JP2021509269A - アルカロイドを含有する材料の調製のための方法、およびこの方法から調製された構成成分を含むエアロゾル形成物品 - Google Patents
アルカロイドを含有する材料の調製のための方法、およびこの方法から調製された構成成分を含むエアロゾル形成物品 Download PDFInfo
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Images
Classifications
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- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
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- A24C5/01—Making cigarettes for simulated smoking devices
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- A—HUMAN NECESSITIES
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- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
- A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
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- A24C5/14—Machines of the continuous-rod type
- A24C5/18—Forming the rod
- A24C5/1821—Forming the rod containing different tobacco mixtures, e.g. composite rods
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
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- A24C5/14—Machines of the continuous-rod type
- A24C5/18—Forming the rod
- A24C5/1864—Conditioning means, e.g. drying
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
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- A24C5/14—Machines of the continuous-rod type
- A24C5/18—Forming the rod
- A24C5/1892—Forming the rod with additives, e.g. binding agent, flavorants
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/022—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the choice of material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/88—Thermal treatment of the stream of extruded material, e.g. cooling
- B29C48/911—Cooling
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
Description
Claims (25)
- アルカロイドを含有する材料の調製のための方法であって、
−還元糖と、アルカロイドを含有する材料の粒子とを含む混合物を形成すること、および
−前記混合物を押出成形することであって、押出成形することが、
−前記混合物を押出成形機に供給することと、
−前記混合物を、摂氏約190度以下の第一の温度に加熱することと、
−前記混合物を、前記第一の温度から摂氏約70度以下の第二の温度に冷却することと、
−押出成形された混合物を前記押出成形機から排出することと、を含む押出成形すること、を含む方法。 - 前記押出成形する工程前の前記混合物が、前記混合物の乾燥重量基準で重量当たり約2パーセント〜約30パーセントの還元糖を含む、請求項1に記載の方法。
- 前記還元糖が、グルコース、フルクトース、キシロース、リボース、ガラクトース、およびこれらの混合物から選択される、請求項1〜2のいずれか一項に記載の方法。
- 前記混合物が、前記押出成形する工程の前に重量当たり約2パーセント〜約30パーセントの含水量を有する、請求項1〜3のいずれか一項に記載の方法。
- 前記第一の温度が摂氏約90度〜摂氏約190度である、請求項1〜4のいずれか一項に記載の方法。
- 前記第二の温度が摂氏約30度〜摂氏約70度である、請求項1〜5のいずれか一項に記載の方法。
- 前記混合物が、約10秒〜約80秒から成る前記押出成形機内の滞留時間を有する、請求項1〜6のいずれか一項に記載の方法。
- 加熱が前記押出成形機の第一部内で実施され、また冷却が前記押出成形機の第二部で実施され、前記押出成形機の前記第二部が、押出成形の方向で前記押出成形機の前記第一部の下流にある、請求項1〜7のいずれか一項に記載の方法。
- 前記混合物が、約2秒〜約60秒から成る前記押出成形機の前記第一部内の滞留時間を有する、請求項8に記載の方法。
- 前記混合物が、約2秒〜約60秒から成る前記押出成形機の前記第二部内の滞留時間を有する、請求項8または9に記載の方法。
- 前記押出成形プロセスが、前記混合物を冷却する前記工程の前に約2秒〜約55秒の滞留時間の間、前記混合物を前記第一の温度に保つことを含む、請求項1〜10のいずれか一項に記載の方法。
- 押出成形が、前記混合物のキログラム当たり約150ワット時〜約350ワットワット時の機械的エネルギーを加えることによって実施される、請求項1〜11のいずれか一項に記載の方法。
- −スラリーを形成するために、アルカロイドを含有する前記材料を結合剤と組み合わせることと、
−スラリーを均質化することと、
−スラリーをキャスティングすることと、を含む請求項1〜12のいずれか一項に記載の方法。 - アルカロイドを含有する材料の調製のための方法であって、
−アルカロイドを含有する材料の粒子と還元糖との混合物を形成すること、および
−前記混合物を押出成形することであって、押出成形することが、
−前記混合物を押出成形機に供給することと、
−前記混合物を第一の温度に加熱することと、
−前記混合物を、前記第一の温度より低い第二の温度に冷却することと、
−前記第二の温度にて前記押出成形機から前記混合物を排出することと、を含む押出成形すること、を含み、
前記冷却が、約2秒〜約60秒から成る時間で実施される、方法。 - 押出成形する前記工程前の前記混合物が、前記混合物の乾燥重量基準で重量当たり約2パーセント〜約30パーセントの還元糖を含む、請求項14に記載の方法。
- 前記還元糖がグルコース、フルクトース、キシロース、リボース、ガラクトース、およびこれらの混合物から選択される、請求項14または15に記載の方法。
- 前記混合物が、押出成形する前記工程の前に重量当たり約2パーセント〜約30パーセントの含水量を有する、請求項14〜16のいずれか一項に記載の方法。
- 前記第一の温度が摂氏約190度以下である、請求項14〜17のいずれか一項に記載の方法。
- 前記第二の温度が摂氏約70度以下である、請求項14〜18のいずれか一項に記載の方法。
- 前記混合物が、約10秒〜約80秒から成る前記押出成形機内の滞留時間を有する、請求項14〜19のいずれか一項に記載の方法。
- 加熱が前記押出成形機の第一部で実施され、かつ冷却が前記押出成形機の第二部で実施され、前記押出成形機の前記第二部が、押出成形の方向で前記押出成形機の前記第一部の下流にある、請求項14〜20のいずれか一項に記載の方法。
- 前記押出成形プロセスが、前記混合物を冷却する前記工程の前に約2秒〜約55秒の滞留時間の間、前記混合物を前記第一の温度に保つことを含む、請求項14〜21のいずれか一項に記載の方法。
- 押出成形が、前記混合物のキログラム当たり約150ワット時〜約350ワット時の機械的エネルギーを加えることによって実施される、請求項14〜22のいずれか一項に記載の方法。
- スラリーを形成するために、アルカロイドを含有する前記材料を結合剤と組み合わせることと、
−前記スラリーを均質化することと、
−前記スラリーをキャスティングすることと、を含む、請求項14〜23のいずれか一項に記載の方法。 - 請求項1〜13の方法から、または請求項14〜24の方法から調製される構成成分を含むエアロゾル形成物品。
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EP17211110 | 2017-12-29 | ||
EP17211110.6 | 2017-12-29 | ||
PCT/EP2018/084646 WO2019129494A1 (en) | 2017-12-29 | 2018-12-12 | Method for the preparation of a material containing alkaloids and aerosol forming article comprising a component prepared from it |
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CN (1) | CN111556715B (ja) |
BR (1) | BR112020012923A2 (ja) |
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US20230049209A1 (en) * | 2019-10-11 | 2023-02-16 | Ccobato (Shenzhen) Technology Ltd | Heat-not-burn aerosol-generating article, product and manufacturing method thereof |
KR20230102372A (ko) * | 2021-12-30 | 2023-07-07 | 주식회사 케이티앤지 | 유효 성분 이행량 증진을 위한 기체 발산 매질 제조 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3098492A (en) * | 1960-11-25 | 1963-07-23 | Nat Starch Chem Corp | Method of making tobacco product |
US3203432A (en) * | 1962-05-03 | 1965-08-31 | Brown & Williamson Tobacco | Production of tobacco smoking materials |
JPH01231884A (ja) * | 1988-01-22 | 1989-09-18 | R J Reynolds Tobacco Co | 押出タバコ物質 |
WO2017041920A1 (en) * | 2015-09-08 | 2017-03-16 | Philip Morris Products S.A. | Method of producing high tensile strength homogenized tobacco material |
JP2017518755A (ja) * | 2014-06-24 | 2017-07-13 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | 再構成たばこシートおよび関連する方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB8704197D0 (en) * | 1987-02-23 | 1987-04-01 | British American Tobacco Co | Tobacco reconstitution |
GB9126828D0 (en) * | 1991-12-18 | 1992-02-19 | British American Tobacco Co | Improvements relating to smoking articles |
CN103315378B (zh) * | 2013-06-28 | 2015-06-17 | 湖北中烟工业有限责任公司 | 提高造纸法再造烟叶抗张强度和感官品质的方法 |
CN105578906B (zh) * | 2013-10-14 | 2019-05-21 | 菲利普莫里斯生产公司 | 包含改良条的加热式气溶胶生成制品 |
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- 2018-12-12 KR KR1020207018362A patent/KR20200101365A/ko not_active Application Discontinuation
- 2018-12-12 ES ES18814940T patent/ES2885182T3/es active Active
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Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3098492A (en) * | 1960-11-25 | 1963-07-23 | Nat Starch Chem Corp | Method of making tobacco product |
US3203432A (en) * | 1962-05-03 | 1965-08-31 | Brown & Williamson Tobacco | Production of tobacco smoking materials |
JPH01231884A (ja) * | 1988-01-22 | 1989-09-18 | R J Reynolds Tobacco Co | 押出タバコ物質 |
JP2017518755A (ja) * | 2014-06-24 | 2017-07-13 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | 再構成たばこシートおよび関連する方法 |
WO2017041920A1 (en) * | 2015-09-08 | 2017-03-16 | Philip Morris Products S.A. | Method of producing high tensile strength homogenized tobacco material |
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US20210022386A1 (en) | 2021-01-28 |
EP3731660B1 (en) | 2021-07-21 |
CN111556715B (zh) | 2022-11-18 |
RU2020120708A (ru) | 2022-01-31 |
HUE055363T2 (hu) | 2021-11-29 |
EP3731660A1 (en) | 2020-11-04 |
JP7288444B2 (ja) | 2023-06-07 |
RU2020120708A3 (ja) | 2022-01-31 |
BR112020012923A2 (pt) | 2020-12-01 |
KR20200101365A (ko) | 2020-08-27 |
PL3731660T3 (pl) | 2021-12-13 |
CN111556715A (zh) | 2020-08-18 |
WO2019129494A1 (en) | 2019-07-04 |
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