JP2015504410A5 - - Google Patents
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- Publication number
- JP2015504410A5 JP2015504410A5 JP2014543843A JP2014543843A JP2015504410A5 JP 2015504410 A5 JP2015504410 A5 JP 2015504410A5 JP 2014543843 A JP2014543843 A JP 2014543843A JP 2014543843 A JP2014543843 A JP 2014543843A JP 2015504410 A5 JP2015504410 A5 JP 2015504410A5
- Authority
- JP
- Japan
- Prior art keywords
- microparticles
- precursor
- silica
- porous
- silica particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 37
- 238000000034 method Methods 0.000 claims description 34
- 239000011859 microparticle Substances 0.000 claims description 13
- 239000000377 silicon dioxide Substances 0.000 claims description 13
- 239000002243 precursor Substances 0.000 claims description 12
- 239000002245 particle Substances 0.000 claims description 10
- 239000002105 nanoparticle Substances 0.000 claims description 8
- 239000004094 surface-active agent Substances 0.000 claims description 8
- 238000009833 condensation Methods 0.000 claims description 7
- 230000005494 condensation Effects 0.000 claims description 7
- 230000007062 hydrolysis Effects 0.000 claims description 7
- 238000006460 hydrolysis reaction Methods 0.000 claims description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims description 4
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 claims description 4
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 claims description 4
- 238000002296 dynamic light scattering Methods 0.000 claims description 4
- 125000000524 functional group Chemical group 0.000 claims description 4
- 229920001477 hydrophilic polymer Polymers 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 4
- 125000001453 quaternary ammonium group Chemical group 0.000 claims description 4
- TXDNPSYEJHXKMK-UHFFFAOYSA-N sulfanylsilane Chemical compound S[SiH3] TXDNPSYEJHXKMK-UHFFFAOYSA-N 0.000 claims description 4
- 230000005526 G1 to G0 transition Effects 0.000 claims description 3
- 239000002356 single layer Substances 0.000 claims description 3
- 239000003381 stabilizer Substances 0.000 claims description 3
- UUEWCQRISZBELL-UHFFFAOYSA-N 3-trimethoxysilylpropane-1-thiol Chemical compound CO[Si](OC)(OC)CCCS UUEWCQRISZBELL-UHFFFAOYSA-N 0.000 claims description 2
- 238000001354 calcination Methods 0.000 claims description 2
- 238000004811 liquid chromatography Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 238000005580 one pot reaction Methods 0.000 claims description 2
- 125000003396 thiol group Chemical group [H]S* 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 238000003775 Density Functional Theory Methods 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1120665.3 | 2011-12-01 | ||
| GB1120665.3A GB2497105B (en) | 2011-12-01 | 2011-12-01 | Process for the preparation of porous silica particles |
| PCT/EP2012/073405 WO2013079396A1 (en) | 2011-12-01 | 2012-11-22 | Porous particles for liquid chromatography and processes for the preparation thereof |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015504410A JP2015504410A (ja) | 2015-02-12 |
| JP2015504410A5 true JP2015504410A5 (enExample) | 2015-11-19 |
| JP6122438B2 JP6122438B2 (ja) | 2017-04-26 |
Family
ID=45508991
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014543843A Active JP6122438B2 (ja) | 2011-12-01 | 2012-11-22 | 液体クロマトグラフィ用の多孔質粒子およびその調製方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US10493428B2 (enExample) |
| EP (1) | EP2785641B1 (enExample) |
| JP (1) | JP6122438B2 (enExample) |
| CN (1) | CN104010970B (enExample) |
| GB (1) | GB2497105B (enExample) |
| WO (1) | WO2013079396A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10434496B2 (en) | 2016-03-29 | 2019-10-08 | Agilent Technologies, Inc. | Superficially porous particles with dual pore structure and methods for making the same |
| CN112262105B (zh) * | 2018-06-15 | 2023-08-11 | 国立大学法人东北大学 | 核壳型多孔质二氧化硅粒子的制造方法 |
| CN113597416A (zh) * | 2019-03-12 | 2021-11-02 | 巴斯夫欧洲公司 | 成型人造聚合物制品 |
| JP7686006B2 (ja) * | 2020-03-20 | 2025-05-30 | レステック・コーポレーション | スパイク粒子、表面多孔質スパイク粒子、クロマトグラフィー分離装置、およびスパイク粒子を形成するための方法 |
| JP7507968B2 (ja) * | 2020-09-11 | 2024-06-28 | ダブリュ．エル．ゴア アンド アソシエイツ，インコーポレイティド | 熱処理フィブリル化ポリマー膜を含むアフィニティークロマトグラフィーデバイス及びそれを含むマニホールド |
| CN112852188B (zh) * | 2020-12-28 | 2022-09-30 | 广东彤泰新材料科技有限公司 | 一种填料组合物 |
| KR102635292B1 (ko) * | 2021-08-26 | 2024-02-08 | 경희대학교 산학협력단 | 공극 구조 세라믹 나노 입자, 공극 구조 세라믹 나노 입자-탄소 동소체 복합체 및 이들의 제조방법 |
| KR102693133B1 (ko) * | 2021-09-01 | 2024-08-09 | 경희대학교 산학협력단 | 공극 구조의 세라믹 나노 입자-탄소 동소체 복합체를 이용한 리튬 이차전지의 음극 및 이의 제조방법 |
| CN113929128B (zh) * | 2021-10-27 | 2023-06-23 | 烟台佳隆纳米产业有限公司 | CuO@SiO2纳米复合材料的制备方法 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3505785A (en) | 1967-06-20 | 1970-04-14 | Du Pont | Superficially porous supports for chromatography |
| EP1991203A2 (en) * | 2006-02-13 | 2008-11-19 | Advanced Materials Technology, Inc. | Porous microparticles solid cores |
| US20100116743A1 (en) | 2007-06-04 | 2010-05-13 | James Neil Pryor | Silica particles and methods of making and using the same |
| US8685283B2 (en) * | 2008-08-29 | 2014-04-01 | Agilent Technologies, Inc. | Superficially porous metal oxide particles, methods for making them, and separation devices using them |
| US9080056B2 (en) * | 2008-11-26 | 2015-07-14 | University College Cork—National University of Ireland, Cork | Process for preparing silica microparticles |
| US7846337B2 (en) * | 2009-02-17 | 2010-12-07 | Agilent Technologies, Inc. | Superficially porous particles and methods of making and using same |
| CN101961639A (zh) | 2009-07-23 | 2011-02-02 | 中国科学院兰州化学物理研究所 | 二氧化硅核壳型液相色谱填料的制备方法 |
| CN102070148B (zh) | 2009-11-23 | 2012-11-07 | 哈尔滨理工大学 | 单分散微米级球状介孔氧化硅mcm-41合成方法及应用 |
| JP6199184B2 (ja) | 2010-07-26 | 2017-09-20 | ウオーターズ・テクノロジーズ・コーポレイシヨン | 粒度分布の狭い実質的に非多孔質のコアを含む表面多孔質材料、その製造方法及びクロマトグラフィー分離用としてのその使用 |
-
2011
- 2011-12-01 GB GB1120665.3A patent/GB2497105B/en active Active
-
2012
- 2012-11-22 WO PCT/EP2012/073405 patent/WO2013079396A1/en not_active Ceased
- 2012-11-22 CN CN201280059128.4A patent/CN104010970B/zh active Active
- 2012-11-22 EP EP12794688.7A patent/EP2785641B1/en active Active
- 2012-11-22 US US14/361,768 patent/US10493428B2/en active Active
- 2012-11-22 JP JP2014543843A patent/JP6122438B2/ja active Active
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