JP2016521858A - 表面多孔性材料を含むクロマトグラフィーカラムおよび分離デバイス、および超臨界流体クロマトグラフィーおよび他のクロマトグラフィーのためのこれらの使用 - Google Patents

表面多孔性材料を含むクロマトグラフィーカラムおよび分離デバイス、および超臨界流体クロマトグラフィーおよび他のクロマトグラフィーのためのこれらの使用 Download PDF

Info

Publication number
JP2016521858A
JP2016521858A JP2016519596A JP2016519596A JP2016521858A JP 2016521858 A JP2016521858 A JP 2016521858A JP 2016519596 A JP2016519596 A JP 2016519596A JP 2016519596 A JP2016519596 A JP 2016519596A JP 2016521858 A JP2016521858 A JP 2016521858A
Authority
JP
Japan
Prior art keywords
porous
group
core
separation device
butyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2016519596A
Other languages
English (en)
Japanese (ja)
Other versions
JP2016521858A5 (enExample
Inventor
ウィンダム，ケビン・ダニエル
フェアチャイルド，ジェイコブ・ネイサン
イラネタ，パメラ・シー
シャイナー，スティーブン・ジェームズ
ブルースミーシュ，ダリル・ダブリュ
ウォルシュ，ダニエル・ピー
Original Assignee
ウオーターズ・テクノロジーズ・コーポレイシヨン
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ウオーターズ・テクノロジーズ・コーポレイシヨン filed Critical ウオーターズ・テクノロジーズ・コーポレイシヨン
Publication of JP2016521858A publication Critical patent/JP2016521858A/ja
Publication of JP2016521858A5 publication Critical patent/JP2016521858A5/ja
Pending legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/30—Partition chromatography
    • B01D15/305—Hydrophilic interaction chromatography [HILIC]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/32—Bonded phase chromatography
    • B01D15/322—Normal bonded phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/40—Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28059—Surface area, e.g. B.E.T specific surface area being less than 100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28061—Surface area, e.g. B.E.T specific surface area being in the range 100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069—Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069—Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • B01J20/28071—Pore volume, e.g. total pore volume, mesopore volume, micropore volume being less than 0.5 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078—Pore diameter
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078—Pore diameter
    • B01J20/28083—Pore diameter being in the range 2-50 nm, i.e. mesopores
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078—Pore diameter
    • B01J20/28085—Pore diameter being more than 50 nm, i.e. macropores
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282—Porous sorbents
    • B01J20/283—Porous sorbents based on silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804—Compounds having Si-O-C linkages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
JP2016519596A 2013-06-11 2014-06-10 表面多孔性材料を含むクロマトグラフィーカラムおよび分離デバイス、および超臨界流体クロマトグラフィーおよび他のクロマトグラフィーのためのこれらの使用 Pending JP2016521858A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361833699P 2013-06-11 2013-06-11
US61/833,699 2013-06-11
PCT/US2014/041765 WO2014201033A1 (en) 2013-06-11 2014-06-10 Chromatographic columns and separation devices comprising a superficially porous material; and use thereof for supercritical fluid chromatography and other chromatography

Publications (2)

Publication Number Publication Date
JP2016521858A true JP2016521858A (ja) 2016-07-25
JP2016521858A5 JP2016521858A5 (enExample) 2017-07-27

Family

ID=52022714

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2016519596A Pending JP2016521858A (ja) 2013-06-11 2014-06-10 表面多孔性材料を含むクロマトグラフィーカラムおよび分離デバイス、および超臨界流体クロマトグラフィーおよび他のクロマトグラフィーのためのこれらの使用

Country Status (5)

Country Link
US (2) US11577179B2 (enExample)
EP (2) EP3007792A4 (enExample)
JP (1) JP2016521858A (enExample)
CN (2) CN105555383B (enExample)
WO (1) WO2014201033A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102532719B1 (ko) * 2021-12-16 2023-05-16 한국표준과학연구원 액체크로마토그래피 컬럼 충전제

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11439977B2 (en) 2009-06-01 2022-09-13 Waters Technologies Corporation Hybrid material for chromatographic separations comprising a superficially porous core and a surrounding material
EP3964287A1 (en) 2009-06-01 2022-03-09 Waters Technologies Corporation Hybrid material for chromatographic separations
JP6199184B2 (ja) 2010-07-26 2017-09-20 ウオーターズ・テクノロジーズ・コーポレイシヨン 粒度分布の狭い実質的に非多孔質のコアを含む表面多孔質材料、その製造方法及びクロマトグラフィー分離用としてのその使用
US10453675B2 (en) 2013-09-20 2019-10-22 Versum Materials Us, Llc Organoaminosilane precursors and methods for depositing films comprising same
JP6791844B2 (ja) * 2015-03-24 2020-11-25 株式会社ダイセル 超臨界流体クロマトグラフィー用の固定相
ES2805779T3 (es) * 2015-07-29 2021-02-15 Imerys Filtration Minerals Inc Ayudas de filtro de material compuesto a prueba de enfriamiento y métodos relacionados
EP3330704B1 (en) * 2015-07-31 2021-04-07 Daicel Corporation Stationary phase for supercritical fluid chromatography
CN108348818B (zh) * 2015-08-13 2021-05-28 沃特世科技公司 镍-钴合金材料装置和部件
EP3426388A1 (en) * 2016-03-06 2019-01-16 Waters Technologies Corporation Superficially porous materials comprising a coated core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
EP3435079B1 (en) * 2016-03-23 2020-07-29 Daicel Corporation Chromatography stationary phase
WO2017223140A1 (en) * 2016-06-21 2017-12-28 Purdue Research Foundation Uniformly dense stationary phase for chromatography
CN110383060A (zh) 2017-03-08 2019-10-25 沃特世科技公司 使用色谱法确定极性农药
DE102017009236A1 (de) * 2017-10-04 2019-04-04 Dr. Albin Maisch High Performance LC GmbH Oberflächenporöse Trägermaterialien sowie das Verfahren zu deren Herstellung
US11325104B2 (en) * 2017-12-07 2022-05-10 Emp Biotech Gmbh System and method of applied radial technology chromatography
CN108976561B (zh) * 2018-08-03 2021-04-02 阜南佳利工艺品有限公司 一种低气味仿藤条的制备方法
EP3614414A1 (en) * 2018-08-20 2020-02-26 FEI Company Method of examining a sample using a charged particle microscope
JP7112499B2 (ja) * 2018-08-30 2022-08-03 株式会社ダイセル クロマトグラフィー用の固定相
CN109692501B (zh) * 2018-12-29 2021-02-09 武汉谱立科技有限公司 一种色谱柱及其制备方法和应用
US11964874B2 (en) * 2020-06-09 2024-04-23 Agilent Technologies, Inc. Etched non-porous particles and method of producing thereof
CN112451996B (zh) * 2020-11-10 2021-09-24 浙江大学 一种多柱连续流层析捕获蛋白的优化方法
EP4267270A4 (en) * 2020-12-24 2025-07-30 Ligar Lp METHOD, SYSTEM AND/OR APPARATUS FOR THE USE OF LIQUID OR FLUID CARBON DIOXIDE IN THE EXTRACTION AND/OR SOLUBILIZATION OF A SOURCE MATERIAL AND BONDING AND/OR ELUTION WITH A MOLECULARLY IMPRINTED POLYMER
CN112903837B (zh) * 2021-01-14 2022-11-04 中国工程物理研究院材料研究所 一种氢同位素气体分析用金属多孔层开管柱及其制备方法
US20230047460A1 (en) * 2021-07-30 2023-02-16 Agilent Technologies, Inc. Methods of making media of substantially monodisperse populations of polyarylketone or polyarylthioetherketone particles, and containers comprising them
WO2023026251A1 (en) * 2021-08-26 2023-03-02 Waters Technologies Corporation Superficially porous organic polymer particles
US20240082820A1 (en) * 2022-08-26 2024-03-14 Waters Technologies Corporation Core-shell particles having a non-porous core and a porous shell
US12478949B2 (en) 2022-08-26 2025-11-25 Waters Technologies Corporation Composite particles with non-porous hybrid organic-inorganic material
EP4577344A1 (en) * 2022-08-26 2025-07-02 Waters Technologies Corporation Bonded hybrid polymer non-porous particles and their use for bioseparations
CN116422297B (zh) * 2023-04-24 2024-04-30 中国电建集团昆明勘测设计研究院有限公司 一种改性石墨烯材料的制备方法及应用
US20250083090A1 (en) * 2023-09-08 2025-03-13 Spiritus Technologies, Pbc High performance gas adsorbing material

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0084979A2 (en) * 1982-01-26 1983-08-03 Richard Stocks Limited Wheel coupling apparatus
US4415631A (en) * 1980-06-27 1983-11-15 Akzo Porous inorganic support material coated with an organic stationary phase, for use in chromatography, and process for its preparation
US20060207923A1 (en) * 2004-02-12 2006-09-21 Li Guang Q Polar-modified bonded phase materials for chromatographic separations
US20070090052A1 (en) * 2005-10-20 2007-04-26 Broske Alan D Chromatographic stationary phase
US20070189944A1 (en) * 2006-02-13 2007-08-16 Advanced Materials Technology, Inc. Porous microparticles with solid cores
JP2010533124A (ja) * 2007-07-13 2010-10-21 ユニバーシティ・カレッジ・コークーナショナル・ユニバーシティ・オブ・アイルランド，コーク 微粒子合成方法
WO2012018596A2 (en) * 2010-07-26 2012-02-09 Waters Technologies Corporation Superficially porous materials comprising a substantially nonporous hybrid core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
US20120055860A1 (en) * 2009-06-01 2012-03-08 Waters Technologies Corporation Hybrid inorganic/organic materials having novel surface modification; process for the preparation of inorganic/organic hybrid materials; and use of said particles for chromatographic separations
JP2012509974A (ja) * 2008-11-26 2012-04-26 ユニバーシティ・カレッジ・コークーナショナル・ユニバーシティ・オブ・アイルランド，コーク シリカ微粒子を製造する方法
WO2013173494A1 (en) * 2012-05-15 2013-11-21 Waters Technologies Corporation Chromatographic materials

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2357184A1 (de) 1973-11-16 1975-05-22 Merck Patent Gmbh Verfahren zur herstellung von organisch modifizierten siliciumdioxiden
JP2504005B2 (ja) * 1986-11-17 1996-06-05 東ソー株式会社 充填剤およびその製法
US5374755A (en) 1992-07-17 1994-12-20 Millipore Corporation Liquid chromatography stationary phases with reduced silanol interactions
US5576453A (en) 1994-07-18 1996-11-19 Es Industries Stable, sterically-protected, bonded phase silicas prepared from bifunctional silanes
US6686035B2 (en) 1999-02-05 2004-02-03 Waters Investments Limited Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation
US6528167B2 (en) 2001-01-31 2003-03-04 Waters Investments Limited Porous hybrid particles with organic groups removed from the surface
AU2003265996A1 (en) 2002-09-10 2004-04-30 Waters Investments Limited A chromatographic column and methods for controlling sorbent density
DE10393599T5 (de) 2002-10-30 2005-10-27 Waters Investments Ltd., New Castle Poröse anorganische/organische Homogene copolymerische Hybridmaterialien für chromatographische Auftrennungen und Verfahren für deren Herstellung
US7074491B2 (en) 2003-11-04 2006-07-11 Dionex Corporation Polar silanes for binding to substrates and use of the bound substrates
WO2006019988A1 (en) 2004-07-30 2006-02-23 Waters Investments Limited Porous inorganic/organic hybrid materials with ordered domains for chromatographic separations and processes for their preparation
US7402243B2 (en) 2004-09-10 2008-07-22 Dionex Corporation Organosilanes and substrate bonded with same
WO2006039507A2 (en) 2004-10-01 2006-04-13 Phenomenex, Inc. Ph stable chromatographic media using templated multilayer organic/inorganic grafting
CN1262476C (zh) 2004-11-03 2006-07-05 武汉理工大学 单分散二氧化硅微孔微球及其制备方法
JP4936208B2 (ja) 2005-06-20 2012-05-23 株式会社豊田中央研究所 コアシェル型球状シリカ系メソ多孔体及びコアシェル型球状シリカ系メソ多孔体の製造方法
US9308520B2 (en) 2005-12-16 2016-04-12 Akzo Nobel N.V. Silica based material
WO2007122930A1 (ja) 2006-04-20 2007-11-01 Asahi Glass Company, Limited コアシェル型シリカおよびその製造方法
JP5152600B2 (ja) 2007-02-21 2013-02-27 ウオーターズ・テクノロジーズ・コーポレイシヨン 高い有機物含有量および向上性細孔形状を有するクロマトグラフィー分離用の多孔質無機／有機ハイブリッド粒子
JP5319554B2 (ja) 2007-02-22 2013-10-16 ウオーターズ・テクノロジーズ・コーポレイシヨン 分離を実行するための装置、機器、及び、方法
US7534352B2 (en) 2007-05-01 2009-05-19 Agilent Technologies, Inc. Reversed endcapping and bonding of chromatographic stationary phases using hydrosilanes
US20090218276A1 (en) 2008-02-29 2009-09-03 Brigham Young University Functionalized diamond particles and methods for preparing the same
US9248383B2 (en) 2008-04-08 2016-02-02 Waters Technologies Corporation Composite materials containing nanoparticles and their use in chromatography
US8277883B2 (en) 2008-06-13 2012-10-02 Agilent Technologies, Inc. Porous silica microspheres having organosilane modified surfaces
US9284456B2 (en) 2008-08-29 2016-03-15 Agilent Technologies, Inc. Superficially porous metal oxide particles, methods for making them, and separation devices using them
US8685283B2 (en) 2008-08-29 2014-04-01 Agilent Technologies, Inc. Superficially porous metal oxide particles, methods for making them, and separation devices using them
US20100061367A1 (en) 2008-09-11 2010-03-11 Pradeep Sindhu Methods and apparatus related to lossless operation within a data center
US7846337B2 (en) 2009-02-17 2010-12-07 Agilent Technologies, Inc. Superficially porous particles and methods of making and using same
US8219758B2 (en) 2009-07-10 2012-07-10 Apple Inc. Block-based non-transparent cache
IN2012DN00363A (enExample) * 2009-08-04 2015-08-21 Waters Technologies Corp
WO2012110995A1 (en) 2011-02-16 2012-08-23 Glantreo Limited Silica core-shell microparticles

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4415631A (en) * 1980-06-27 1983-11-15 Akzo Porous inorganic support material coated with an organic stationary phase, for use in chromatography, and process for its preparation
EP0084979A2 (en) * 1982-01-26 1983-08-03 Richard Stocks Limited Wheel coupling apparatus
US20060207923A1 (en) * 2004-02-12 2006-09-21 Li Guang Q Polar-modified bonded phase materials for chromatographic separations
US20070090052A1 (en) * 2005-10-20 2007-04-26 Broske Alan D Chromatographic stationary phase
US20070189944A1 (en) * 2006-02-13 2007-08-16 Advanced Materials Technology, Inc. Porous microparticles with solid cores
JP2010533124A (ja) * 2007-07-13 2010-10-21 ユニバーシティ・カレッジ・コークーナショナル・ユニバーシティ・オブ・アイルランド，コーク 微粒子合成方法
JP2012509974A (ja) * 2008-11-26 2012-04-26 ユニバーシティ・カレッジ・コークーナショナル・ユニバーシティ・オブ・アイルランド，コーク シリカ微粒子を製造する方法
US20120055860A1 (en) * 2009-06-01 2012-03-08 Waters Technologies Corporation Hybrid inorganic/organic materials having novel surface modification; process for the preparation of inorganic/organic hybrid materials; and use of said particles for chromatographic separations
WO2012018596A2 (en) * 2010-07-26 2012-02-09 Waters Technologies Corporation Superficially porous materials comprising a substantially nonporous hybrid core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
WO2012018598A1 (en) * 2010-07-26 2012-02-09 Waters Technologies Corporation Superficially porous materials comprising a substantially nonporous core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
US20130112605A1 (en) * 2010-07-26 2013-05-09 Waters Technologies Corporation Superficially porous materials comprising a substantially nonporous core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
WO2013173494A1 (en) * 2012-05-15 2013-11-21 Waters Technologies Corporation Chromatographic materials

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102532719B1 (ko) * 2021-12-16 2023-05-16 한국표준과학연구원 액체크로마토그래피 컬럼 충전제

Also Published As

Publication number Publication date
CN105555383A (zh) 2016-05-04
US20230173406A1 (en) 2023-06-08
EP3007792A4 (en) 2017-05-03
CN108176078A (zh) 2018-06-19
EP3936226A2 (en) 2022-01-12
WO2014201033A1 (en) 2014-12-18
US20160184736A1 (en) 2016-06-30
US11577179B2 (en) 2023-02-14
EP3007792A1 (en) 2016-04-20
EP3936226A3 (en) 2022-03-16
CN105555383B (zh) 2018-03-20

Similar Documents

Publication Publication Date Title
US20230173406A1 (en) Chromatographic columns and separation devices comprising a superficially porous material; and use thereof for supercritical fluid chromatography and other chromatography
US12427502B2 (en) Superficially porous materials comprising a substantially nonporous core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
US20240390877A1 (en) Porous materials with controlled porosity; process for the preparation thereof; and use thereof for chromatographic separations
US9248383B2 (en) Composite materials containing nanoparticles and their use in chromatography
JP2015163895A (ja) クロマトグラフ分離用ハイブリッド材料
US20230041546A1 (en) Superficially porous materials comprising a substantially nonporous hybrid core having narrow particle size distribution

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20170609

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20170609

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20180612

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20180910

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20181211

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20190625

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20190919

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20191224

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200616

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20200910

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20201215

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20210105