CN105555383B - 包含表面多孔材料的色谱柱和分离装置及其用于超临界流体色谱及其他色谱的用途 - Google Patents
包含表面多孔材料的色谱柱和分离装置及其用于超临界流体色谱及其他色谱的用途 Download PDFInfo
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- CN105555383B CN105555383B CN201480044773.8A CN201480044773A CN105555383B CN 105555383 B CN105555383 B CN 105555383B CN 201480044773 A CN201480044773 A CN 201480044773A CN 105555383 B CN105555383 B CN 105555383B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/30—Partition chromatography
- B01D15/305—Hydrophilic interaction chromatography [HILIC]
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/32—Bonded phase chromatography
- B01D15/322—Normal bonded phase
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/40—Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
- B01J20/28004—Sorbent size or size distribution, e.g. particle size
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
- B01J20/28016—Particle form
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
- B01J20/28057—Surface area, e.g. B.E.T specific surface area
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
- B01J20/28057—Surface area, e.g. B.E.T specific surface area
- B01J20/28059—Surface area, e.g. B.E.T specific surface area being less than 100 m2/g
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
- B01J20/28057—Surface area, e.g. B.E.T specific surface area
- B01J20/28061—Surface area, e.g. B.E.T specific surface area being in the range 100-500 m2/g
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
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- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
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- B01J20/28069—Pore volume, e.g. total pore volume, mesopore volume, micropore volume
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
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- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
- B01J20/28078—Pore diameter
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
- B01J20/28078—Pore diameter
- B01J20/28083—Pore diameter being in the range 2-50 nm, i.e. mesopores
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
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- B01J20/283—Porous sorbents based on silica
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
- B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
- B01J20/3234—Inorganic material layers
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/12—Organo silicon halides
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
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- Chemical & Material Sciences (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Inorganic Chemistry (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810135720.7A CN108176078A (zh) | 2013-06-11 | 2014-06-10 | 色谱柱和分离装置及其用途 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361833699P | 2013-06-11 | 2013-06-11 | |
| US61/833699 | 2013-06-11 | ||
| PCT/US2014/041765 WO2014201033A1 (en) | 2013-06-11 | 2014-06-10 | Chromatographic columns and separation devices comprising a superficially porous material; and use thereof for supercritical fluid chromatography and other chromatography |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810135720.7A Division CN108176078A (zh) | 2013-06-11 | 2014-06-10 | 色谱柱和分离装置及其用途 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105555383A CN105555383A (zh) | 2016-05-04 |
| CN105555383B true CN105555383B (zh) | 2018-03-20 |
Family
ID=52022714
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810135720.7A Pending CN108176078A (zh) | 2013-06-11 | 2014-06-10 | 色谱柱和分离装置及其用途 |
| CN201480044773.8A Active CN105555383B (zh) | 2013-06-11 | 2014-06-10 | 包含表面多孔材料的色谱柱和分离装置及其用于超临界流体色谱及其他色谱的用途 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810135720.7A Pending CN108176078A (zh) | 2013-06-11 | 2014-06-10 | 色谱柱和分离装置及其用途 |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US11577179B2 (enExample) |
| EP (2) | EP3007792A4 (enExample) |
| JP (1) | JP2016521858A (enExample) |
| CN (2) | CN108176078A (enExample) |
| WO (1) | WO2014201033A1 (enExample) |
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| US11439977B2 (en) | 2009-06-01 | 2022-09-13 | Waters Technologies Corporation | Hybrid material for chromatographic separations comprising a superficially porous core and a surrounding material |
| WO2010141426A1 (en) | 2009-06-01 | 2010-12-09 | Waters Technologies Corporation | Hybrid material for chromatographic separations |
| EP4353682B1 (en) | 2010-07-26 | 2025-11-12 | Waters Technologies Corporation | Superficially porous materials comprising a substantially nonporous hybrid core having narrow particle size distribution, useful for chromatographic separations |
| US10453675B2 (en) | 2013-09-20 | 2019-10-22 | Versum Materials Us, Llc | Organoaminosilane precursors and methods for depositing films comprising same |
| CN107430100B (zh) * | 2015-03-24 | 2021-03-19 | 株式会社大赛璐 | 超临界流体色谱用的固定相 |
| EP3328515B1 (en) * | 2015-07-29 | 2020-04-29 | Imerys Filtration Minerals, Inc. | Chill-proofing composite filter aid and related methods |
| JP6810039B2 (ja) * | 2015-07-31 | 2021-01-06 | 株式会社ダイセル | 超臨界流体クロマトグラフィー用の固定相 |
| CN108348818B (zh) | 2015-08-13 | 2021-05-28 | 沃特世科技公司 | 镍-钴合金材料装置和部件 |
| US11642653B2 (en) | 2016-03-06 | 2023-05-09 | Waters Technologies Corporation | Hybrid material for chromatographic separations comprising a superficially porous core and a surrounding material |
| WO2017164289A1 (ja) * | 2016-03-23 | 2017-09-28 | 株式会社ダイセル | クロマトグラフィー用の固定相 |
| US20190257801A1 (en) * | 2016-06-21 | 2019-08-22 | Purdue Research Foundation | Uniformly dense stationary phase for chromatography |
| EP3593128A1 (en) | 2017-03-08 | 2020-01-15 | Waters Technologies Corporation | Polar pesticide determination using chromatography |
| DE102017009236A1 (de) * | 2017-10-04 | 2019-04-04 | Dr. Albin Maisch High Performance LC GmbH | Oberflächenporöse Trägermaterialien sowie das Verfahren zu deren Herstellung |
| US11325104B2 (en) * | 2017-12-07 | 2022-05-10 | Emp Biotech Gmbh | System and method of applied radial technology chromatography |
| CN108976561B (zh) * | 2018-08-03 | 2021-04-02 | 阜南佳利工艺品有限公司 | 一种低气味仿藤条的制备方法 |
| EP3614414A1 (en) * | 2018-08-20 | 2020-02-26 | FEI Company | Method of examining a sample using a charged particle microscope |
| CN112638519B (zh) * | 2018-08-30 | 2023-11-10 | 株式会社大赛璐 | 色谱用固定相 |
| CN109692501B (zh) * | 2018-12-29 | 2021-02-09 | 武汉谱立科技有限公司 | 一种色谱柱及其制备方法和应用 |
| US11964874B2 (en) * | 2020-06-09 | 2024-04-23 | Agilent Technologies, Inc. | Etched non-porous particles and method of producing thereof |
| CN112451996B (zh) * | 2020-11-10 | 2021-09-24 | 浙江大学 | 一种多柱连续流层析捕获蛋白的优化方法 |
| WO2022137206A1 (en) * | 2020-12-24 | 2022-06-30 | Ligar Limited Partnership | Method, system and/or apparatus for use of liquid or fluid carbon dioxide in extraction and/or solubilising source material and binding and/or elution with a molecularly imprinted polymer |
| CN112903837B (zh) * | 2021-01-14 | 2022-11-04 | 中国工程物理研究院材料研究所 | 一种氢同位素气体分析用金属多孔层开管柱及其制备方法 |
| US20230047460A1 (en) * | 2021-07-30 | 2023-02-16 | Agilent Technologies, Inc. | Methods of making media of substantially monodisperse populations of polyarylketone or polyarylthioetherketone particles, and containers comprising them |
| CN117881474A (zh) * | 2021-08-26 | 2024-04-12 | 沃特世科技公司 | 表面多孔有机聚合物颗粒 |
| KR102532719B1 (ko) * | 2021-12-16 | 2023-05-16 | 한국표준과학연구원 | 액체크로마토그래피 컬럼 충전제 |
| EP4577342A1 (en) * | 2022-08-26 | 2025-07-02 | Waters Technologies Corporation | Core-shell particles having a non-porous core and a porous shell |
| US20240092959A1 (en) * | 2022-08-26 | 2024-03-21 | Waters Technologies Corporation | Bonded hybrid polymer non-porous particles and their use for bioseparations |
| EP4577341A1 (en) | 2022-08-26 | 2025-07-02 | Waters Technologies Corporation | Composite particles with non-porous hybrid organic-inorganic material |
| CN116422297B (zh) * | 2023-04-24 | 2024-04-30 | 中国电建集团昆明勘测设计研究院有限公司 | 一种改性石墨烯材料的制备方法及应用 |
| US20250083090A1 (en) * | 2023-09-08 | 2025-03-13 | Spiritus Technologies, Pbc | High performance gas adsorbing material |
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| Publication number | Publication date |
|---|---|
| US20160184736A1 (en) | 2016-06-30 |
| WO2014201033A1 (en) | 2014-12-18 |
| US11577179B2 (en) | 2023-02-14 |
| EP3936226A2 (en) | 2022-01-12 |
| EP3007792A4 (en) | 2017-05-03 |
| JP2016521858A (ja) | 2016-07-25 |
| US20230173406A1 (en) | 2023-06-08 |
| EP3936226A3 (en) | 2022-03-16 |
| CN105555383A (zh) | 2016-05-04 |
| EP3007792A1 (en) | 2016-04-20 |
| CN108176078A (zh) | 2018-06-19 |
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