から、JIS G 0551の切断法によって算出した。さらに、表面のC濃度はEPMA(Electron Probe Micro Analyzer)で測定を実施した。 The crystal grain size number of the surface shown in Table 2 was calculated by the cutting method of JIS G 0551 from two fields of view taken with an optical microscope at a magnification of 400 or 1000. Furthermore, the C concentration on the surface was measured with an EPMA (Electron Probe Micro Analyzer).

また、ショットピーニグ層の圧縮残留応力は、表面~100μmまでを電界研磨によって追い込み、X線回折を用いて測定した。表2では圧縮残留応力が1300Paと、高い値を示している。 In addition, the compressive residual stress of the shot peening layer was measured by electropolishing to 100 μm from the surface and using X-ray diffraction. Table 2 shows a high compressive residual stress of 1300 Pa.

1 捩り試験片
2 φ7mmの貫通穴
3 φ4mmの貫通穴
1 torsion test piece 2 φ7mm through hole 3 φ4mm through hole

Claims (4)

化学成分として、質量%で、C:0.33~0.43%、Si:0.45~0.65%、Mn:0.20~0.40%、P:0.030%以下、S:0.030%以下、Ni:0.25%以下、Cr:1.70~2.00%、Al:0.010~0.040%、N:0.0200%以下を含有し、残部Feおよび不可避不純物からなり、浸炭焼入れ・焼戻し状態における鋼部品の、表面硬さが650Hv以上、芯部硬さが450Hv以上、全硬化層の深さが1.0~2.6mm、かつ下記式で表される断面平均硬さが550Hv以上、表面の結晶粒度番号が7.0以上、表面のC濃度が0.60~1.00%であることを特徴とする鋼部品。
Figure 2023002842000009
a:捩り試験片1の半径、Hv(r):ビッカース硬さ、r:中心からの距離
As chemical components, in mass%, C: 0.33 to 0.43%, Si: 0.45 to 0.65%, Mn: 0.20 to 0.40%, P: 0.030% or less, S : 0.030% or less, Ni: 0.25% or less, Cr: 1.70 to 2.00%, Al: 0.010 to 0.040%, N: 0.0200% or less, and the balance Fe and unavoidable impurities, the surface hardness of the steel part in the carburized, quenched and tempered state is 650 Hv or more, the core hardness is 450 Hv or more, the depth of the fully hardened layer is 1.0 to 2.6 mm, and the following formula A steel part having an average cross-sectional hardness of 550 Hv or more, a surface grain size number of 7.0 or more, and a surface C concentration of 0.60 to 1.00%.
Figure 2023002842000009
a: radius of torsion test piece 1, Hv (r): Vickers hardness, r: distance from center
請求項1に記載の化学成分に加えて、質量%で、Mo:0.10~0.30%、Nb:0.02~0.07%を含有し、残部Feおよび不可避不純物からなり、浸炭焼入れ・焼戻し状態における鋼部品の、表面硬さが650Hv以上、芯部硬さが450Hv以上、全硬化層の深さが1.0~2.6mm、かつ下記式で表される断面平均硬さが550Hv以上、表面の結晶粒度番号が7.0以上、表面のC濃度が0.60~1.00%であることを特徴とする鋼部品。
Figure 2023002842000010
a:捩り試験片1の半径、Hv(r):ビッカース硬さ、r:中心からの距離
In addition to the chemical components described in claim 1, it contains Mo: 0.10 to 0.30% and Nb: 0.02 to 0.07% in mass%, and the balance is Fe and unavoidable impurities, carburizing The steel part in the quenched/tempered state has a surface hardness of 650 Hv or more, a core hardness of 450 Hv or more, a depth of the hardened layer of 1.0 to 2.6 mm, and an average cross-sectional hardness represented by the following formula. is 550 Hv or more, the surface grain size number is 7.0 or more, and the surface C concentration is 0.60 to 1.00%.
Figure 2023002842000010
a: radius of torsion test piece 1, Hv (r): Vickers hardness, r: distance from center
請求項1または請求項2の化学成分に加えて、質量%で、Ti:0.010~0.050%、B:0.0003~0.0030%を含有し、残部Feおよび不可避不純物からなり、浸炭焼入れ・焼戻し状態における鋼部品の、表面硬さが650Hv以上、芯部硬さが450Hv以上、全硬化層の深さが1.0~2.6mm、かつ下記式で表される断面平均硬さが550Hv以上、表面の結晶粒度番号が7.0以上、表面のC濃度が0.60~1.00%であることを特徴とする鋼部品。
Figure 2023002842000011
a:捩り試験片1の半径、Hv(r):ビッカース硬さ、r:中心からの距離
In addition to the chemical components of claim 1 or claim 2, it contains Ti: 0.010 to 0.050%, B: 0.0003 to 0.0030%, and the balance is Fe and unavoidable impurities. , The surface hardness of the steel part in the carburized, quenched and tempered state is 650 Hv or more, the core hardness is 450 Hv or more, the depth of the entire hardened layer is 1.0 to 2.6 mm, and the cross-sectional average represented by the following formula A steel part having a hardness of 550 Hv or more, a surface grain size number of 7.0 or more, and a surface C concentration of 0.60 to 1.00%.
Figure 2023002842000011
a: radius of torsion test piece 1, Hv (r): Vickers hardness, r: distance from center
浸炭焼入れ・焼戻しされた状態の自動車用機械部品にショットピーニング層を有し、このショットピーニング層の表面硬さが700Hv以上、かつ表面の圧縮残留応力が1000MPa以上の値を有していることを特徴とする請求項1~3のいずれか1項に記載の鋼部品。 A carburized, quenched and tempered automobile mechanical part has a shot peening layer, and the shot peening layer has a surface hardness of 700 Hv or more and a surface compressive residual stress of 1000 MPa or more. Steel component according to any one of the preceding claims.
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