JP2012502139A - 過塩基性カルボン酸金属塩複合グリースおよび製造方法 - Google Patents
過塩基性カルボン酸金属塩複合グリースおよび製造方法 Download PDFInfo
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- JP2012502139A JP2012502139A JP2011526071A JP2011526071A JP2012502139A JP 2012502139 A JP2012502139 A JP 2012502139A JP 2011526071 A JP2011526071 A JP 2011526071A JP 2011526071 A JP2011526071 A JP 2011526071A JP 2012502139 A JP2012502139 A JP 2012502139A
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- Prior art keywords
- grease
- acid
- alkaline earth
- earth metal
- overbased
- Prior art date
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- -1 carboxylic acid alkaline earth metal salt Chemical class 0.000 claims abstract description 77
- 239000002131 composite material Substances 0.000 claims abstract description 73
- 239000002243 precursor Substances 0.000 claims abstract description 61
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims abstract description 60
- 239000008139 complexing agent Substances 0.000 claims abstract description 58
- 238000006243 chemical reaction Methods 0.000 claims abstract description 51
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 36
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- 150000004665 fatty acids Chemical class 0.000 claims abstract description 35
- 150000001342 alkaline earth metals Chemical class 0.000 claims abstract description 18
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- ZCZLQYAECBEUBH-UHFFFAOYSA-L calcium;octadec-9-enoate Chemical group [Ca+2].CCCCCCCCC=CCCCCCCCC([O-])=O.CCCCCCCCC=CCCCCCCCC([O-])=O ZCZLQYAECBEUBH-UHFFFAOYSA-L 0.000 claims description 65
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- 239000011777 magnesium Substances 0.000 claims description 4
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- RXPKHKBYUIHIGL-UHFFFAOYSA-L calcium;12-hydroxyoctadecanoate Chemical group [Ca+2].CCCCCCC(O)CCCCCCCCCCC([O-])=O.CCCCCCC(O)CCCCCCCCCCC([O-])=O RXPKHKBYUIHIGL-UHFFFAOYSA-L 0.000 description 12
- 230000008569 process Effects 0.000 description 12
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- YAQXGBBDJYBXKL-UHFFFAOYSA-N iron(2+);1,10-phenanthroline;dicyanide Chemical compound [Fe+2].N#[C-].N#[C-].C1=CN=C2C3=NC=CC=C3C=CC2=C1.C1=CN=C2C3=NC=CC=C3C=CC2=C1 YAQXGBBDJYBXKL-UHFFFAOYSA-N 0.000 description 1
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- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 150000004692 metal hydroxides Chemical class 0.000 description 1
- 229910052976 metal sulfide Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000021281 monounsaturated fatty acids Nutrition 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229960002446 octanoic acid Drugs 0.000 description 1
- 229940049964 oleate Drugs 0.000 description 1
- 229960002969 oleic acid Drugs 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- VGTPKLINSHNZRD-UHFFFAOYSA-N oxoborinic acid Chemical compound OB=O VGTPKLINSHNZRD-UHFFFAOYSA-N 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 150000003017 phosphorus Chemical class 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 235000015096 spirit Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229960004274 stearic acid Drugs 0.000 description 1
- 150000004763 sulfides Chemical class 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- VLCLHFYFMCKBRP-UHFFFAOYSA-N tricalcium;diborate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]B([O-])[O-].[O-]B([O-])[O-] VLCLHFYFMCKBRP-UHFFFAOYSA-N 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M117/00—Lubricating compositions characterised by the thickener being a non-macromolecular carboxylic acid or salt thereof
- C10M117/02—Lubricating compositions characterised by the thickener being a non-macromolecular carboxylic acid or salt thereof having only one carboxyl group bound to an acyclic carbon atom, cycloaliphatic carbon atom or hydrogen
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M121/00—Lubricating compositions characterised by the thickener being a compound of unknown or incompletely defined constitution
- C10M121/04—Reaction products
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/26—Overbased carboxylic acid salts
- C10M2207/2613—Overbased carboxylic acid salts used as thickening agents
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/08—Resistance to extreme temperature
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/26—Waterproofing or water resistance
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/40—Low content or no content compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/62—Food grade properties
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/74—Noack Volatility
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/10—Semi-solids; greasy
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US9459808P | 2008-09-05 | 2008-09-05 | |
| US61/094,598 | 2008-09-05 | ||
| PCT/US2009/041378 WO2010027532A1 (en) | 2008-09-05 | 2009-04-22 | Overbased metal carboxylate complex grease and process for making |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JP2012502139A true JP2012502139A (ja) | 2012-01-26 |
Family
ID=41797394
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011526071A Pending JP2012502139A (ja) | 2008-09-05 | 2009-04-22 | 過塩基性カルボン酸金属塩複合グリースおよび製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20110092404A1 (es) |
| EP (1) | EP2344612A4 (es) |
| JP (1) | JP2012502139A (es) |
| KR (1) | KR20110059561A (es) |
| CN (1) | CN102015983A (es) |
| CA (1) | CA2722005A1 (es) |
| MX (1) | MX2010011509A (es) |
| RU (1) | RU2010142947A (es) |
| WO (1) | WO2010027532A1 (es) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110234745A (zh) * | 2016-12-21 | 2019-09-13 | 福斯油品集团 | 复合钙基润滑脂和复合磺酸钙基润滑脂在钢丝绳润滑中的应用 |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9976102B2 (en) | 2011-10-31 | 2018-05-22 | Nch Corporation | Composition and method of manufacturing calcium sulfonate greases using alkali metal hydroxide and delayed addition of non-aqueous converting agents |
| US9976101B2 (en) | 2011-10-31 | 2018-05-22 | Nch Corporation | Method of manufacturing calcium sulfonate greases using delayed addition of non-aqueous converting agents |
| EP2773589B1 (en) * | 2011-10-31 | 2019-03-13 | NCH Corporation | Calcium hydroxyapatite based calcium sulfonate grease compositions and method of manufacture |
| US9458406B2 (en) | 2011-10-31 | 2016-10-04 | Nch Corporation | Calcium hydroxyapatite based sulfonate grease compositions and method of manufacture |
| CN104560282B (zh) * | 2013-10-25 | 2017-03-01 | 中国石油化工股份有限公司 | 磺酸盐、其制备方法及包含该磺酸盐的润滑脂及其制备方法 |
| FR3013056B1 (fr) * | 2013-11-13 | 2018-01-19 | Total Marketing Services | Procede de preparation d'une graisse sulfonate de calcium complexe |
| US10392577B2 (en) | 2016-05-18 | 2019-08-27 | Nch Corporation | Composition and method of manufacturing overbased sulfonate modified lithium carboxylate grease |
| US10087387B2 (en) | 2016-05-18 | 2018-10-02 | Nch Corporation | Composition and method of manufacturing calcium magnesium sulfonate greases |
| US10087388B2 (en) | 2016-05-18 | 2018-10-02 | Nch Corporation | Composition and method of manufacturing calcium sulfonate and calcium magnesium sulfonate greases using a delay after addition of facilitating acid |
| US10087391B2 (en) | 2016-05-18 | 2018-10-02 | Nch Corporation | Composition and method of manufacturing calcium magnesium sulfonate greases without a conventional non-aqueous converting agent |
| US10519393B2 (en) | 2016-05-18 | 2019-12-31 | Nch Corporation | Composition and method of manufacturing calcium magnesium sulfonate greases |
| US11078438B2 (en) * | 2017-07-24 | 2021-08-03 | Chemtool Incorporated | Extreme pressure metal sulfonate grease |
| US11661563B2 (en) | 2020-02-11 | 2023-05-30 | Nch Corporation | Composition and method of manufacturing and using extremely rheopectic sulfonate-based greases |
| CN114806688A (zh) * | 2022-04-25 | 2022-07-29 | 宝鸡文理学院 | 一种工业机器人用复合磺酸钙基润滑脂及其制备方法 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3466245A (en) * | 1967-07-31 | 1969-09-09 | Gulf Research Development Co | Method of preparing calcium soap-calcium salt greases |
| CA949055A (en) * | 1968-05-08 | 1974-06-11 | Continental Oil Company | Method for preparing highly basic grease and rust inhibiting compositions |
| US4253976A (en) * | 1979-02-21 | 1981-03-03 | The Lubrizol Corporation | Magnesium oxide-carboxylate complexes, method for their preparation, and compositions containing the same |
| US5919741A (en) * | 1998-01-20 | 1999-07-06 | The Lubrizol Corporation | Overbased carboxylate gels |
| US6100226A (en) * | 1998-05-20 | 2000-08-08 | The Lubrizol Corporation | Simple metal grease compositions |
| JP3948642B2 (ja) * | 1998-08-21 | 2007-07-25 | 信越化学工業株式会社 | 熱伝導性グリース組成物及びそれを使用した半導体装置 |
| JP2000169873A (ja) * | 1998-12-02 | 2000-06-20 | Shin Etsu Chem Co Ltd | シリコーングリース組成物 |
| US6063742A (en) * | 1999-03-01 | 2000-05-16 | The Lubrizol Corporation | Grease compositions |
| US6495494B1 (en) * | 2000-06-16 | 2002-12-17 | Ecolab Inc. | Conveyor lubricant and method for transporting articles on a conveyor system |
| CN1126807C (zh) * | 2000-07-19 | 2003-11-05 | 中国石油天然气股份有限公司兰州炼化分公司 | 一种复合型超高碱值金属清净剂的制备方法 |
| US7163912B2 (en) * | 2001-05-18 | 2007-01-16 | Omg Americas, Inc. | Lubricant compositions containing an overbased amorphous alkaline earth metal salt as a metal protectant |
| US20060194704A1 (en) * | 2003-07-11 | 2006-08-31 | Akzo Nobel N.V. | Highly over-based light colored liquid alkaline earth metal carboxylate |
| US7407920B2 (en) * | 2004-07-29 | 2008-08-05 | Crompton Corporation | Overbased calcium salicylate greases |
| US7422999B2 (en) * | 2005-02-14 | 2008-09-09 | The Lubrizol Corporation | Overbased vaterite containing salt composition |
| US20080274923A1 (en) * | 2007-05-01 | 2008-11-06 | Omg Americas, Inc. | Overbased metal carboxylate calcite-containing greases |
| CN101153239B (zh) * | 2007-08-27 | 2010-12-01 | 无锡市高润杰化学有限公司 | 一种复合磺酸钙基润滑脂的生产方法 |
| US20090264327A1 (en) * | 2008-04-21 | 2009-10-22 | Omg Americas, Inc. | Overbased metal carboxylate precursor and process for making |
| DE102008034959A1 (de) * | 2008-07-25 | 2010-01-28 | Fuchs Petrolub Ag | Calcium/Lithium-Komplexfette und gekapseltes Gleichlaufgelenk enthaltend diese sowie deren Anwendung |
-
2009
- 2009-04-22 KR KR1020107019934A patent/KR20110059561A/ko not_active Application Discontinuation
- 2009-04-22 JP JP2011526071A patent/JP2012502139A/ja active Pending
- 2009-04-22 MX MX2010011509A patent/MX2010011509A/es unknown
- 2009-04-22 US US12/995,680 patent/US20110092404A1/en not_active Abandoned
- 2009-04-22 WO PCT/US2009/041378 patent/WO2010027532A1/en active Application Filing
- 2009-04-22 EP EP09811873A patent/EP2344612A4/en not_active Withdrawn
- 2009-04-22 CN CN2009801140092A patent/CN102015983A/zh active Pending
- 2009-04-22 CA CA2722005A patent/CA2722005A1/en not_active Abandoned
- 2009-04-22 RU RU2010142947/04A patent/RU2010142947A/ru not_active Application Discontinuation
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110234745A (zh) * | 2016-12-21 | 2019-09-13 | 福斯油品集团 | 复合钙基润滑脂和复合磺酸钙基润滑脂在钢丝绳润滑中的应用 |
| JP2020514452A (ja) * | 2016-12-21 | 2020-05-21 | フックス ペイトロルブ エスエー | カルシウム複合潤滑グリースの使用及びワイヤーロープの潤滑のためのカルシウムスルホネート複合潤滑グリース |
| JP7007383B2 (ja) | 2016-12-21 | 2022-02-10 | フックス ペイトロルブ エスエー | カルシウム複合潤滑グリースの使用及びワイヤーロープの潤滑のためのカルシウムスルホネート複合潤滑グリース |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20110059561A (ko) | 2011-06-02 |
| EP2344612A4 (en) | 2012-08-29 |
| WO2010027532A1 (en) | 2010-03-11 |
| US20110092404A1 (en) | 2011-04-21 |
| CN102015983A (zh) | 2011-04-13 |
| RU2010142947A (ru) | 2012-04-27 |
| EP2344612A1 (en) | 2011-07-20 |
| MX2010011509A (es) | 2011-03-04 |
| CA2722005A1 (en) | 2010-03-11 |
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