JP2012500238A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2012500238A5 JP2012500238A5 JP2011523343A JP2011523343A JP2012500238A5 JP 2012500238 A5 JP2012500238 A5 JP 2012500238A5 JP 2011523343 A JP2011523343 A JP 2011523343A JP 2011523343 A JP2011523343 A JP 2011523343A JP 2012500238 A5 JP2012500238 A5 JP 2012500238A5
- Authority
- JP
- Japan
- Prior art keywords
- amount
- alcohols
- minutes
- reaction
- alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 14
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical class CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical class CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 150000001412 amines Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000010533 azeotropic distillation Methods 0.000 description 2
- -1 dicarboxylic acid diester Chemical class 0.000 description 2
- 150000005690 diesters Chemical group 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000013067 intermediate product Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- CSDSSGBPEUDDEE-UHFFFAOYSA-N 2-formylpyridine Chemical compound O=CC1=CC=CC=N1 CSDSSGBPEUDDEE-UHFFFAOYSA-N 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- XUWHAWMETYGRKB-UHFFFAOYSA-N piperidin-2-one Chemical compound O=C1CCCCN1 XUWHAWMETYGRKB-UHFFFAOYSA-N 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008038376.7 | 2008-08-19 | ||
| DE102008038376A DE102008038376A1 (de) | 2008-08-19 | 2008-08-19 | Verfahren zur Herstellung von 3,7-Diaza-bicyclo[3.3.1]nonan-Verbindungen |
| PCT/EP2009/005937 WO2010020383A1 (de) | 2008-08-19 | 2009-08-17 | Verfarhen zur herstellung von 3,7-diaza-bicyclo[3.3.1]nonan-verbindungen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012500238A JP2012500238A (ja) | 2012-01-05 |
| JP2012500238A5 true JP2012500238A5 (enExample) | 2013-10-31 |
| JP5592370B2 JP5592370B2 (ja) | 2014-09-17 |
Family
ID=41278731
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011523343A Active JP5592370B2 (ja) | 2008-08-19 | 2009-08-17 | ３，７−ジアザ−ビシクロ［３．３．１］ノナン化合物の製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8293910B2 (enExample) |
| EP (1) | EP2318409B1 (enExample) |
| JP (1) | JP5592370B2 (enExample) |
| DE (1) | DE102008038376A1 (enExample) |
| ES (1) | ES2388622T3 (enExample) |
| WO (1) | WO2010020383A1 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102005027619A1 (de) * | 2005-06-15 | 2006-12-28 | Clariant Produkte (Deutschland) Gmbh | Verfahren zur Herstellung von 3,7-Diaza-bicyclo[3.3.1]nonan-Verbindungen |
| DE102008045207A1 (de) * | 2008-08-30 | 2010-03-04 | Clariant International Limited | Bleichkatalysatormischungen bestehend aus Mangansalzen und Oxalsäure oder deren Salze |
| DE102008064009A1 (de) | 2008-12-19 | 2010-06-24 | Clariant International Ltd. | Verfahren zur Herstellung von 3,7-Diaza-bicyclo[3.3.1]nonan-Metall-Komplexen |
| CN102875550B (zh) * | 2011-07-12 | 2016-01-06 | 常州合全药业有限公司 | 1,3,7-三取代-3,7-二氮杂双环[3,3,1]壬烷衍生物及制备方法 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1182143A (en) * | 1966-03-01 | 1970-02-25 | United States Borax Chem | Bleaching Compositions and Methods. |
| US4414127A (en) * | 1981-07-06 | 1983-11-08 | Syntex (U.S.A.) Inc. | Contact lens cleaning solutions |
| GR76237B (enExample) | 1981-08-08 | 1984-08-04 | Procter & Gamble | |
| US4481129A (en) | 1981-12-23 | 1984-11-06 | Lever Brothers Company | Bleach compositions |
| GB8329762D0 (en) | 1983-11-08 | 1983-12-14 | Unilever Plc | Manganese adjuncts |
| GB8405189D0 (en) | 1984-02-28 | 1984-04-04 | Interox Chemicals Ltd | Peroxide activation |
| US4728455A (en) | 1986-03-07 | 1988-03-01 | Lever Brothers Company | Detergent bleach compositions, bleaching agents and bleach activators |
| BR9507984A (pt) | 1994-06-13 | 1997-11-18 | Unilever Nv | Catalisador de alvejamento e de oxidação e composição alvejante |
| DE4443177A1 (de) | 1994-12-05 | 1996-06-13 | Henkel Kgaa | Aktivatormischungen für anorganische Perverbindungen |
| US6734155B1 (en) * | 1997-07-09 | 2004-05-11 | The Procter & Gamble Company | Cleaning compositions comprising an oxidoreductase |
| CA2248476A1 (en) | 1997-10-01 | 1999-04-01 | Unilever Plc | Bleach activation |
| DE19909546C1 (de) | 1999-03-04 | 2000-06-29 | Consortium Elektrochem Ind | Mehrkomponentensystem zur enzymkatalysierten Oxidation von Substraten sowie Verfahren zur enzymkatalysierten Oxidation |
| GB9930422D0 (en) | 1999-12-22 | 2000-02-16 | Unilever Plc | Bleach catalysts |
| GB0030673D0 (en) | 2000-12-15 | 2001-01-31 | Unilever Plc | Ligand and complex for catalytically bleaching a substrate |
| GB0104980D0 (en) | 2001-02-28 | 2001-04-18 | Unilever Plc | Liquid cleaning compositions and their use |
| CA2472189A1 (en) | 2002-02-28 | 2003-09-04 | Unilever Plc | Bleach catalyst enhancement |
| EP1523482A1 (en) | 2002-06-06 | 2005-04-20 | Unilever N.V. | Ligand and complex for catalytically bleaching a substrate |
| DE10304131A1 (de) | 2003-02-03 | 2004-08-05 | Clariant Gmbh | Verwendung von Übergangsmetallkomplexen als Bleichkatalysatoren |
| DE10345273A1 (de) | 2003-09-30 | 2005-04-21 | Clariant Gmbh | Verwendung von Übergangsmetallkomplexen mit Lactamliganden als Bleichkatalysatoren |
| GB0325432D0 (en) * | 2003-10-31 | 2003-12-03 | Unilever Plc | Ligand and complex for catalytically bleaching a substrate |
| GB0411304D0 (en) | 2004-05-21 | 2004-06-23 | Fellows Adrian N | An antimicrobial composition |
| DE102005027619A1 (de) * | 2005-06-15 | 2006-12-28 | Clariant Produkte (Deutschland) Gmbh | Verfahren zur Herstellung von 3,7-Diaza-bicyclo[3.3.1]nonan-Verbindungen |
| DE102008045207A1 (de) * | 2008-08-30 | 2010-03-04 | Clariant International Limited | Bleichkatalysatormischungen bestehend aus Mangansalzen und Oxalsäure oder deren Salze |
| DE102008045215A1 (de) * | 2008-08-30 | 2010-03-04 | Clariant International Ltd. | Verwendung von Mangan-Oxalatenn als Bleichkatalysatoren |
| DE102008064009A1 (de) * | 2008-12-19 | 2010-06-24 | Clariant International Ltd. | Verfahren zur Herstellung von 3,7-Diaza-bicyclo[3.3.1]nonan-Metall-Komplexen |
-
2008
- 2008-08-19 DE DE102008038376A patent/DE102008038376A1/de not_active Withdrawn
-
2009
- 2009-08-17 US US13/059,470 patent/US8293910B2/en active Active
- 2009-08-17 WO PCT/EP2009/005937 patent/WO2010020383A1/de not_active Ceased
- 2009-08-17 EP EP09777909A patent/EP2318409B1/de active Active
- 2009-08-17 JP JP2011523343A patent/JP5592370B2/ja active Active
- 2009-08-17 ES ES09777909T patent/ES2388622T3/es active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5317701B2 (ja) | ４−（ベンゾイミダゾリルメチルアミノ）−ベンゾアミド及びその塩の改良された製造方法 | |
| CN1972919B (zh) | 制备4-(苯并咪唑基甲氨基)-苯甲脒的方法 | |
| JP5317702B2 (ja) | ４−（ベンゾイミダゾリルメチルアミノ）−ベンゾアミドの塩の改良された製造方法 | |
| CN102344415B (zh) | 阿奇沙坦中间体的制备方法 | |
| JP2015500335A5 (enExample) | ||
| JP2009527501A5 (enExample) | ||
| JP2012515142A5 (enExample) | ||
| JP2009512627A (ja) | ９−ヒドロキシリスペリドン（パリペリドン）の合成方法 | |
| JP2012500238A5 (enExample) | ||
| CN102367253A (zh) | 一种制备他达拉非晶型a的方法 | |
| CN108586379B (zh) | 一种3-氨基呋咱-4-甲酰胺的制备方法 | |
| JP5256029B2 (ja) | ３，７−ジアザ−ビシクロ［３．３．１］ノナン化合物の製造方法 | |
| JP5592370B2 (ja) | ３，７−ジアザ−ビシクロ［３．３．１］ノナン化合物の製造方法 | |
| CZ2007457A3 (cs) | Zpusob výroby 4´ -[[4-methyl-6-(1-methyl-1H-benzimidazol-2-yl)-2-propyl-1H-benzimidazol-1yl]methyl]biphenyl-2-karboxylové kyseliny (telmisartanu) | |
| JP2012524044A (ja) | ２，４，６−オクタトリエン−１−酸及び２，４，６−オクタトリエン−１−オールの調製方法 | |
| RU2012134703A (ru) | Новый полиморф (пмл) гидрохлорида сложного (6-диметиламино метил-2-нафталенил) эфира (4-гидроксикарбамоил-фенил)-карбаминовой кислоты | |
| JP7252978B2 (ja) | ２－（１－（ｔｅｒｔ－ブトキシカルボニル）ピペリジン－４－イル）安息香酸を調製するためのプロセス | |
| CN101921194A (zh) | 一种制备4-氯二苯甲胺的方法 | |
| JP2002519343A (ja) | オキシイミダゾールを調製するための方法 | |
| WO2020038812A1 (en) | New process for the preparation of amenamevir | |
| JP4790901B2 (ja) | ４−アミノ−５−シアノイミダゾール誘導体及びその中間体の製造方法 | |
| JP5064872B2 (ja) | Ｎ−（２−アミノ−１，２−ジシアノビニル）イミデート類の製造方法 | |
| JP2007534737A5 (enExample) | ||
| TWI614256B (zh) | 合成四氫異喹啉噁唑烷的方法 | |
| US20120165527A1 (en) | process for the preparation of pure paliperidone |