JP2021042129A - 硬質ラノリン脂肪酸のエステル化物を含有する化粧料 - Google Patents
硬質ラノリン脂肪酸のエステル化物を含有する化粧料 Download PDFInfo
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- JP2021042129A JP2021042129A JP2019162549A JP2019162549A JP2021042129A JP 2021042129 A JP2021042129 A JP 2021042129A JP 2019162549 A JP2019162549 A JP 2019162549A JP 2019162549 A JP2019162549 A JP 2019162549A JP 2021042129 A JP2021042129 A JP 2021042129A
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- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019166 vitamin D Nutrition 0.000 description 1
- 239000011710 vitamin D Substances 0.000 description 1
- 150000003710 vitamin D derivatives Chemical class 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
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- 235000020234 walnut Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
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Landscapes
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Abstract
Description
に関する。
タイン;ホスファチジルコリン、ホスファチジルエタノールアミン、ホスファチジルセリン、スフィンゴミエリン等のスフィンゴリン脂質、リゾレシチン、水素添加大豆リン脂質、部分水素添加大豆リン脂質、水素添加卵黄リン脂質、部分水素添加卵黄リン脂質、水酸化レシチン等のリン脂質類;シリコーン系両性界面活性剤等;高分子界面活性剤では、ポリビニルアルコール、アルギン酸ナトリウム、デンプン誘導体、トラガントガム、アクリル酸・メタアクリル酸アルキル共重合体;シリコーン系各種界面活性剤が好ましいものとして挙げられる。
化粧料、ボディ化粧料、軟膏等の皮膚外用剤等が挙げられる。本発明の効果を発揮させる
観点から、特に毛髪化粧料、皮膚化粧料、メイクアップ化粧料に好ましく使用することができる。本発明の化粧料は、通常の方法に従って製造することができる。
プー、クリームシャンプー、コンディショニングシャンプー、ふけ用シャンプー、ヘアカ
ラー用シャンプー、リンス一体型シャンプー等のシャンプー; リンス、トリートメント、
ヘアパック、ヘアミスト等のコンディショナー; ヘアフォーム、ヘアムース、ヘアスプレ
ー、ヘアワックス、ヘアジェル、ヘアクリーム、ウォーターグリース、セットローション
、ポマード、チック等の整髪料; カラーローション、ヘアトニック、ヘアリキッド、ヘア
ブロー、枝毛コート、ヘアオイル、パーマネントウェーブ用剤、ストレートパーマ剤、酸
化染毛剤、ヘアブリーチ、ヘアカラープレトリートメント、ヘアカラーアフタートリート
メント、パーマプレトリートメント、パーマアフタートリートメント、ヘアマニキュア、
育毛剤が好ましいものとして挙げられる。
攪拌機、温度計、ガス導入管を備えた500mLの反応器に、硬質ラノリン脂肪酸(ラノリン脂肪酸SH、日本精化社製)250g(0.47モル)およびエチレングリコール29g(0.47モル)、50%リン酸水溶液0.5gを仕込み、窒素気流中140℃まで加熱した後、5時間かけて190〜210℃まで加熱し、生成する水を除去しながら5時間エステル化反応を行った。その後、MEKで希釈し、脱酸、水洗、脱溶媒、水蒸気脱臭を行い、目的の硬質ラノリン脂肪酸のエステル化物をワックス状物として得た。
エチレングリコールの仕込み量を29gから14gへ変更した以外は、合成例1と同様にエステル化反応を行い、目的の硬質ラノリン脂肪酸のエステル化物をワックス状物として得た。
エチレングリコール29gを、エチレングリコール29gとポリエチレングリコール(平均分子量200)1gに変更した以外は、合成例1と同様にエステル化反応を行い、目的の硬質ラノリン脂肪酸のエステル化物をワックス状物として得た。
エチレングリコール29gを、ペンタエリスリトール31gに変更した以外は、合成例1と同様にエステル化反応を行い、目的の硬質ラノリン脂肪酸のエステル化物をワックス状物として得た。
エチレングリコール29gを、ベヘニルアルコール153gに変更した以外は、合成例1と同様にエステル化反応を行い、目的の硬質ラノリン脂肪酸のエステル化物をワックス状物として得た。
硬質ラノリン脂肪酸をラノリン脂肪酸(ラノリン脂肪酸W、日本精化社製)に変更した以外は、合成例1と同様にエステル化反応を行い、目的のラノリン脂肪酸のエステル化物を若干軟性のある固形状物として得た。
本発明の合成例1〜5の硬質ラノリン脂肪酸のエステル化物を用いて、表1に記載の組成でヘアワックス(実施例1〜5)を作製した。比較として、比較合成例1のエステル化物を配合したヘアワックス(比較例1)、カルナウバロウを配合したヘアワックス(比較例2)、キャンデリラロウを配合したヘアワックス(比較例3)を作製した。得られたヘアワックスについて、以下の方法で使用感及び毛髪セット力を評価した。結果は表1に併記した。
<使用感評価方法>
健常黒髪人毛の毛束(長さ25cm、1g)に各ヘアワックス0.06gを塗布し、塗布時の使用感を官能にて下記の基準で評価した。
◎:非常に良い、○:良い、△:やや良くない、×:良くない
<毛髪セット力評価方法>
上記の使用感評価で得られたヘアワックスを塗布した毛束を、20回櫛を通した後、棒状になるように整えた。この毛束を垂直に立つように片端を地面に固定し、温度20℃、湿度45%の条件で3時間放置した後、毛束の形状維持状態を目視で観察し、下記の基準で毛髪セット力を評価した。
◎:非常に良い、○:良い、△:やや良くない、×:良くない
本発明の合成例1〜5の硬質ラノリン脂肪酸のエステル化物を用いて、表2に記載の組成でクリーム(実施例6〜10)を作製した。比較として、比較合成例1のエステル化物を配合したクリーム(比較例4)、カルナウバロウを配合したクリーム(比較例5)、キャンデリラロウを配合したクリーム(比較例6)を作製した。得られたクリームについて、以下の方法で使用感(コク、肌なじみ、乾燥後のしっとり感)を評価した。結果は表2に併記した。
<評価方法>
上腕内側部に各クリームを一定量塗布し、コク、肌なじみ、乾燥後のしっとり感を官能にて下記の基準で評価した。
◎:非常に良い、○:良い、△:やや良くない、×:良くない
本発明の合成例1〜5の硬質ラノリン脂肪酸のエステル化物を用いて、表3に記載の組成で口紅(実施例11〜15)を作製した。比較として、比較合成例1のエステル化物を配合した口紅(比較例7)、カルナウバロウを配合した口紅(比較例8)、キャンデリラロウを配合した口紅(比較例9)を作製した。得られた口紅について、以下の方法で使用感(つや、しっとり感)を評価した。結果は表3に併記した。
<使用感評価方法>
各口紅を唇に一定量塗布し、塗布後の使用感(つや、しっとり感)を官能にて下記の基準で評価した。
◎:非常に良い、○:良い、△:やや良くない、×:良くない
本発明の合成例1〜5の硬質ラノリン脂肪酸のエステル化物を用いて、表4に記載の組成でヘアコンディショナー(実施例16〜20)を作製した。比較として、比較合成例1のエステル化物を配合したヘアコンディショナー(比較例10)、カルナウバロウを配合したヘアコンディショナー(比較例11)、キャンデリラロウを配合したヘアコンディショナー(比較例12)を作製した。得られたヘアコンディショナーについて、以下の方法で使用感を評価した。結果は表4に併記した。
<使用感評価方法>
健常黒髪人毛に2剤式ブリーチ剤にてブリーチ処理を1回行い、損傷した毛束5gを作製した。作製した毛束に各ヘアコンディショナー0.5gを塗布し、2分間放置後、流水下で30秒間すすぎ流し、ドライヤーで乾燥した。得られた毛束について、使用感(ダメージ感の低減、滑らかさ、しっとり感)を官能にて下記の基準で評価した。
◎:非常に良い、○:良い、△:やや良くない、×:良くない
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 8.0
Plandool−ISS(日本精化) 1.0
トリエチルヘキサノイン(日本精化) 1.0
Plandool−G(日本精化) 9.0
トリ水添ロジングリセリル 1.0
PPG−1ベヘネス−15 5.0
ポリウレタン−1 2.0
コレステロール 0.5
セバシン酸ジエチル 2.0
セテス−7 1.0
ジメチコン 3.0
アジピン酸ジイソプロピル(日本精化) 5.0
B部
グリセリン 5.0
フェノキシエタノール 0.6
メチルパラベン 0.2
精製水 合計で100となる量
C部
(アクリレーツ/メタクリル酸ステアレス−20)コポリマー 3.0
精製水 20.0
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。A部にB部を攪拌しながら徐々に加え、均一に混合した後、冷却した(D部)。D部にC部を加え均一に混合した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 13.0
Plandool−SUN(日本精化) 2.0
LUSPLAN DD−DA7(日本精化) 2.7
トリ水添ロジングリセリル 0.3
Plandool−DP(日本精化) 5.0
トリエチルヘキサノイン(日本精化) 3.0
PEG−40水添ヒマシ油 1.0
ステアレス−30 1.0
エルカラクトンMCT(日本精化) 1.0
(アクリル酸アルキル/ジアセトンアクリルアミド)コポリマーAMP 1.0
コメヌカロウ 2.0
ヒドロキシステアリン酸 6.0
ステアリン酸グリセリル 1.0
ジメチコン 3.0
セバシン酸ジイソプロピル(日本精化) 5.0
セテス−2 0.5
セテス−20 2.5
BHT 0.05
フェノキシエタノール 0.6
メチルパラベン 0.2
B部
BG 3.0
水酸化Na 0.5
(アクリレーツ/アクリル酸アルキル(C10−30))クロスポリマー 0.1
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。A部にB部を攪拌しながら徐々に加え、均一に混合した後、冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1のエステル化物 13.0
Plandool−ISS(日本精化) 1.0
Plandool−G(日本精化) 2.7
トリ水添ロジングリセリル 0.3
ジメチコン 6cs 10.0
Ecolano DP−50(日本精化) 0.5
ホホバ種子油 4.0
ステアリン酸グリセリル 2.0
セテス−10 2.0
トコフェロール 0.05
パラフィンワックス 2.0
PEG−20水添ヒマシ油 1.3
ミツロウ 1.5
メトキシケイヒ酸エチルヘキシル 1.8
PEG−90M 3.0
B部
フェノキシエタノール 0.6
メチルパラベン 0.15
PG 3.0
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。A部にB部を攪拌しながら徐々に加え、均一に混合した後、冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 6.0
LUSPLAN DD−IS(日本精化) 2.5
パルミチン酸セチル 2.5
ジメチコン 100cs 8.0
オリーブ油 2.0
スクワラン 3.0
テオプロマグランジフロルム種子脂 0.3
ステアリン酸 2.0
ステアリン酸グリセリル 0.8
セテス−7 1.0
トコフェロール 0.05
マイクロクリスタリンワックス 2.0
コメヌカロウ 2.5
PEG−40水添ヒマシ油 1.3
セテス−20 1.5
ミツロウ 1.5
B部
フェノキシエタノール 0.4
メチルパラベン 0.15
カルボマー 0.1
EDTA−4Na 0.05
TEA 0.2
PG 3.0
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。A部にB部を攪拌しながら徐々に加え、均一に混合した後、冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 6.0
脂肪酸(C18−35)グリコール 6.0
ジオレイン酸PEG−120メチルグルコース 5.0
ラノリン脂肪酸オクチルドデシル 5.0
ステアリン酸 4.0
LUSPLAN DD−DHR(日本精化) 2.7
カルナウバロウ 3.0
セバシン酸ジエチル 2.0
エルカラクトンDES 2.0
ジメチコン(10万cs) 1.0
シクロペンタシロキサン 1.0
セテス−2 2.0
セテス−7 2.0
セテス−20 1.0
ジココジモニウムクロリド(75%) 1.0
プロピルパラベン 0.1
B部
トリエタノールアミン 0.3
メチルパラベン 0.2
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、溶解させた。別容器にB部をとり、約80℃に加温し均一に溶解させた(B部)。A部にB部を徐々に加え、均一に混合した。室温まで冷却した後、pHを調整した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 4.0
Plandool−G(日本精化) 2.7
ミリスチン酸オクチルドデシル 6.0
ナタネ油 5.0
スクワラン 5.0
ステアリン酸 2.0
ミツロウ 3.0
LUSPLAN SR−DM4(日本精化) 2.0
PEG−60水添ヒマシ油 1.0
ステアリン酸グリセリル(SE) 1.0
ラウロイルリシン 0.5
セテス−7 2.0
カプリン酸グリセリル 1.0
B部
トリエタノールアミン 0.3
プロパンジオール 5.0
ペンチレングリコール 3.0
へキシレングリコール 0.8
Neosolue−AquaS(日本精化) 0.4
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、溶解させた。別容器にB部をとり、約80℃に加温し均一に溶解させた(B部)。A部にB部を徐々に加え、均一に混合した。室温まで冷却した後、pHを調整した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 9.0
ハードラノリン 6.0
水添ポリイソブテン 6.0
エチルヘキサン酸セチル(日本精化) 5.0
マイクロクリスタリンワックス 5.0
ヒドロキシステアリン酸 3.0
セタノール 2.0
トコフェロール 0.05
シリカ 1.0
ポリアクリル酸メチル 0.5
エチルヘキシルトリアゾン 2.0
ステアレス−20 1.0
プロピルパラベン 0.1
B部
水酸化Na 0.8
メチルパラベン 0.20
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、溶解させた。別容器にB部をとり、約80℃に加温し均一に溶解させた。A部にB部を徐々に加え、均一に混合した。室温まで冷却した後、pHを調整した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例2のエステル化物 4.0
リンゴ酸ジイソステアリル 合計で100となる量
イソノナン酸イソトリデシル 3.0
テトライソステアリン酸ペンタエリスリチル 3.0
Plandool−S(日本精化) 0.2
トリオクタノイン(日本精化) 6.0
テトラエチルヘキサン酸アスコルビル 2.0
ポリエチレン 5.0
トリイソステアリン酸ポリグリセリル−2 0.5
ジメチコン 2.0
グリチルレチン酸ステアリル 0.05
フェノキシエタノール 0.6
酸化チタン 0.5
マイクロクリスタリンワックス 0.8
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
全成分を約80℃に加温し、均一に混合した後、室温まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例4のエステル化物 10.0
ミツロウ 3.0
酢酸セルロース 2.0
パルミチン酸エチルヘキシル 5.0
エチルヘキサン酸セチル 2.0
ワセリン 1.5
ミネラルオイル 2.0
ステアリン酸 1.0
ステアリルアルコール 1.0
セテス−20 2.0
ステアリン酸ソルビタン 2.0
ポリソルベート60 1.0
ジステアリン酸PEG−250 1.0
タルク 1.0
B部
カルボキシビニルポリマー 0.1
ビニルピロリドン−N,N−ジメチルアミノエチルメタクリル酸
共重合体ジエチル硫酸塩 0.1
精製水 10.0
C部
ポリエチレングリコール 1.0
ジグリセリン 1.0
グリセリン 2.0
カプリリルグリコール 0.5
トリエタノールアミン 0.2
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を80℃で攪拌しながら均一に混合した。別容器にB部をとり、粘性の液とした。別容器にC部をとり、均一に溶解させた。80℃でA部にC部を攪拌しながら加え、乳化した。乳化後、約50℃まで冷却したのち、B部を混合し均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例5のエステル化物 8.0
ヒマワリ種子ロウ 3.0
酢酸セルロース 2.0
パルミチン酸エチルヘキシル 5.0
イソノナン酸イソノニル 2.0
ミリスチン酸イソプロピル 2.0
ワセリン 1.5
スクワラン 2.0
ヒドロキシステアリン酸 1.0
ミリスチルアルコール 1.0
セテス−20 2.0
ステアリン酸ソルビタン 2.0
PEG−60水添ヒマシ油 1.0
ジステアリン酸PEG−250 1.0
エチルヘキシルグリセリン 0.5
B部
カルボキシビニルポリマー 0.1
ビニルピロリドン−N,N−ジメチルアミノエチルメタクリル酸
共重合体ジエチル硫酸塩 0.1
Tremoist−TP(日本精化) 0.1
精製水 10.0
C部
ポリエチレングリコール 1.0
BG 5.0
グリセリン 2.0
カプリリルグリコール 0.5
トリエタノールアミン 0.2
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を80℃で攪拌しながら均一に混合した。別容器にB部をとり、粘性の液とした。別容器にC部をとり、均一に溶解させた。80℃でA部にC部を攪拌しながら加え、乳化した。乳化後、約50℃まで冷却したのち、B部を混合し均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例3のエステル化物 10.0
ミツロウ 3.0
マイクロクリスタリンワックス 2.0
エチルヘキサン酸セチル 5.0
シクロペンタシロキサン 8.0
ジメチコン 1.5
ミネラルオイル 2.0
ステアリン酸 1.0
ステアリルアルコール 1.0
セテス−20 2.0
ステアリン酸グリセリル 2.0
ポリソルベート−60 1.0
ジラウロイルグルタミン酸リシンNa 0.3
結晶性セルロース 1.0
B部
カルボキシビニルポリマー 0.1
アクリル酸/アクリル酸アルキル(C10-30)コポリマー 0.1
精製水 10.0
C部
ポリエチレングリコール 1.0
エタノール 5.0
グリセリン 2.0
デキストリン 0.2
カプリリルグリコール 0.5
加水分解ダイズタンパク 0.2
トリエタノールアミン 0.2
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を80℃で攪拌しながら均一に混合した。別容器にB部をとり、粘性の液とした。別容器にC部をとり、均一に溶解させた。80℃でA部にC部を攪拌しながら加え、乳化した。乳化後、約50℃まで冷却したのち、B部を混合し均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 8.0
Ecolano MAC(日本精化) 1.0
ポリエチレン 3.0
パラフィン 3.0
マイクロクリスタリンワックス 2.0
ミツロウ 2.0
コメヌカロウ 2.0
インドデカン 5.0
ミネラルオイル 5.0
パルミチン酸エチルヘキシル 3.0
ドデカン 2.0
ジメチコン 1.0
ステアリン酸 2.0
セテス−10 2.0
セテス−15 3.0
セテス−6 2.0
ステアリン酸グリセリル(SE) 2.0
B部
イヌリン(日本精化) 0.5
ヒドロキシエチルセルロース 0.1
(アクリレーツ/アクリル酸アルキル(C1−18)/アルキル(C1−8)
アクリルアミド)コポリマーAMP 0.1
精製水 10.0
C部
BG 3.0
エタノール 5.0
EDTA−2Na 0.02
フェノキシエタノール 0.25
メチルパラベン 0.05
水酸化Na 0.25
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を80℃で攪拌しながら均一に混合した。別容器にB部をとり、粘性の液とした。別容器にC部をとり、均一に溶解させた。80℃でA部にC部を攪拌しながら加え、乳化した。乳化後、約50℃まで冷却したのち、B部を混合し均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 4.0
フィッシャートロプシュワックス 1.0
セテアリルアルコール 1.0
Ecolano DP−50(日本精化) 0.5
PPG−1ベヘネス−15 6.0
ラウロアンホ酢酸Na 3.0
ラウレス−7クエン酸 2.0
ポリオキシエチレン(60)フィトステロール 1.0
B部
ポリウレタン−14アクリレーツコポリマーAMP 0.1
アクリレーツ/メタクリル酸ステアレス−20クロスポリマー 0.1
(ビニルピロリドン/VA)コポリマー 0.1
酢酸ビニル・ビニルピロリドン共重合体 0.05
(アクリル酸Na/アクリロイルジメチルタウリンNa)コポリマー0.05
ヒドロキシエチルセルロース 0.05
キサンタンガム 0.05
精製水 10.0
C部
BG 8.0
エタノール 5.0
Neosolue−Aqulio(日本精化) 1.0
Phytopresome MEL(日本精化) 1.0
イソステアロイル加水分解シルク 0.1
水酸化Na 0.3
フェノキシエタノール 0.2
メチルパラベン 0.05
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を80℃で攪拌しながら均一に混合した。別容器にB部をとり、粘性の液とした。別容器にC部をとり、均一に溶解させた。80℃でA部にC部を攪拌しながら加え、乳化した。乳化後、約50℃まで冷却したのち、B部を混合し均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 4.0
セテアリルアルコール 1.0
コハク酸ジエチルヘキシル(日本精化) 2.0
Neosolue−DiSM(日本精化) 2.0
ステアリン酸グリセリル 2.0
ポリオキシエチレン(60)フィトステロール 1.0
ポリソルベート−60 6.0
B部
ポリウレタン−14アクリレーツコポリマーAMP 0.1
アクリレーツ/メタクリル酸ステアレス−20クロスポリマー 0.1
(ビニルピロリドン/VA)コポリマー 0.1
酢酸ビニル・ビニルピロリドン共重合体 0.05
(アクリル酸Na/アクリロイルジメチルタウリンNa)コポリマー0.05
(アクリル酸アルキル/ジアセトンアクリルアミド)コポリマーAMP 0.1
ヒドロキシエチルセルロース 0.05
キサンタンガム 0.05
精製水 10.0
C部
BG 8.0
エタノール 5.0
Neosolue−Aqulio(日本精化) 2.0
イソステアロイル加水分解シルク 0.1
水酸化Na 0.3
フェノキシエタノール 0.2
メチルパラベン 0.05
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を80℃で攪拌しながら均一に混合した。別容器にB部をとり、粘性の液とした。別容器にC部をとり、均一に溶解させた。80℃でA部にC部を攪拌しながら加え、乳化した。乳化後、約50℃まで冷却したのち、B部を混合し均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 1.0
LUSPLAN SR−DM4(日本精化) 1.0
ステアリルアルコール 1.7
エチルヘキサン酸セチル(日本精化) 1.2
ステアラミドプロピルジメチルアミン 1.0
Plandool−H(日本精化) 0.2
Plandool−DP(日本精化) 0.2
ハードラノリン 1.0
ステアリン酸グリセリル 0.3
Ecolano DC−30(日本精化) 0.5
PEG−25水添ヒマシ油 1.0
セテス−20 0.3
B部
イヌリン(日本精化) 0.5
乳酸 0.4
精製水 合計で100となる量
C部
ヒドロキシエチルセルロース 0.4
BG 2.0
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部を約80℃でそれぞれ混合した。B部をA部に加え乳化し、約60℃に冷却後、C部を添加した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 0.2
パルミチン酸イソプロピル(日本精化) 0.2
セバシン酸ジエチルヘキシル(日本精化) 1.0
オレイン酸 0.2
B部
ラウレス硫酸アンモニウム 5.0
ラウレス硫酸Na(25%) 10.0
ココイルグルタミン酸TEA(30%) 3.0
ラウリルヒドロキシスルタイン(30%) 7.0
ラウリン酸K 1.0
ジステアリン酸グリコール 0.5
ステアロキシプロピルジメチルアミン 0.5
PPG−17 0.3
ジエチルヘキサン酸ネオペンチルグリコール 0.4
ラノリン脂肪酸 0.3
イソデシルグリセリルエーテル 0.4
コカミドMEA 1.0
ラウレス−4 0.3
ラウレス−16 0.2
ステアレス−6 0.2
硝酸ミコナゾール 0.75
フェノキシエタノール 0.3
C部
ソルビトール 1.6
メチルパラベン 0.2
EDTA−2Na 0.05
リン酸 0.03
安息香酸Na 0.3
精製水 合計で100となる量
D部
ポリクオタニウム−10 0.2
グアーヒドロキシプロピルトリモニウムクロリド 0.1
Tremoist−TP(日本精化) 0.02
精製水 6.7
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
あらかじめ混合しておいたA部と、B部を約80℃で均一に混合した(E部)。別にとっておいたC部を約60℃に加温、均一にした。E部にC部を攪拌しながら徐々に加え、均一に混合した後、約50℃まで冷却した。さらにD部を加え均一に混合した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 2.0
ラノリン脂肪酸 0.1
イソステアリン酸 0.1
スルホコハク酸ラウレス2Na(26%) 10.0
ラウロアンホ酢酸Na(30%) 7.0
ラウリル硫酸TEA(40%) 6.0
ラウレス−2 1.0
ジオレイン酸PEG−120メチルグルコース 1.0
テトラオレイン酸ソルベス−60 3.5
カプリリルグルコシド 0.3
ジステアリン酸グリコール 0.5
PEG−2コカミン 1.2
PEG−60水添ヒマシ油 0.5
ジヘプタン酸ネオペンチルグリコール 0.3
オレイン酸グリセリル 0.8
フェノキシエタノール 0.3
B部
EDTA−2Na 0.05
メチルパラベン 0.15
精製水 合計で100となる量
C部
ポリクオタニウム−10 0.1
グアーヒドロキシプロピルトリモニウムクロリド 0.3
塩化Na 0.3
アスコルビン酸 0.3
ヒアルロン酸Na 0.3
精製水 19.3
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
B部を約80℃に加温し均一に溶解させた。別容器にA部をとり、加温し、溶解させた。A部にB部を徐々に加え、均一に混合し、約60℃でC部を加えた。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例4のエステル化物 2.0
イソステアリン酸 0.1
ココイルメチルタウリンNa(30%) 8.0
コカミドプロピルベタイン(30%) 5.0
ラウレス硫酸Na(25%) 6.0
ラウレス−2 1.0
テトラオレイン酸ソルベス−60 3.5
カプリリルグルコシド 0.3
コカミドDEA 3.0
PEG−20水添ヒマシ油 0.5
ジヘプタン酸ネオペンチルグリコール 0.3
オレイン酸エチル 0.3
B部
EDTA−2Na 0.05
メチルパラベン 0.15
プロパンジオール 0.5
精製水 合計で100となる量
C部
ポリクオタニウム−10 0.1
グアーヒドロキシプロピルトリモニウムクロリド 0.3
塩化Na 0.3
アスコルビン酸 0.3
スイゼンジノリ多糖体 0.1
精製水 19.3
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
B部を約80℃に加温し均一に溶解させた。別容器にA部をとり、加温し、溶解させた。A部にB部を徐々に加え、均一に混合し、約60℃でC部を加えた。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例2のエステル化物 0.2
Plandool−LG2(日本精化) 0.03
Neosolue−AquaS(日本精化) 0.1
イヌリン(日本精化) 0.5
ラウレス−4カルボン酸Na(28%) 10.0
ラウレス−6カルボン酸 4.0
コカミドプロピルベタイン(30%) 10.0
ラウロイルメチルアラニンNa(30%) 5.0
イソステアリン酸 0.3
コカミドメチルMEA 3.0
水酸化Na 1%液 0.5
ポリクオタニウム−10 0.8
ジステアリン酸グリコール 0.5
ポリクオタニウム−7 0.5
安息香酸Na 0.3
EDTA−2Na 0.05
フェノキシエタノール 0.4
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
全成分を約80℃で加温して均一に攪拌混合した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例4のエステル化物 0.5
Neosolue−Aqulio(日本精化) 0.2
ジメチコン 0.3
エチルへキサン酸セチル 1.0
エルカラクトンMCT(日本精化) 2.0
セテアリルアルコール 3.5
パルミチン酸デキストリン 0.2
PEG−200 0.5
Ecolano DP−50(日本精化) 0.5
ベヘニン酸ジメチルアミノプロピルアミド 0.2
セトリモニウムクロリド(30%) 1.0
ベヘントリモニウムクロリド(80%) 1.0
トリデセス−6 0.3
BHT 0.03
B部
NanoRepair−CMC5(日本精化) 5.0
ヒドロキシエチルセルロース 0.4
Tremoist−TP(日本精化) 0.02
(アクリロイルジメチルタウリンアンモニウム/VP)コポリマー 0.02
BG 1.8
グリセリン 4.0
メチルパラベン 0.2
クエン酸 0.05
精製水 合計で100となる量
C部
イソドデカン 0.2
PPG−3カプリリルエーテル 0.5
パンテノール 0.1
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
B部を約80℃に加温し溶解させた。別容器にA部を加え、加温し、溶解させた。A部にB部を徐々に加え、均一に混合した。約50℃でC部を攪拌しながら添加し、均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1のエステル化物 0.2
ポリクオタニウム−37 2.0
スクワラン 2.0
PPG−3カプリリルエーテル 2.0
Ecolano CA−NH(日本精化) 0.5
マイクロクリスタリンワックス 0.1
ラノリンアルコール 0.2
パラフィンワックス 0.1
ポリエチレンワックス 0.1
ミツロウ 0.1
モクロウ 0.2
セレシン 0.1
ジカプリン酸PG 1.0
コレステロール 0.2
エチルへキサン酸セチル 1.0
キャンデリラロウエキス 0.1
エルカ酸オクチルドデシル 4.5
酢酸トコフェロール 0.02
エルカラクトンMCT(日本精化) 2.0
トリポリヒドロキシステアリン酸ジペンタエリスリチル 1.5
PPG−5フィトステリル 0.5
グリセリン 4.0
ソルビトール 2.0
フェノキシエタノール 0.5
B部
加水分解コンキオリン 0.1
加水分解ケラチン 0.1
パンテノール 0.1
ヒアルロン酸ヒドロキシプロピルトリモニウム 0.01
ポリクオタニウム−11 0.2
グリコシルトレハロース 0.1
グリセリルグルコシド 0.3
アルギニン 0.1
C部
精製水 合計で100となる量
ヒドロキシプロピルデンプンリン酸 1.0
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
C部を均一に分散し、約80℃に加温した。次にA部を約80℃に加温し溶解させた。C部を攪拌しながらA部加え、均一に混合後、約40℃まで冷却させた。次いで、B部を加え、均一に混合した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例5のエステル化物 0.2
Plandool−LG2(日本精化) 0.5
プロパンジオール 3.0
ベヘナミドプロピルジメチルアミン 1.5
セタノール 2.2
ステアリルアルコール 0.8
水添ナタネ油アルコール 0.5
ジエチルヘキサン酸ネオペンチルグリコール 0.8
ホホバ種子油 1.0
ステアリン酸グリセリル 0.4
プロピルパラベン 0.1
コカミドMEA 0.8
ベヘントリモニウムクロリド 0.5
コメヌカワックス 0.5
グリセリン 1.0
B部
NanoRepair−CMC5 1.0
硝酸ミコナゾール 0.2
乳酸 0.4
精製水 合計で100となる量
C部
アモジメチコン 3.0
セバシン酸ジエチルヘキシル(日本精化) 1.0
ポリクオタニウム−7 0.15
ミリスチン酸PPG−3ベンジルエーテル 0.5
D部
Tremoist−TP(日本精化) 0.01
精製水 10.0
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃で均一に混合した。別にとっておいたB部を約60℃に加温、均一にした。A部にB部を攪拌しながら徐々に加え、均一に混合した後、約50℃まで冷却した。さらにC部、D部を加え均一に混合した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1のエステル化物 0.5
ドデカン 1.5
Neosolue−Aqulio(日本精化) 0.2
Neosolue−DiSM(日本精化) 0.2
LUSPLAN SR−DM4(日本精化) 0.5
キャンデリラワックス 0.2
パルミチン酸イソプロピル 1.0
エチルへキサン酸セチル 1.0
セテアリルアルコール 3.5
PEG−200 0.5
ヒドロキシエチルセルロース 0.4
セトリモニウムクロリド(30%) 1.0
ベヘントリモニウムクロリド(80%) 1.0
トリデセス−6 0.3
BHT 0.03
B部
メチルパラベン 0.01
クエン酸 0.05
精製水 合計で100となる量
C部
ジメチコン(400万cs) 1.0
ジメチコン(100cs) 3.0
シクロメチコン 3.0
PPG−3ミリスチル 0.5
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
B部を約80℃に加温し溶解させた。別容器にA部を加え、加温し、溶解させた。A部にB部を徐々に加え、均一に混合した。約50℃でC部を攪拌しながら添加し、均一にした。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1のエステル化物 0.2
LUSPLAN SR−DM4(日本精化) 0.8
Neosolue−DiSM(日本精化) 0.3
Neosolue−MP(日本精化) 0.2
ステアリルアルコール 2.0
セタノール 1.2
ステアルトリモニウムクロリド 1.0
Ecolano CA−NH(日本精化) 0.3
PEG−45M 0.8
Plandool−LG1(日本精化) 0.3
エルカラクトンDES(日本精化) 1.0
トウツバキ種子油 0.4
ヒドロキシエチルウレア 0.5
炭酸ジカプリリル 2.0
PPG−1/PEG−1ステアラミン 1.0
スクワラン 0.1
イソセテス−10 0.5
ヒマワリワックス 0.8
ココイルアルギニンエチルPCA 0.2
フェノキシエタノール 0.2
トコフェロール 0.05
B部
DPG 2.2
グリセリン 1.3
ソルビトール 3.5
BG 1.0
ヒドロキシセルロース 0.07
NanoRepair−EL(日本精化) 1.0
クエン酸 適量
EDTA−2Na 0.01
精製水 合計で100となる量
C部
ポリクオタニウム−61 0.3
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃で均一に混合した。別にとっておいたB部を約60℃に加温、均一にした。A部にB部を攪拌しながら徐々に加え、均一に混合した後、約50℃まで冷却した。さらにC部を加え均一に混合した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1のエステル化物 2.0
Plandool−LG3(日本精化) 2.0
Plandool−H(日本精化) 2.0
Plandool−DP(日本精化) 1.0
Plandool−MAS(日本精化) 1.0
パルミチン酸イソプロピル(日本精化) 5.0
セタノール 1.2
フェニルトリメチコン 3.0
エチルパラベン 0.1
ミリスチン酸イソプロピル(日本精化) 3.0
ミネラルオイル 2.0
水添ポリイソブテン 1.0
B部
ステアロキシヒドロキシプロピルメチルセルロース 0.1
キサンタンガム 0.1
精製水 20.0
C部
Phytocompo−PP(日本精化) 1.0
ペンチレングリコール 3.0
グリセリン 8.0
D部
VCエチル(日本精化) 1.0
アルブチン(日本精化) 1.0
精製水 5.0
E部
フェノキシエタノール 0.2
メチルパラベン 0.15
フィチン酸 0.5
クエン酸 0.1
クエン酸Na pHが4.5になる量
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、E部をそれぞれ約70℃に加温し、均一に溶解させた。B部を攪拌して粘性の液とした。C部を約70℃に加温し、均一に分散させた。C部をホモディスパーにて攪拌しながらA部を加えた後、E部を攪拌しながら添加した。約50℃でD部、B部を加え、攪拌して均一に溶解した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 0.2
Plandool−H(日本精化) 1.0
セバシン酸ジエチルヘキシル(日本精化) 5.0
コハク酸ジエチルヘキシル(日本精化) 5.0
セタノール 1.2
フェニルトリメチコン 3.0
エチルパラベン 0.1
ミリスチルアルコール 2.0
オレイルアルコール 1.0
B部
ステアロキシヒドロキシプロピルメチルセルロース 0.1
キサンタンガム 0.1
精製水 20.0
C部
Phytocompo−PP(日本精化) 1.0
ペンチレングリコール 2.0
1,2−ヘキサンジオール 1.0
BG 5.0
グリセリン 8.0
D部
アルブチン(日本精化) 1.0
トラネキサム酸(日本精化) 1.0
精製水 5.0
E部
亜硫酸Na 0.05
フィチン酸 0.5
クエン酸 0.1
クエン酸Na pHが4.5になる量
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、E部をそれぞれ約70℃に加温し、均一に溶解させた。B部を攪拌して粘性の液とした。C部を約70℃に加温し、均一に分散させた。C部をホモディスパーにて攪拌しながらA部を加えた後、E部を攪拌しながら添加した。約50℃でD部、B部を加え、攪拌して均一に溶解した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
グリセリン 3.0
ジグリセリン 1.0
BG 7.0
Phytocompo−C(日本精化) 1.0
水添リゾリン脂質(日本精化) 0.1
B部
合成例2のエステル化物 1.0
トリオクタノイン(日本精化) 3.0
LUSPLAN SR−DM4(日本精化) 0.5
水添ポリイソブテン 3.5
イソドデカン 1.5
セトステアリルアルコール 1.0
アラキルアルコール 0.1
ホホバアルコール 3.0
キミルアルコール 0.3
セラキルアルコール 0.1
ヘキシルデカノール 0.5
C部
(アクリル酸ヒドロキシエチル/アクリロイルジメチルタウリンNa)コポリマー
0.2
Tremoist−TP(日本精化) 0.03
カルボマー 0.1
精製水 20.0
D部
Neosolue−AquaS(日本精化) 0.5
ポリクオタニウム−51 1.0
アスコルビルグルコシド 1.0
水酸化カリウム 0.2
フェノキシエタノール 0.05
メチルパラベン 0.01
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部、D部をそれぞれ混合し、約70℃に加温し、均一に溶解、分散させた。C部を混合し、攪拌して粘性の液とした。A部をホモディスパーにて攪拌しながらB部を加えた後、D部を加えて乳化した。冷却し約50℃にて、C部を加え、攪拌して約40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例5のエステル化物 0.3
スクワラン 5.0
ステアリン酸 1.0
Plandool−ISS(日本精化) 1.0
マカデミアナッツ油 3.0
水添ホホバ油 2.0
ワセリン 2.0
オリーブ油脂肪酸セテアリル 1.0
オリーブ油脂肪酸ソルビタン 0.8
ラノリン脂肪酸アルギニン塩 1.5
オレイン酸ポリグリセリル−10 1.0
B部
アクリル酸・メタクリル酸アルキル共重合体 0.1
水酸化K 0.07
(アクリロイルジメチルタウリンアンモニウム/
メタクリル酸ベヘネス−25)クロスポリマー 0.2
Tremoist−SL(日本精化) 1.0
精製水 10.0
加水分解ポリγ−グルタミン酸K 0.1
ポリグルタミン酸Na 0.1
オリゴペプチド−24 0.05
C部
イヌリン(日本精化) 1.0
グリセリン 9.0
プロパンジオール 10.0
PEG−8 5.0
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、C部をそれぞれ混合し、約70℃に加温し、均一に溶解、分散させた。B部を混合し、攪拌して粘性の液とした。C部をホモミキサーにて攪拌しながらA部を加えて乳化した。冷却し約50℃にて、B部を加え、攪拌して約40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
グリセリン 12.0
BG 6.0
Phytocompo−PP(日本精化) 2.5
B部
合成例1のエステル化物 0.2
オリーブ油 1.5
シア脂 1.0
Neosolue−DiSM(日本精化) 5.0
ステアリン酸スクロース 0.8
セテアリルグルコシド 1.2
ベヘニルアルコール 1.5
セラミド2 0.01
セラミド3 0.01
セラミド5 0.01
セラミド6 0.01
テトラヘキシルデカン酸アスコルビル 7.0
ラウロイルサルコシンイソプロピル 2.0
水添ココグリセリル 3.0
セタノール 2.5
ステアリン酸ソルビタン 0.8
C部
キサンタンガム 0.05
Tremoist−SL(日本精化) 1.0
チューベロース多糖体 0.01
水溶性コラーゲン 0.05
加水分解コラーゲン 0.5
ピロ亜硫酸Na 0.03
アルブチン(日本精化) 1.0
トラネキサム酸(日本精化) 1.0
D部
Neosolue−Aqulio(日本精化) 1.0
プロパンジオール 3.0
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部、D部をそれぞれ混合し、約70℃に加温し、均一に溶解、分散させた。C部を混合し、攪拌して粘性の液とした。A部をホモディスパーにて攪拌しながらB部を加えた後、D部を加えて乳化した。冷却し約50℃にて、C部を加え、攪拌して約40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例4のエステル化物 2.0
Plandool−LG2(日本精化) 2.0
Plandool−H(日本精化) 2.0
スクワラン 8.0
ステアリン酸 1.0
Plandool−ISS(日本精化) 1.0
マカデミアナッツ油 3.0
水添ホホバアルコール 2.0
オリーブ油脂肪酸セテアリル 1.0
オリーブ油脂肪酸ソルビタン 0.8
オレイン酸ポリグリセリル−10 1.0
ラウリン酸ポリグリセリル−10 0.5
B部
アクリル酸・メタクリル酸アルキル共重合体 0.1
水酸化K 0.07
アクリル酸ヒドロキシエチル/アクリロイル
ジメチルタウリンNa)コポリマー 0.05
(アクリロイルジメチルタウリンアンモニウム/メタクリル酸ベヘネス−25)
クロスポリマー 0.05
Tremoist−TP(日本精化) 0.02
精製水 10.0
加水分解ポリγ−グルタミン酸K 0.1
ポリグルタミン酸Na 0.1
オリゴペプチド−24 0.05
C部
Neosolue−Aqua(日本精化) 1.0
トラネキサム酸(日本精化) 1.0
マンノシルエリストールリピッド 0.2
ジグリセリン 5.0
プロパンジオール 3.0
PEG−8 2.0
ピロ亜硫酸Na 0.03
メチルパラベン 0.1
フェノキシエタノール 0.3
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、C部をそれぞれ混合し、約70℃に加温し、均一に溶解、分散させた。B部を混合し、攪拌して粘性の液とした。C部をホモミキサーにて攪拌しながらA部を加えて乳化した。冷却し約50℃にて、B部を加え、攪拌して約40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 5.0
Plandool−LG2(日本精化) 2.0
Plandool−S(日本精化) 2.0
Neosolue−Aqulio(日本精化) 2.0
リンゴ酸ジイソステアリル 6.0
コハク酸ジエチルヘキシル(日本精化) 2.0
Neosolue−DiSM(日本精化) 2.0
ミネラルオイル 23.0
セバシン酸ジエチルヘキシル 10.0
PEG−25水添ヒマシ油 3.0
トリイソステアリン酸PEG−20グリセリル 4.0
イソステアリン酸PEG−12 3.0
セスキオレイン酸ソルビタン 1.5
オレイン酸ポリオキシエチレンソルビタン 0.3
ステアリン酸ポリグリセリル−6 0.5
ステアリン酸グリセリル 1.0
マイクロクリスタリンワックス 2.0
トコフェロール 0.05
プロピルパラベン 0.05
B部
Neosolue−Aqulio(日本精化) 1.0
ジグリセリン 3.0
DPG 5.0
メチルパラベン 0.05
エデト酸3Na 0.02
フェノキシエタノール 0.2
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を秤りとり、約80℃に加温して溶解した。B部を秤りとり、約80℃に加温する。攪拌しながらA部にB部を徐々に加え、混合後40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 0.5
Plandool−LG2(日本精化) 2.0
ステアリン酸K 10.0
パルミチン酸K 10.0
ミリスチン酸K 10.0
ラウリン酸K 4.0
ラウロイルサルコシンイソプロピル 0.8
PEG1500 10.0
グリセリン 15.0
モノステアリン酸グリセリル 1.0
POE(20)ソルビタンモノステアレート 2.0
B部
Tremoist−TP(日本精化) 0.02
ヒドロキシプロピルメチルセルロース 0.05
チューベロース多糖体 0.05
カチオン化グァーガム 0.05
ポリクオタニウム−7 0.5
ポリクオタニウム−39 0.5
メチルパラベン 0.1
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を秤りとり、約80℃に加温して溶解した。B部を秤りとり、約80℃に加温する。攪拌しながらA部にB部を徐々に加え、混合後40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 1.0
Neosolue−DiSM(日本精化) 8.0
Ecolano CLE−S(日本精化) 5.0
LUSPLAN DD−DA7(日本精化) 0.5
スクワラン 8.0
マカデミアナッツ油 0.5
ローズヒップ油 1.0
メドウフォーム油 1.0
ワセリン 15.0
マイクロクリスタリンワックス 2.0
ステアリン酸グリセリル 2.0
セタノール 2.0
リン酸セチル 1.0
ラノリンアルコール 3.0
プロピルパラベン 0.1
トコフェロール 0.05
パーフルオロポリエーテル 1.0
B部
グリセリン 8.0
プロパンジオール 5.0
メチルパラベン 0.1
エチルヘキシルグリセリン 0.5
水酸化Na 0.5
水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
B部を約70℃に加温し溶解させた。別の容器にA部をとり、約80℃に加温し溶解させた。B部にA部をホモミキサーで攪拌しながら添加し乳化した。乳化後、約40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例4のエステル化物 0.2
ステアリン酸K 10.0
パルミチン酸K 10.0
ミリスチン酸K 10.0
ラウリン酸K 4.0
ラノリン脂肪酸アルギニン塩 3.0
ラウロイルサルコシンイソプロピル 0.8
PEG1500 10.0
グリセリン 15.0
Plandool−SUN(日本精化) 0.2
モノステアリン酸グリセリル 1.0
POE(20)ソルビタンモノステアレート 2.0
B部
イヌリン(日本精化) 1.0
Tremoist−TP(日本精化) 0.02
Phytopresome MEL(日本精化) 1.0
ポリクオタニウム−7 0.5
ポリクオタニウム−39 0.5
メチルパラベン 0.01
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温して溶解した。B部を約80℃に加温した。攪拌しながらA部にB部を徐々に加え、混合後40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例2のエステル化物 4.0
水添ポリイソブテン 6.0
LUSPLAN DD−DA7(日本精化) 3.0
ポリブテン 8.0
ポリエチレン 5.0
エチルセルロース 0.2
合成ワックス 1.2
シア脂 3.0
酸化鉄 2.3
マイカ 1.5
酸化チタン 2.5
赤202 1.5
エチルヘキサン酸セチル(日本精化) 5.0
セスキオレイン酸ソルビタン 1.0
トコフェロール 0.05
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
全成分を約80℃に加温し、均一に混合した後、室温まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例2のエステル化物 7.5
(ジフェニルメチルシロキシフェニルメチコン/フェニルシルセスキオキサン)
クロスポリマー 15.0
エチルヘキサン酸セチル(日本精化) 合計で100となる量
トリエチルヘキサン酸トリメチロールプロパン(日本精化) 10.0
イソヘキサデカン 8.0
トリメリト酸トリトリデシル 8.0
ビースワックス 8.0
セレシン 3.0
ステアリン酸 2.0
モクロウ 2.0
LUSPLAN DD−DA5(日本精化) 3.0
ワセリン 2.5
精製ラノリン(日本精化) 2.0
Plandool−LG2(日本精化) 6.0
リンゴ酸ジイソステアリル 5.0
Neosolue−DiSM(日本精化) 5.0
ミネラルオイル 5.0
セスキイソステアリン酸ソルビタン 0.1
Neosolue−Aqua(日本精化) 0.1
Neosolue−DE(日本精化) 0.5
パルミチン酸イソプロピル(日本精化) 0.1
メトキシケイヒ酸オクチル 0.01
トコフェロール 0.1
ブチルカルバミン酸ヨウ化プロピニル 0.01
酸化チタン 適量
酸化亜鉛 適量
ベニバナ赤 適量
赤226 適量
黄5 適量
ホウケイ酸(Ca/Al) 適量
シリカ 適量
酸化スズ 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
全成分を約80℃に加温し、均一に混合、混錬した後、室温まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例1のエステル化物 3.0
Plandool−G(日本精化) 1.0
Plandool−LG1(日本精化) 7.0
LUSPLAN PI−DA(日本精化) 5.0
テトラエチルヘキサン酸ペンタエリスリチル(日本精化) 10.0
リンゴ酸ジイソステアリル 合計で100となる量
トリ(カプリン酸/カプリル酸)グリセリル(日本精化) 10.0
スクワラン 7.0
イソノナン酸イソトリデシル 8.0
トリメリト酸トリエチルヘキシル 3.0
アジピン酸ジイソブチル 3.0
セバシン酸ジエチル 3.0
マイクロクリスタリンワックス 5.0
ポリエチレン、マイクロクリスタリンワックス混合物 8.0
メチルパラベン 適量
デヒドロ酢酸 適量
酸化チタン 適量
赤218 適量
赤214 適量
赤202 適量
酸化鉄 適量
黄色4 適量
ホウケイ酸(Ca/Al)、酸化チタン、シリカ、酸化スズ 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
全成分を約80℃に加温し、均一に混合、混錬した後、室温まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2のエステル化物 1.0
イソドデカン 10.0
トリ(カプリン酸/カプリル酸)グリセリル(日本精化) 4.0
メトキシケイヒ酸エチルヘキシル 3.0
Plandool−SUN(日本精化) 1.0
Plandool−LG2(日本精化) 1.0
Plandool−LG4(日本精化) 1.0
ワセリン 1.0
イソノナン酸イソトリデシル 2.0
テトラヘキシルデカン酸アスコルビル 0.1
パルミチン酸デキストリン 0.3
イソステアリン酸ソルビタン 1.5
トリベヘニン 0.5
(アクリル酸ブチル/ジメタクリル酸グリコール)クロスポリマー、
シリカ、(メタクリル酸メチル/ジメタクリル酸グリコール)クロスポリマー混合物
2.0
窒化ホウ素 1.0
ポリソルベート20 2.0
PEG−60水添ヒマシ油 1.0
ジステアルジモニウムヘクトライト(20%) 2.5
ポリプロピルシルセスキオキサンシクロペンタシロキサン混合物 1.0
マイカ 15.0
タルク 4.0
酸化亜鉛 5.0
酸化チタン 10.0
酸化鉄 1.5
B部
DPG 4.0
マルチトール(75%液) 1.0
Neosolue−AquaS(日本精化) 0.4
塩化Na 1.0
BG 1.0
Tremoist−SL(日本精化) 1.0
エタノール 0.5
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約70℃に加温、よく攪拌し均一に分散させた。B部を約70℃に加温、均一にしたのちA部にB部を加え、約70℃で撹拌、乳化し、約40℃まで冷却した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
Phytocompo−PP(日本精化) 1.0
BG 10.0
グリセリン 9.0
B部
合成例2のエステル化物 0.5
メトキシケイヒ酸エチルヘキシル 7.0
ジエチルアミノヒドロキシベンゾイル安息香酸ヘキシル 7.0
ベヘニルアルコール 4.0
Plandool−LG1(日本精化) 0.5
Plandool−MAS(日本精化) 1.0
C部
イヌリン(日本精化) 0.3
精製水 合計で100となる量
D部
キサンタンガム 0.2
ヒアルロン酸Na 0.01
精製水 10.0
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を均一に分散した。B部、C部をそれぞれ約70℃に加温溶解した。A部にB部を徐々に添加後、C部を徐々に添加し、乳化した。攪拌しながら冷却し、45℃でD部、E部を加え、均一に混合した。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
超微粒子酸化チタン 5.0
精製水 合計で100となる量
BG 7.0
エデト酸二ナトリウム 0.05
トリエタノールアミン 1.0
B部
合成例2のエステル化物 0.2
オキシベンゾン 3.0
パラメトキシケイヒ酸オクチル 5.0
t−ブチルメトキシベンゾイルメタン 3.0
セバシン酸ジエチルヘキシル(日本精化) 8.0
Plandool−H(日本精化) 2.0
Plandool−SUN(日本精化) 2.0
Plandool−MAS(日本精化) 0.1
Plandool−LG1(日本精化) 0.1
Plandool−LG2(日本精化) 0.1
Plandool−LG3(日本精化) 0.1
Plandool−LG4(日本精化) 0.1
LUSPLAN PI−DA(日本精化) 3.0
エチルヘキサン酸セチル(日本精化) 3.0
セバシン酸ジイソプロピル(日本精化) 5.0
ステアリルアルコール 3.0
バチルアルコール 1.0
ステアリン酸 3.0
グリセリルモノステアレート 3.0
ポリアクリル酸エチル 1.0
ラノリン脂肪酸 0.5
酸化防止剤、香料 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を加熱溶解し、十分分散させる。この中にB部を加熱溶解させたものを加え、ホモジナイザーを用いて乳化分散し、室温まで撹拌冷却した。
〇Ecolano DP−50:クオタニウム−33、DPG
〇Ecolano CA−NH(旧カチオンNH):クオタニウム−33、BG
〇Ecolano DC−30(旧ベルポールDC−50):ジヒドロコレス−30
〇Ecolano MAC(旧YOFCO MAC):マカデミアナッツ油脂肪酸コレステリル
〇Ecolano CLE−S(旧YOFCO CLE−S):ラノリン脂肪酸コレステリル
〇LUSPLAN DD−IS:ジイソステアリン酸ダイマージリノレイル
〇LUSPLAN PI−DA:ダイマージリノール酸ジ(イソステアリル/フィトステリル)
〇LUSPLAN DD−DHR:ダイマージリノレイル水添ロジン縮合物
〇LUSPLAN DD−DA5:ダイマージリノール酸ダイマージリノレイル
〇LUSPLAN DD−DA7:ダイマージリノール酸ダイマージリノレイル
〇LUSPLAN SR−DM4:ダイマージリノール酸ダイマージリノレイル、トリ(カプリル酸/カプリン酸)グリセリル
〇Neosolue−DiSM:リンゴ酸ジイソステアリル
〇Neosolue−Aqulio:シクロヘキサンジカルボン酸ビスエトキシジグリコール
〇Neosolue−Aqua:(エイコサン二酸/テトラデカン二酸)ポリグリセリル−10、グリセリン
〇Neosolue−AquaS:(エイコサン二酸/テトラデカン二酸)ポリグリセリル−10、グリセリン
〇Neosolue−MP:ジネオペンタン酸メチルペンタンジオール
〇Neosolue−DE:ジネオペンタン酸ジエチルペンタンジオール
〇Plandool−H:ダイマージリノール酸(フィトステリル/イソステアリル/セチル/ステアリル/ベヘニル)
〇Plandool−S:ダイマージリノール酸(フィトステリル/イソステアリル/セチル/ステアリル/ベヘニル)
〇Plandool−G:ダイマージリノール酸ダイマージリノレイルビス(ベヘニル/イソステアリル/フィトステリル)
〇Plandool−DP:ビスジグリセリルポリアシルアジペート−2
〇Plandool−ISS:イソステアリン酸フィトステリル
〇Plandool−SUN:ヒマワリ種子油脂肪酸フィトステリル
〇Plandool−MAS:マカデミアナッツ油脂肪酸フィトステリル
〇Plandool−LG1:ラウロイルグルタミン酸ジ(フィトステリル/オクチルドデシル/ベヘニル)
〇Plandool−LG2:ラウロイルグルタミン酸ジ(フィトステリル/オクチルドデシル)
〇Plandool−LG3:ラウロイルグルタミン酸ジ(フィトステリル/オクチルドデシル/ベヘニル)
〇Plandool−LG4:ラウロイルグルタミン酸ジ(フィトステリル/オクチルドデシル/ベヘニル)
〇Phytocompo−PP:水添レシチン、フィトステロールズ
〇Phytocompo−C:水添レシチン、フィトステロールズ、セラミド2、セラミド3、セラミド6II
〇Phytopresome MEL:糖脂質、水添レシチン、BG、精製水
〇エルカラクトンMCT:γ−ドコサラクトン、トリ(カプリル酸/カプリン酸)グリセリル
〇エルカラクトンDES:γ−ドコサラクトン、セバシン酸ジエチル
〇Tremoist−TP:シロキクラゲ多糖体
〇Tremoist−SL:シロキクラゲ多糖体水溶液(1%)
〇NanoRepair−CMC5:セラミド1、セラミド2、セラミド3、セラミド5、セラミド6、コレステロール、クオタニウム−33含有組成物
〇NanoRepair−EL:γ−ドコサラクトン、ダイズステロール含有組成物
〇VCエチル:3−O−エチルアスコルビン酸
Claims (6)
- 硬質ラノリン脂肪酸と、炭素数12〜26の飽和直鎖アルコール又は/及び多価アルコールとのエステル化物を含有する化粧料。
- 炭素数12〜26の飽和直鎖アルコールがラウリルアルコール、ミリスチルアルコール、セチルアルコール、ステアリルアルコール、アラキジルアルコール、ベヘニルアルコール、リグノセリルアルコール、及びセリルアルコールから選択される1種又は2種以上であることを特徴とする請求項1に記載の化粧料。
- 多価アルコールがエチレングリコール、ジエチレングリコール、トリエチレングリコール、ポリエチレングリコール、1,3−プロパンジオール、プロピレングリコール、ジプロピレングリコール、1,2−ブチレングリコール、1,3−ブチレングリコール、1,4−ブチレングリコール、ネオペンチルグリコール、トリメチロールプロパン、ペンタエリスリトール、ジペンタエリスリトール、グリセリン、ジグリセリン、及びポリグリセリンから選択される1種又は2種以上であることを特徴とする請求項1又は2に記載の化粧料。
- 化粧料が毛髪用であることを特徴とする請求項1〜3のいずれかに記載の化粧料。
- 化粧料が皮膚用であることを特徴とする請求項1〜3のいずれかに記載の化粧料。
- 化粧料がメイクアップ用であることを特徴とする請求項1〜3のいずれかに記載の化粧料。
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JPH05345709A (ja) * | 1992-01-30 | 1993-12-27 | Helene Curtis Inc | シャンプー組成物およびその製造方法 |
JP2009522268A (ja) * | 2005-12-30 | 2009-06-11 | エイボン プロダクツ インコーポレーテッド | まつげをカールする方法 |
JP2010270029A (ja) * | 2009-05-20 | 2010-12-02 | Shiseido Co Ltd | 水中油型乳化皮膚外用剤 |
JP2011195528A (ja) * | 2010-03-23 | 2011-10-06 | Nippon Fine Chem Co Ltd | 合成エステルワックス |
JP2013087123A (ja) * | 2011-10-13 | 2013-05-13 | Nippon Fine Chem Co Ltd | 硬質ラノリン脂肪酸用いたモンタン酸およびモンタン酸ワックスの代替方法 |
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JPH05345709A (ja) * | 1992-01-30 | 1993-12-27 | Helene Curtis Inc | シャンプー組成物およびその製造方法 |
JP2009522268A (ja) * | 2005-12-30 | 2009-06-11 | エイボン プロダクツ インコーポレーテッド | まつげをカールする方法 |
JP2010270029A (ja) * | 2009-05-20 | 2010-12-02 | Shiseido Co Ltd | 水中油型乳化皮膚外用剤 |
JP2011195528A (ja) * | 2010-03-23 | 2011-10-06 | Nippon Fine Chem Co Ltd | 合成エステルワックス |
JP2013087123A (ja) * | 2011-10-13 | 2013-05-13 | Nippon Fine Chem Co Ltd | 硬質ラノリン脂肪酸用いたモンタン酸およびモンタン酸ワックスの代替方法 |
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