JP2016106046A - Producing method of scribing wheel - Google Patents

Abstract

PROBLEM TO BE SOLVED: To provide a scribing wheel capable of scribing a weak material substrate to enhance reinforcement in an end surface of a separated substrate.SOLUTION: A rotational axis is arranged on the center of a discoidal scribing wheel substrate. A blade having V shape section is formed on a circumference part. Diamond film is formed on the blade. Herein, diamond cores are applied and grown by chemical vapor deposition to form the diamond film. Film thickness is defined as 15 to 30 μm. Particle diameter of diamond is defined as 2 μm or less of average particle diameter. After that, a ridgeline part is polished so that difference between polished blade angle and unpolished blade angle of the diamond film is 5 to 10°.Thereby, roughness in the ridgeline part is improved. When a weak material substrate is subjected to scribing to be divided with a scribing wheel, precision in end surface of the divided substrates are increased, resulting in improvement in end surface strength.SELECTED DRAWING: Figure 3B

Description

  The present invention relates to a method of manufacturing a scribing wheel for scribing by pressing and rolling on a brittle material substrate.

Conventional scribing wheels are based on a disc made of cemented carbide or polycrystalline sintered diamond (hereinafter referred to as PCD). PCD is obtained by sintering diamond particles together with cobalt or the like. The scribing wheel is formed by cutting the circumferential edges obliquely from both sides of a disk as a base material to form a V-shaped cutting edge on the circumferential surface. The scribing wheel formed in this way is rotatably attached to a scribing head of a scribing device, pressed against the brittle material substrate with a predetermined load, and moved along the surface of the brittle material substrate to roll it. You can scribe while.

  Patent Document 1 discloses a glass cutting blade in which a V-shaped blade edge surface is coated with diamond in order to increase the life of the glass cutting blade for cutting a glass substrate. This blade for cutting a glass is shaped by coating a diamond film on the surface of a cutting edge formed of a ceramic that is compatible with diamond and then polishing the diamond film. It has been shown that by using such a glass cutting blade, the high-hardness glass can be cut such that the blade has a long life and the cut surface is smooth.

  Patent Document 2 discloses a diamond-coated cutting blade in which a base material such as cemented carbide is coated with a diamond layer in order to prevent slippage or deterioration of cutting quality when cutting an optical fiber, a glass substrate, or the like. ing. This document is characterized in that the surface of the diamond layer is not smoothed after coating.

Japanese Patent Laid-Open No. 04-224128 JP 2011-126754 A

  It has been found that when the brittle material substrate is actually scribed using the glass cutting blade described in Patent Document 1, chipping of the blade edge, peeling of the diamond film, and the like are likely to occur. Even in the diamond-coated cutting blade described in Patent Document 2, since the surface is not smoothed, when the brittle material substrate is scribed, the end face accuracy of the substrate is deteriorated as compared with the case where the polishing is not performed. However, the end face strength is inferior.

  The present invention has been made in view of such problems, and in a scribing wheel coated with a diamond film, improves the end face strength and end face accuracy of the brittle material substrate when the brittle material substrate is scribed and broken. An object of the present invention is to provide a method for manufacturing a scribing wheel.

In order to solve this problem, a method for manufacturing a scribing wheel according to the present invention is a scribing wheel having a ridgeline formed along a circumferential portion of a disk and having a cutting edge composed of the ridgeline and inclined surfaces on both sides of the ridgeline. A method of manufacturing, wherein the scribing is formed by polishing the disk-shaped scribing wheel base material so as to be cut obliquely from both sides of the side surface along the circumference of the disk-shaped scribing wheel substrate, and forming a blade edge portion composed of a slope and a ridge line on the circumferential portion. A diamond nucleus is formed on the edge of the wheel base material, and a diamond film made of diamond particles having an average particle diameter of 2 μm or less is grown by chemical vapor deposition to form a diamond film. plane including becomes perpendicular to the rotation axis of the scribing wheel base, and a cutting edge angle after polishing of the diamond film, Difference in edge angle before grinding is polished so as 5 to 10 °, the film thickness in the vicinity of the ridge line after polishing is to a 5 to 25 [mu] m.

  Here, the diamond film may have a multilayer structure by repeating the generation of diamond nuclei and the growth of the diamond layer a plurality of times.

  Here, a groove in which a ridge line portion of the polishing region is notched at a predetermined interval may be provided, and a portion between the grooves may be formed as a protrusion.

Here, the arithmetic average roughness Ra of the surface of the diamond film after polishing may be 0.03 μm or less .
Furthermore, the edge angle after polishing the diamond film may be 115 to 150 °.

  According to the present invention having such a feature, since the surface roughness of the cutting edge of the scribing wheel can be reduced by polishing as compared with a scribing wheel made of a diamond film having a large diamond particle size, the brittle material The end face accuracy of the substrate is improved, and the end face strength can be improved. In addition, when scribing a brittle material substrate having high hardness, it is possible to obtain an effect that it is difficult to cause chipping or peeling due to fine unevenness in the ridge line portion.

FIG. 1A is a front view of a scribing wheel according to a first embodiment of the present invention. FIG. 1B is a side view of the scribing wheel according to the first embodiment. FIG. 2 is a conceptual diagram showing a state in which a diamond multilayer film is formed on a scribing wheel substrate according to the first embodiment of the present invention. FIG. 3A is an enlarged cross-sectional view of a ridge line portion before polishing of the blade edge according to the first embodiment. FIG. 3B is an enlarged cross-sectional view of a ridge line portion after polishing according to the first embodiment. FIG. 4A is a front view of a scribing wheel according to the second embodiment of the present invention. FIG. 4B is an enlarged cross-sectional view of a ridge line portion after polishing according to the second embodiment. FIG. 4C is an enlarged view of the circular portion shown in FIG. 4A. FIG. 5A is a diagram showing the edge angle and arithmetic average roughness of the scribing wheel before and after polishing according to Example 1 and Comparative Example 1. FIG. 5B is a diagram showing the edge angle and arithmetic average roughness of the scribing wheel before and after polishing according to Example 2 and Comparative Example 2. FIG. 5C is a diagram showing the edge angle and arithmetic average roughness of the scribing wheel before and after polishing according to Example 3 and Comparative Example 3.

  FIG. 1A is a front view of a scribing wheel according to the first embodiment of the present invention, and FIG. 1B is a side view thereof. When manufacturing a scribing wheel, for example, a through-hole 12 serving as an axial hole is first formed in the center of a disc 11 serving as a cemented carbide or ceramic scribing wheel base as shown in FIG. 1A. Next, a shaft such as a motor (not shown) is connected to the through hole 12 to rotate the central axis of the through hole 12 as the rotation shaft 12a, and the entire circumference of the disk 11 is connected to the rotation shaft 12a from both sides of the disk. On the other hand, it is slanted and formed into a vertical V-shape as shown in FIG. 1B. The V-shaped slope formed in this way is defined as a polishing surface 13.

  Next, formation of the diamond thin film formed on the polished surface 13 will be described. First, the V-shaped polished surface 13 is roughened in advance so that the diamond film can be easily attached. Next, the scribing wheel base material 11 is maintained at a predetermined temperature, pressure, atmosphere, etc., and a diamond nucleus 20 is generated on the surface of the polished surface as shown in an enlarged cross-sectional view in the vicinity of the edge line of the blade edge in FIG. This nucleus is made of single crystal diamond or agglomerated single crystal diamond, and has an outer diameter of, for example, several nm to several tens of nm. Then, the diamond nuclei 20 are grown by chemical vapor deposition (CVD) to form a diamond thin film as shown in FIG. In this growth, the average particle diameter of diamond is 2 μm or less, preferably 1 μm or less. The film thickness is, for example, 10 to 30 μm. When the film thickness exceeds 30 μm, the diamond film is easily peeled off during film formation, and when it is less than 10 μm, the film thickness after polishing becomes too thin.

  Note that a necessary film thickness may be obtained by repeating the above film formation a plurality of times. Specifically, the diamond nucleus 20 is first grown by chemical vapor deposition (CVD) to form a diamond thin film having a thickness of 2 μm, for example, as shown in FIG. Then, again with the same temperature, pressure, atmosphere, etc., as shown in FIG. 2C, diamond nuclei 20 are generated on the surface of the diamond thin film. Then, as shown in FIG. 2 (d), diamond nuclei are grown under the same conditions until the average grain size of the diamond is 2 μm or less, preferably 1 μm or less. Thus, by repeating the deposition of the diamond nuclei and the crystal growth a plurality of times, a plurality of films of two or more layers, for example, a multilayer film of ten layers can be formed as shown in FIG.

  In this manner, as shown in FIG. 3A, a diamond film 14 having an average particle diameter of 2 μm or less, preferably 1 μm or less can be formed on the polished surface 13.

  Thereafter, at least the tip portion is polished so that the tip is sharp. FIG. 3B is a partially enlarged sectional view showing the state after the polishing. Here, the polishing may be performed in two stages of rough polishing and final polishing, and may have an obtuse angle of, for example, about 5 ° with respect to the original diamond film 14. Then, the surface including the circle composed of the ridge line after polishing is set to be perpendicular to the rotation axis 12a. Here, the region to be polished may be only a belt-like portion including the ridge line in the center. The region of the width w of polishing in FIG. 3B shows this tip portion, that is, the polishing region of the diamond film on both sides of the ridgeline. For example, the value of the width w is 10 to 30 μm. When the diamond film having the above-described film thickness is polished in this way, the thickness d of the thinnest portion near the ridge line of the diamond film 14 becomes, for example, 5 μm to 25 μm. If the thickness d is small, the diamond film may be peeled off during scribing, and if it is too large, there is a problem that it is easily cracked by internal stress. Further, when a diamond film is formed a plurality of times to form a multi-layered diamond film, if the polishing amount is large, the surface of the blade edge after polishing may be non-uniform due to the discontinuity of the layer. For this reason, when polishing a diamond film having a multilayer structure, it is preferable to perform polishing so that the surface of the blade edge is uniform, for example, by reducing the polishing amount.

  The scribing wheel is polished by an abrasive such as a grindstone. One inclined surface of the diamond film formed on the cutting edge of the scribing wheel is subjected to rough polishing or finish polishing with a grindstone. By processing with a grindstone, it becomes easy to grind the inclined surface at the same angle over the entire circumference of the scribing wheel. In the polishing step, polishing is performed until the arithmetic average roughness Ra of the surface after polishing becomes 0.03 μm or less, preferably 0.015 μm or less. Further, it is preferable to polish until the arithmetic average roughness Ra of the ridge line is 0.03 μm or less, preferably 0.015 μm or less. In the present invention, by setting the particle diameter of the diamond film 14 to 2 μm or less, polishing can be easily performed so that the arithmetic average roughness Ra of the surface after polishing is 0.03 μm or less, preferably 0.015 μm or less. .

  By polishing in this way, the average roughness of the diamond film in contact with the brittle material substrate is smaller than that of a conventional scribing wheel made of sintered diamond, so that the roughness of the edge portion and the edge line can be made fine. Therefore, by scribing and dividing a brittle material substrate, for example, a ceramic substrate, using this scribing wheel, the accuracy of the end face of the cut surface of the brittle material substrate is improved, and the end face strength can be improved accordingly. . By reducing the roughness of the cutting edge and the ridgeline, an effect that the diamond film is difficult to peel can be obtained. Therefore, the scribing wheel of the present invention is suitable for scribing a ceramic substrate.

  Next, a second embodiment of the present invention will be described. Japanese Patent No. 3074143 proposes a scribing wheel in which a large number of grooves are formed at predetermined intervals on the circumferential surface of the scribing wheel, and a high penetration type is formed with protrusions therebetween. The present invention can also be applied to such a scribing wheel. 4A is a front view of the scribing wheel of this embodiment, FIG. 4B is an enlarged cross-sectional view of the previous ridge line portion, and FIG. 4C is an enlarged view of the circular portion indicated by the one-dot chain line in FIG. 4A. When manufacturing a scribing wheel, first, a through hole 42 serving as a shaft hole is formed in the center of a disc 41 serving as a scribing wheel base material made of cemented carbide or ceramic as shown in FIG. 4A. Next, a shaft such as a motor is communicated with the through hole 42 and rotated around the central axis, and the entire circumference of the disc 41 is polished from both sides to form a V shape. The V-shaped slope formed in this way is defined as a polishing surface 43. Also in this case, the multi-layer diamond film 44 is coated by repeating the CVD method on the cutting edge portion of the scribing wheel as in the first embodiment, and polished by the method described above. When the diamond film 44 is 20 μm, the groove 45 is formed within the thickness range of the diamond film 44 as shown in FIG. 4C. Since the depth of the groove of the scribing wheel for achieving the high penetration type is, for example, about 10 μm, the groove 45 is formed in the diamond film 44 to obtain a high penetration type scribing wheel.

  Alternatively, a scribing wheel may be formed by forming a groove in a V-shaped cutting edge portion of the scribing wheel in advance, and coating and polishing this scribing wheel with a diamond film by a CVD method.

  The state before polishing of the scribing wheel according to the example and the state after polishing will be described in comparison with a comparative example. In both the examples and comparative examples, a cemented carbide scribing wheel substrate having an outer diameter of 2 mm is used. The scribing wheels of Examples 1, 2, and 3 are formed by forming a diamond film having a particle size of 2 μm or less by the chemical vapor deposition method according to the first embodiment. A larger diamond film having a diameter of about 5 μm is formed. In both Example 1 and Comparative Example 1, the cutting edge angle before polishing was 110 °, and in rough polishing, polishing was performed using a No. 8000 abrasive so that the cutting edge angle became 115 ° after completion of rough polishing. Then, polishing was performed using a No. 15000 abrasive so as to be 120 ° after finishing polishing. The thickness d of the thinnest part near the ridgeline of the diamond film 14 is set to 20 μm, for example. For these two examples, the arithmetic average roughness Ra on the inclined surface on the ridge line portion and on the line parallel to the ridge line a certain distance from the ridge line portion is shown in FIG. 5A.

  In Example 2 and Comparative Example 2, the blade edge angle before polishing is 125 °, so that it is 130 ° after rough polishing using No. 8000 abrasive and 135 ° after final polishing using No. 15000 abrasive. Polished. For these two examples, the arithmetic average roughness Ra on the inclined surface on the ridge line portion and the line parallel to the ridge line a certain distance from the ridge line portion is shown in FIG. 5B.

  In each of Example 3 and Comparative Example 3, the blade edge angle is 140 ° before polishing, and is 145 ° after rough polishing using No. 8000 abrasive and 150 ° after final polishing using No. 15000 abrasive. So that it is polished. For these two examples, the arithmetic average roughness Ra on the inclined surface on the ridge line portion and the line parallel to the ridge line a certain distance from the ridge line portion was as shown in FIG. 5C.

  In Examples 1 to 3 and Comparative Examples 1 to 3, the polishing process was possible without chipping the surface during polishing. In Examples 1 to 3, the arithmetic average roughness is smaller than in Examples 1 to 3. This is considered to be because the grain size increases due to the growth of diamond, and therefore the average roughness also increases. And even if rough polishing and finish polishing are performed, all of Examples 1 to 3 have a better finished state than the comparative example of coarse grains, and the arithmetic average roughness of Examples 1 to 3 is the maximum of the inclined surface of Example 1. It was 0.015 μm. Further, in the scribing wheels of Examples 1 to 3, there were some scribing wheels having an arithmetic average roughness of 0.015 μm or less at the stage of rough polishing. Therefore, when a scribing wheel is manufactured by polishing a diamond film having a particle size of 2 μm or less, the polishing process can be simplified. In addition, when finishing polishing similar to that of a diamond film having a large particle size, the arithmetic average roughness of the surface can be made smaller, so the end face of the brittle material substrate cut after scribing using this scribing wheel The accuracy can be further improved.

  The scribing wheel of the present invention can provide a scribing wheel that can cut a brittle material substrate having high wear resistance and peeling resistance and high end face strength, and can be suitably used for a scribing apparatus.

DESCRIPTION OF SYMBOLS 10,40 Scribing wheel 11,41 Disk 12,42 Through-hole 13,43 Polishing surface 14,44 Diamond film 16 Circumferential surface 20 Diamond nucleus 45 Groove

Claims (5)

A method of manufacturing a scribing wheel, in which a ridge line is formed along a circumferential portion of a disc, and the ridge line has a cutting edge made of inclined surfaces on both sides of the ridge line,
A blade-shaped scribing wheel base material is formed by cutting and grinding from both sides along the circumference of the disc-shaped scribing wheel base material to form a cutting edge portion composed of a slope and a ridgeline.
Diamond nuclei are generated at the cutting edge portion of the scribing wheel base material, and a diamond film made of diamond particles having an average particle size of 2 μm or less is grown by chemical vapor deposition to form a diamond film,
The surface including the circle formed by the ridgeline of the diamond film is perpendicular to the rotation axis of the scribing wheel base material , and the difference between the blade edge angle after polishing the diamond film and the blade edge angle before polishing is 5 to 10 °. The manufacturing method of the scribing wheel which grind | polished so that it might become and set the film thickness of the edge line vicinity after grinding | polishing to 5-25 micrometers.   Diamond nuclei are generated at the cutting edge portion of the scribing wheel base material, a diamond layer is grown by chemical vapor deposition, new diamond nuclei are generated on the surface of the diamond layer, and the new diamond layer is chemically vaporized. The method of manufacturing a scribing wheel according to claim 1, wherein the diamond film is formed by repeating the growth by a phase growth method a plurality of times.   The manufacturing method of the scribing wheel of Claim 1 which formed the groove | channel notched by the predetermined interval in the ridgeline part of the said grinding | polishing area | region, and made the space | interval between it. The method of manufacturing a scribing wheel according to claim 1, wherein the arithmetic average roughness Ra of the surface of the diamond film after polishing is 0.03 µm or less. The method of manufacturing a scribing wheel according to claim 1, wherein the edge angle after polishing the diamond film is 115 to 150 °.