JP2012193143A - Cosmetics for eyelashes - Google Patents
Cosmetics for eyelashes Download PDFInfo
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- JP2012193143A JP2012193143A JP2011057864A JP2011057864A JP2012193143A JP 2012193143 A JP2012193143 A JP 2012193143A JP 2011057864 A JP2011057864 A JP 2011057864A JP 2011057864 A JP2011057864 A JP 2011057864A JP 2012193143 A JP2012193143 A JP 2012193143A
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- eyelashes
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- 210000000720 eyelash Anatomy 0.000 title claims abstract description 59
- 239000002537 cosmetic Substances 0.000 title claims abstract description 25
- 235000019693 cherries Nutrition 0.000 claims abstract description 14
- 229940108690 glucosyl hesperidin Drugs 0.000 claims description 10
- 241000167854 Bourreria succulenta Species 0.000 claims 2
- 230000006378 damage Effects 0.000 abstract description 13
- 241001290151 Prunus avium subsp. avium Species 0.000 abstract description 12
- 235000011442 Prunus x yedoensis Nutrition 0.000 abstract description 10
- 241000220307 Prunus yedoensis Species 0.000 abstract description 10
- 238000002156 mixing Methods 0.000 abstract description 9
- 239000003599 detergent Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 33
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
- 210000004209 hair Anatomy 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 239000001100 (2S)-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)chroman-4-one Substances 0.000 description 9
- QUQPHWDTPGMPEX-UHFFFAOYSA-N Hesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(COC4C(C(O)C(O)C(C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-UHFFFAOYSA-N 0.000 description 9
- QUQPHWDTPGMPEX-UTWYECKDSA-N aurantiamarin Natural products COc1ccc(cc1O)[C@H]1CC(=O)c2c(O)cc(O[C@@H]3O[C@H](CO[C@@H]4O[C@@H](C)[C@H](O)[C@@H](O)[C@H]4O)[C@@H](O)[C@H](O)[C@H]3O)cc2O1 QUQPHWDTPGMPEX-UTWYECKDSA-N 0.000 description 9
- APSNPMVGBGZYAJ-GLOOOPAXSA-N clematine Natural products COc1cc(ccc1O)[C@@H]2CC(=O)c3c(O)cc(O[C@@H]4O[C@H](CO[C@H]5O[C@@H](C)[C@H](O)[C@@H](O)[C@H]5O)[C@@H](O)[C@H](O)[C@H]4O)cc3O2 APSNPMVGBGZYAJ-GLOOOPAXSA-N 0.000 description 9
- QUQPHWDTPGMPEX-QJBIFVCTSA-N hesperidin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]4[C@@H]([C@H](O)[C@@H](O)[C@H](C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-QJBIFVCTSA-N 0.000 description 9
- VUYDGVRIQRPHFX-UHFFFAOYSA-N hesperidin Natural products COc1cc(ccc1O)C2CC(=O)c3c(O)cc(OC4OC(COC5OC(O)C(O)C(O)C5O)C(O)C(O)C4O)cc3O2 VUYDGVRIQRPHFX-UHFFFAOYSA-N 0.000 description 9
- 229940025878 hesperidin Drugs 0.000 description 9
- ARGKVCXINMKCAZ-UHFFFAOYSA-N neohesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(CO)O3)OC3C(C(O)C(O)C(C)O3)O)=CC(O)=C2C(=O)C1 ARGKVCXINMKCAZ-UHFFFAOYSA-N 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 229940058015 1,3-butylene glycol Drugs 0.000 description 7
- 235000019437 butane-1,3-diol Nutrition 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- 239000002904 solvent Substances 0.000 description 5
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 3
- 238000013329 compounding Methods 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 3
- 239000008213 purified water Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- QZKRHPLGUJDVAR-UHFFFAOYSA-K EDTA trisodium salt Chemical compound [Na+].[Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O QZKRHPLGUJDVAR-UHFFFAOYSA-K 0.000 description 2
- 241000272185 Falco Species 0.000 description 2
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 2
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 238000005452 bending Methods 0.000 description 2
- 239000007844 bleaching agent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 230000037308 hair color Effects 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 2
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 2
- 229960002216 methylparaben Drugs 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 108090000623 proteins and genes Chemical class 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 150000005846 sugar alcohols Polymers 0.000 description 2
- CLAHOZSYMRNIPY-UHFFFAOYSA-N 2-hydroxyethylurea Chemical compound NC(=O)NCCO CLAHOZSYMRNIPY-UHFFFAOYSA-N 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 241001672694 Citrus reticulata Species 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 description 1
- 235000004789 Rosa xanthina Nutrition 0.000 description 1
- 241000220222 Rosaceae Species 0.000 description 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 229940064004 antiseptic throat preparations Drugs 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 1
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- POLCUAVZOMRGSN-UHFFFAOYSA-N dipropyl ether Chemical compound CCCOCCC POLCUAVZOMRGSN-UHFFFAOYSA-N 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 230000003700 hair damage Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 229940031575 hydroxyethyl urea Drugs 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 150000002772 monosaccharides Chemical class 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000003531 protein hydrolysate Chemical class 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000003021 water soluble solvent Substances 0.000 description 1
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- Cosmetics (AREA)
Abstract
Description
本発明は、サクラエキスを含有することを特徴とするまつ毛用化粧料に関する。より具体的には、サクラエキスを含有することにより、傷んだまつ毛に対し損傷改善、補修効果に優れたまつ毛用化粧料に関する。 The present invention relates to a cosmetic for eyelashes characterized by containing a cherry extract. More specifically, the present invention relates to a cosmetic for eyelashes that contains a cherry extract and is excellent in damage improvement and repair effect on damaged eyelashes.
毛髪については、ヘアカラーやブリーチ、パーマネントウェーブといった化学的な要因、ドライヤーやヘアカーラーによる熱によって損傷することが知られている。そして、このような毛髪損傷を改善、補修する方法として、ヒドロキシエチルウレアと特定のポリマーを配合する方法（特許文献１）、ペプチドと特定の有機溶剤を配合する方法（特許文献２）、Ｃ３からＣ５単糖類及びその誘導体を配合する方法（特許文献３）、有機酸と芳香族カルボン酸を配合する方法（特許文献４）、有機酸とポリプロピレングリコールを配合する方法（特許文献５）、塩基性アミノ酸とタンパク質、タンパク加水分解物、タンパク誘導体を配合する方法（特許文献６）等が知られている。 It is known that hair is damaged by chemical factors such as hair color, bleach, and permanent wave, and heat from a hair dryer or hair curler. And as a method for improving and repairing such hair damage, a method of blending hydroxyethyl urea and a specific polymer (Patent Document 1), a method of blending a peptide and a specific organic solvent (Patent Document 2), from C3 A method of blending C5 monosaccharide and derivatives thereof (Patent Document 3), a method of blending organic acid and aromatic carboxylic acid (Patent Document 4), a method of blending organic acid and polypropylene glycol (Patent Document 5), basic A method of blending amino acid and protein, protein hydrolyzate, protein derivative (Patent Document 6) and the like are known.
一方、近年アイメイクの流行によりマスカラやつけまつ毛を使用する女性が増え、まつ毛に対する関心が非常に高まっている。それとともに、まつ毛の損傷を訴える女性が増えてきている。しかしながら、まつ毛の場合は毛髪と異なり、ヘアカラーやブリーチ、パーマネントウェーブ、ドライヤー、ヘアカーラーによる処理を行う訳ではない。すなわち、まつ毛と毛髪では損傷のメカニズムが異なる。しかしながら、これまでまつ毛の損傷のメカニズムは明らかにされていない。 On the other hand, in recent years, the number of women who use mascara and false eyelashes has increased due to the trend of eye makeup, and interest in eyelashes has increased greatly. Along with this, an increasing number of women complain of eyelash damage. However, in the case of eyelashes, unlike hair, treatment with hair color, bleach, permanent wave, dryer or hair curler is not performed. That is, the mechanism of damage differs between eyelashes and hair. However, the mechanism of eyelash damage has not been clarified so far.
そこで、本発明者らが鋭意研究を行った結果、まつ毛の損傷はビューラーによる折り曲げ、引っ張りやマスカラ使用後のクレンジング剤によるこすり落とし等の物理的要因によって引き起こされることが明らかとなった。しかしながら、上記先行技術では、まつ毛の損傷が改善されるか明らかにされていないのが現状であった。 Thus, as a result of intensive studies by the present inventors, it has been clarified that eyelash damage is caused by physical factors such as bending by a buhler, pulling and rubbing off by a cleansing agent after using mascara. However, in the above prior art, it has not been clarified whether the eyelash damage is improved.
本発明は、傷んだまつ毛に対し損傷改善、補修効果に優れたまつ毛用化粧料を提供することを目的とする。 An object of this invention is to provide the cosmetics for eyelashes which were excellent in damage improvement and the repair effect with respect to the damaged eyelash.
かかる事情に鑑み、本発明者らは鋭意研究を行った結果、サクラエキスにまつ毛損傷の改善、補修効果があることを見出した。さらに、グルコシルヘスペリジンを配合することにより、サクラエキスによるまつ毛損傷の改善、補修効果が向上することを見出し、本発明を完成させた。 In view of such circumstances, as a result of intensive studies, the present inventors have found that the cherry extract has an effect of improving and repairing eyelash damage. Furthermore, the present inventors completed the present invention by finding that blending glucosyl hesperidin improves the eyelash damage caused by the cherry extract and improves the repair effect.
すなわち本発明は、まつ毛損傷の改善、補修効果に優れたまつ毛用化粧料である。 That is, the present invention is a cosmetic for eyelashes that is excellent in improving and repairing eyelash damage.
以下、本発明を詳細に説明する。 Hereinafter, the present invention will be described in detail.
本発明で使用されるサクラエキスは、バラ科に属するソメイヨシノ（学名：Ｐｒｕｎｕｓ Ｙｅｄｏｅｎｓｉｓ）の抽出物であり、市販されている品種又は自生するものを利用することができる。また使用される部位は特に限定されないが葉が好ましい。市販品としては一丸ファルコス社製のサクラエキスＢ（一丸ファルコス社製：ソメイヨシノ葉エキス２％、水４９％、ＢＧ４９％の混合溶液）等が挙げられる。 The cherry extract used in the present invention is an extract of Yoshino cherry tree (scientific name: Prunus Yedoensis) belonging to the Rosaceae family, and commercially available varieties or native ones can be used. Moreover, although the site | part used is not specifically limited, a leaf is preferable. Commercially available products include Ichimaru Falcos Sakura Extract B (Ichimaru Falcos: mixed solution of Yoshino cherry leaf extract 2%, water 49%, BG 49%) and the like.
また、本発明で使用するサクラエキスの抽出法は特に限定されず、例えば、加熱抽出したものであっても良いし、常温又は低温で抽出したものであっても良い。抽出する溶媒としては、例えば、水、低級１価アルコール類（メタノール、エタノール、１−プロパノール、２−プロパノール、１−ブタノール、２−ブタノール等）、液状多価アルコール（１，３−ブチレングリコール、プロピレングリコール等）、炭化水素（ヘキサン、ペンタン等）、ケトン類（アセトン、メチルエチルケトン等）、エーテル類（エチルエーテル、テトラヒドロフラン、プロピルエーテル等）、アセトニトリル等が挙げられる。これらの溶媒は単独で用いても２種以上を混合して用いてもよい。好ましくは、水あるいは水溶性溶媒（水と任意の割合で混合可能な溶媒。例えば、エタノール、１，３−ブチレングリコール、プロピレングリコール等）のうち１種又は２種以上の溶媒を用いるのが良い。抽出物はそのまま用いても良いし、溶媒を一部、又は全部留去して用いても良い。 Moreover, the extraction method of the cherry extract used by this invention is not specifically limited, For example, what was extracted by heating may be used, and what was extracted at normal temperature or low temperature may be used. Examples of the solvent to be extracted include water, lower monohydric alcohols (methanol, ethanol, 1-propanol, 2-propanol, 1-butanol, 2-butanol, etc.), liquid polyhydric alcohols (1,3-butylene glycol, Propylene glycol, etc.), hydrocarbons (hexane, pentane, etc.), ketones (acetone, methyl ethyl ketone, etc.), ethers (ethyl ether, tetrahydrofuran, propyl ether, etc.), acetonitrile and the like. These solvents may be used alone or in combination of two or more. Preferably, one or two or more solvents among water or a water-soluble solvent (solvent that can be mixed with water in an arbitrary ratio. For example, ethanol, 1,3-butylene glycol, propylene glycol, etc.) may be used. . The extract may be used as it is, or a part or all of the solvent may be distilled off.
本発明のまつ毛用化粧料には、上記抽出物をそのまま使用しても良く、必要に応じて、濃縮、希釈及び濾過処理、活性炭等による脱色、脱臭処理等をして用いても良い。更には、抽出した溶液を濃縮乾固、噴霧乾燥、凍結乾燥等の処理を行い、乾燥物として用いても良い。 In the cosmetic for eyelashes of the present invention, the above extract may be used as it is, and may be used after concentration, dilution and filtration treatment, decolorization with activated carbon or the like, deodorization treatment, and the like. Further, the extracted solution may be subjected to a treatment such as concentration to dryness, spray drying, freeze drying, etc., and used as a dried product.
本発明におけるサクラエキスの配合量は特に限定されないが、乾燥物として、０．０００１〜０．１重量％の範囲が好ましい。０．０００１重量％未満では効果が低く、また０．１重量％を超えても効果に増強はみられず、非経済的である。 Although the compounding quantity of the cherry extract in this invention is not specifically limited, The range of 0.0001 to 0.1 weight% is preferable as a dried product. If it is less than 0.0001% by weight, the effect is low, and if it exceeds 0.1% by weight, the effect is not enhanced, which is uneconomical.
本発明においては、さらにグルコシルヘスペリジンを配合することにより、本発明の効果をより高めることができる。グルコシルヘスペリジンは、ミカン等の柑橘類の皮に含まれるポリフェノールの一種のヘスペリジンに糖を結合させた糖転移ヘスペリジンである。 In this invention, the effect of this invention can be heightened more by mix | blending glucosyl hesperidin further. Glucosyl hesperidin is a sugar-transferred hesperidin in which a sugar is bound to a kind of polyphenol hesperidin contained in citrus peels such as mandarin oranges.
グルコシルヘスペリジンの例としては、α−モノグルコシルヘスペリジン、α−ジグルコシルヘスペリジン、α−トリグルコシルヘスペリジン、α−テトラグルコシルヘスペリジン及びα−ペンタグルコシルヘスペリジン等が挙げられる。具体例としては、（株）林原生物化学研究所製の林原ヘスペリジンＳ等が挙げられる。 Examples of glucosyl hesperidin include α-monoglucosyl hesperidin, α-diglucosyl hesperidin, α-triglucosyl hesperidin, α-tetraglucosyl hesperidin, α-pentaglucosyl hesperidin, and the like. Specific examples include Hayashibara Hesperidin S manufactured by Hayashibara Biochemical Research Institute.
本発明におけるグルコシルヘスペリジンの配合量は特に限定されないが、０．０１〜１重量％の範囲が好ましい。０．０１重量％未満では効果が低く、また１重量％を超えても効果に増強はみられず、非経済的である。 Although the compounding quantity of the glucosyl hesperidin in this invention is not specifically limited, The range of 0.01 to 1 weight% is preferable. If it is less than 0.01% by weight, the effect is low, and if it exceeds 1% by weight, the effect is not enhanced, which is uneconomical.
本発明のまつ毛用化粧料には、さらに目的に応じて、本発明の効果を損なわない量的、質的範囲内で、まつ毛用化粧料に通常配合し得る成分を添加してもよい。このような成分としては、例えば、粉体、増粘剤、皮膜形成剤、ファイバー、アルコール類、多価アルコール類、界面活性剤、炭化水素、エステル等の油脂類、シリコーン油、保湿剤、防腐剤、香料、紫外線吸収剤、酸化防止剤等が挙げられる。 Depending on the purpose, the cosmetics for eyelashes of the present invention may further contain components that can be usually blended in the cosmetics for eyelashes within a quantitative and qualitative range that does not impair the effects of the present invention. Examples of such components include powders, thickeners, film forming agents, fibers, alcohols, polyhydric alcohols, surfactants, oils and fats such as hydrocarbons, esters, silicone oils, humectants, antiseptics, and the like. Agents, fragrances, ultraviolet absorbers, antioxidants and the like.
本発明のまつ毛化粧料をまつ毛に塗布する方法は、均一に塗布できる方法であれば特に制限されない。 The method for applying the eyelash cosmetic of the present invention to the eyelashes is not particularly limited as long as it can be applied uniformly.
次に、本発明に用いるサクラエキスの製造例及び本発明の実施例を挙げて詳しく説明するが、本発明はこれらに限定されるものではない。配合量はすべて重量％である。 Next, although the manufacture example of the cherry extract used for this invention and the Example of this invention are given and demonstrated in detail, this invention is not limited to these. All compounding amounts are in weight percent.
製造例１ サクラエキス（ソメイヨシノの葉の５０％１，３−ブチレングリコール抽出物）
ソメイヨシノの葉１００ｇを生のまま細かく切断し、１，３−ブチレングリコールの５０重量％水溶液を１ｋｇ加え、室温で２日間抽出した。抽出後、その抽出液を濾過してソメイヨシノの葉の５０％１，３−ブチレングリコール抽出物を９５０ｇ得た。なお、この抽出物の乾燥重量は、１９ｇ（２．０重量％）である。
Production Example 1 Sakura Extract (50% 1,3-butylene glycol extract of Yoshino cherry leaves)
100 g of Yoshino cherry leaves were cut into raw pieces, 1 kg of a 50 wt% aqueous solution of 1,3-butylene glycol was added, and the mixture was extracted at room temperature for 2 days. After extraction, the extract was filtered to obtain 950 g of 50% 1,3-butylene glycol extract of Yoshino cherry leaves. The dry weight of this extract is 19 g (2.0% by weight).
製造例２ サクラエキス（ソメイヨシノの葉の熱水抽出物）
ソメイヨシノの葉１００ｇを生のまま細かく切断し、１ｋｇの精製水を加え、１００℃で２時間抽出した。得られた抽出液を濾過し、濃縮した後に凍結乾燥してソメイヨシノの葉の熱水抽出物８．５ｇを得た。
Production Example 2 Sakura extract (hot water extract of Yoshino cherry leaves)
100 g of Yoshino cherry leaves were cut into raw pieces, 1 kg of purified water was added, and the mixture was extracted at 100 ° C. for 2 hours. The obtained extract was filtered, concentrated and freeze-dried to obtain 8.5 g of a hot water extract of Yoshino cherry leaves.
実施例１〜３及び比較例１〜４
下記の表１に示す処方及び下記製法により、まつ毛用化粧料を調製し、以下に示す評価方法及び判定基準により評価し、結果を併せて表１に示した。
Examples 1-3 and Comparative Examples 1-4
Cosmetics for eyelashes were prepared according to the formulation shown in Table 1 below and the following production method, evaluated according to the evaluation methods and criteria shown below, and the results are shown in Table 1.
（製法）
成分（４）を除くすべての成分を室温にて均一混合した後、成分（４）を添加してまつ毛用化粧料を得た。
(Manufacturing method)
After all the components except the component (4) were uniformly mixed at room temperature, the component (4) was added to obtain a cosmetic for eyelashes.
（評価方法１：まつ毛補修効果）
健常なまつ毛に対して、ビューラーで折り曲げながら５０回引っ張り、ダメージ毛を得た。このダメージ毛を実施例、比較例のまつ毛用化粧料に１時間浸漬した後、水洗、乾燥した。このようにして得られたまつ毛を走査型電子顕微鏡にて観察し、上記のダメージ毛と比較して補修効果が認められるか、以下に示す判定基準に従って判定した。
＜判定基準＞
◎：明らかに補修効果が認められた（健常なまつ毛と同等）
○：補修効果が認められた
△：少し補修効果が認められた
×：補修効果が認められなかった
(Evaluation method 1: Eyelash repair effect)
The healthy eyelashes were pulled 50 times while being bent with a buller to obtain damaged hairs. This damaged hair was immersed in the cosmetics for eyelashes of Examples and Comparative Examples for 1 hour, washed with water and dried. The eyelashes thus obtained were observed with a scanning electron microscope, and it was determined according to the following criteria whether the repair effect was recognized as compared with the damaged hair.
<Criteria>
◎: Clearly repaired effect (equivalent to healthy eyelashes)
○: Repair effect recognized △: Repair effect slightly recognized ×: Repair effect not recognized
（評価方法２：ハリ、コシ実感効果）
２０〜４０代の女性被験者５名に、上記実施例及び比較例のまつ毛用化粧料を一日一回連続して３０日間、洗顔後のまつ毛に根元から先端に向かって塗布する使用試験を行った。試験終了後、ハリ、コシ実感効果の有無について、以下の評価基準により評点を付し、実施例及び比較例のまつ毛用化粧料ごとに評点の平均点を算出して、以下に示す判定基準に従って判定した。
＜評価基準＞
〔使用感〕 〔評点〕
ハリ、コシを実感する ：５
ハリ、コシを少し実感する ：４
ハリ、コシをほんの少し実感する ：３
ハリ、コシをあまり実感しない ：２
ハリ、コシを実感しない ：１
＜判定基準＞
〔評点の平均点〕 〔判定〕
４以上 ◎
３以上４未満 ○
２以上３未満 △
２未満 ×
(Evaluation method 2: effect of firmness and stiffness)
5 female subjects in their 20s and 40s were tested to apply the eyelash cosmetics of the above examples and comparative examples once a day for 30 days to the eyelashes after face washing from the root to the tip. It was. After completion of the test, regarding the presence or absence of the effect of firmness and stiffness, give a score according to the following evaluation criteria, calculate the average score for each eyelash cosmetic of Examples and Comparative Examples, according to the criteria shown below Judged.
<Evaluation criteria>
[Use feeling] [score]
Feel the elasticity and stiffness ： 5
I feel a little bit of tension and elasticity: 4
I feel a little bit of tension and stiffness: 3
Hari, I don't really feel the stiffness: 2
Harsh, do not feel the stiffness: 1
<Criteria>
[Average score] [Judgment]
4 or more ◎
3 or more and less than 4 ○
2 or more and less than 3
Less than 2 ×
実施例１、２はいずれも、まつ毛補修効果、ハリ、コシ実感効果ともに良好であった。また、実施例１にグルコシルヘスペリジンを配合した実施例３は、実施例１からハリ、コシ実感効果がさらに上がった。それに対して、サクラエキスを配合していない比較例１は、まつ毛補修効果、ハリ、コシ実感効果ともに認められなかった。また、毛髪補修成分として知られている加水分解コラーゲン液を配合した比較例２及びＤ−キシロースを配合した比較例３は、まつ毛補修効果は不十分であり、ハリ、コシ実感効果は認められなかった。グルコシルヘスペリジンを単独で配合した比較例４は、まつ毛補修効果、ハリ、コシ実感効果ともに認められず、サクラエキスと併用することでまつ毛補修効果、ハリ、コシ実感効果が得られることが明らかとなった。 In each of Examples 1 and 2, the eyelash repair effect, elasticity, and firmness were both good. In addition, in Example 3 in which glucosyl hesperidin was blended with Example 1, the effect of firmness and stiffness was further improved from Example 1. On the other hand, in Comparative Example 1 in which no cherry extract was blended, neither eyelash repair effect, firmness, or firmness effect was observed. Moreover, the comparative example 2 which mix | blended the hydrolyzed collagen liquid known as a hair repair component, and the comparative example 3 which mix | blended D-xylose are inadequate in eyelash repair effect, and a firmness and a firm feeling effect are not recognized. It was. In Comparative Example 4 in which glucosyl hesperidin alone was blended, neither the eyelash repair effect, the firmness, or the firmness effect was observed, but it was revealed that the eyelash repair effect, the firmness, and the firmness effect could be obtained when used in combination with the cherry extract. It was.
実施例１及び実施例４〜７
下記表２に示す処方によりまつ毛用化粧料を調製し、上記評価方法及び判定基準により評価し、結果を併せて表２に示した。
Example 1 and Examples 4-7
A cosmetic for eyelashes was prepared according to the formulation shown in Table 2 below, and evaluated according to the evaluation method and criteria described above. The results are also shown in Table 2.
実施例１及び実施例４〜７はいずれも、まつ毛補修効果、ハリ、コシ実感効果ともに良好であった。特に、実施例１及び実施例５〜７がまつ毛補修効果において非常に良好であった。このことから、特に効果があるのは、サクラエキスを乾燥物として０．０００１重量％以上配合したときであることが明らかとなった。 In both Example 1 and Examples 4 to 7, the eyelash repair effect, elasticity, and firmness feeling effect were both good. Especially Example 1 and Examples 5-7 were very favorable in the eyelash repair effect. From this, it became clear that the effect is particularly effective when the cherry extract is blended in an amount of 0.0001% by weight or more as a dry product.
実施例８
成分 配合量（重量％）
（１）カルボキシビニルポリマー １．０
（２）ヒドロキシエチルセルロース ０．５
（３）１，３−ブチレングリコール ５．０
（４）水酸化カリウム ０．５
（５）９５エタノール ５．０
（６）エデト酸三ナトリウム ０．０２
（７）メチルパラベン ０．２
（８）サクラエキス（注２） ０．１
（９）精製水 ８７．６８
合計 １００．０
注２：サクラエキスＢ（一丸ファルコス社製、乾燥物として２．０重量％）
（製法）
成分（４）を除くすべての成分を室温にて均一混合した後、成分（４）を添加してまつ毛用化粧料を得た。
Example 8
Ingredient Amount (wt%)
(1) Carboxyvinyl polymer 1.0
(2) Hydroxyethyl cellulose 0.5
(3) 1,3-butylene glycol 5.0
(4) Potassium hydroxide 0.5
(5) 95 ethanol 5.0
(6) Edetate trisodium 0.02
(7) Methylparaben 0.2
(8) Sakura extract (Note 2) 0.1
(9) Purified water 87.68
Total 100.0
Note 2: Sakura extract B (manufactured by Ichimaru Falcos, 2.0% by weight as a dry product)
(Manufacturing method)
After all the components except the component (4) were uniformly mixed at room temperature, the component (4) was added to obtain a cosmetic for eyelashes.
実施例９
成分 配合量（重量％）
（１）カルボキシビニルポリマー １．０
（２）ヒドロキシエチルセルロース ０．５
（３）１，３−ブチレングリコール ５．０
（４）トリエタノールアミン ０．２
（５）９５エタノール ５．０
（６）エデト酸三ナトリウム ０．０２
（７）メチルパラベン ０．２
（８）サクラエキス（注２） ０．１
（９）グルコシルヘスペリジン（注１） ０．１
（９）精製水 ８７．８８
合計 １００．０
（製法）
成分（４）を除くすべての成分を室温にて均一混合した後、成分（４）を添加してまつ毛用化粧料を得た。
Example 9
Ingredient Amount (wt%)
(1) Carboxyvinyl polymer 1.0
(2) Hydroxyethyl cellulose 0.5
(3) 1,3-butylene glycol 5.0
(4) Triethanolamine 0.2
(5) 95 ethanol 5.0
(6) Edetate trisodium 0.02
(7) Methylparaben 0.2
(8) Sakura extract (Note 2) 0.1
(9) Glucosyl hesperidin (Note 1) 0.1
(9) Purified water 87.88
Total 100.0
(Manufacturing method)
After all the components except the component (4) were uniformly mixed at room temperature, the component (4) was added to obtain a cosmetic for eyelashes.
実施例８及び９ともに、まつ毛の補修効果に優れたまつ毛用化粧料であった。
Both Examples 8 and 9 were eyelash cosmetics excellent in eyelash repair effect.
本発明のまつ毛用化粧料は、ビューラーによる折り曲げ、引っ張りやマスカラ使用後のクレンジング剤によるこすり落とし等の物理的要因によって引き起こされるまつ毛の損傷を改善、補修することができる。 The cosmetics for eyelashes of the present invention can improve and repair eyelash damage caused by physical factors such as bending by a buller, pulling and rubbing off by a cleansing agent after using mascara.
Claims (4)
The cosmetic for eyelashes according to claim 3, wherein the content of glucosyl hesperidin is 0.01 to 1% by weight.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2013180969A (en) * | 2012-03-01 | 2013-09-12 | Hoyu Co Ltd | Tension and stiffness giving agent composition |
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