JP2011052206A5 - - Google Patents
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- Publication number
- JP2011052206A5 JP2011052206A5 JP2010145553A JP2010145553A JP2011052206A5 JP 2011052206 A5 JP2011052206 A5 JP 2011052206A5 JP 2010145553 A JP2010145553 A JP 2010145553A JP 2010145553 A JP2010145553 A JP 2010145553A JP 2011052206 A5 JP2011052206 A5 JP 2011052206A5
- Authority
- JP
- Japan
- Prior art keywords
- group
- selenium
- source
- substrate
- providing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011669 selenium Substances 0.000 claims 54
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims 46
- 229910052711 selenium Inorganic materials 0.000 claims 46
- 239000000463 material Substances 0.000 claims 30
- 239000000758 substrate Substances 0.000 claims 29
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 10
- 239000002243 precursor Substances 0.000 claims 10
- 239000011593 sulfur Substances 0.000 claims 10
- 229910052717 sulfur Inorganic materials 0.000 claims 10
- 239000007788 liquid Substances 0.000 claims 8
- 238000004519 manufacturing process Methods 0.000 claims 6
- 125000003118 aryl group Chemical group 0.000 claims 5
- 125000003837 (C1-C20) alkyl group Chemical group 0.000 claims 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 4
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims 4
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 4
- 125000005011 alkyl ether group Chemical group 0.000 claims 4
- 125000005189 alkyl hydroxy group Chemical group 0.000 claims 4
- 229910052782 aluminium Inorganic materials 0.000 claims 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 4
- 125000005013 aryl ether group Chemical group 0.000 claims 4
- 229910052802 copper Inorganic materials 0.000 claims 4
- 239000010949 copper Substances 0.000 claims 4
- 229910052733 gallium Inorganic materials 0.000 claims 4
- 229910052738 indium Inorganic materials 0.000 claims 4
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 claims 4
- 229910052709 silver Inorganic materials 0.000 claims 4
- 239000004332 silver Substances 0.000 claims 4
- 239000011734 sodium Substances 0.000 claims 4
- 229910052708 sodium Inorganic materials 0.000 claims 4
- RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 claims 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims 2
- 238000005054 agglomeration Methods 0.000 claims 2
- 230000002776 aggregation Effects 0.000 claims 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 2
- 239000007795 chemical reaction product Substances 0.000 claims 2
- 238000000151 deposition Methods 0.000 claims 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-O hydrazinium(1+) Chemical compound [NH3+]N OAKJQQAXSVQMHS-UHFFFAOYSA-O 0.000 claims 2
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 2
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- 229910052714 tellurium Inorganic materials 0.000 claims 2
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 claims 2
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims 2
- 125000000008 (C1-C10) alkyl group Chemical group 0.000 claims 1
- KYVBNYUBXIEUFW-UHFFFAOYSA-N 1,1,3,3-tetramethylguanidine Chemical compound CN(C)C(=N)N(C)C KYVBNYUBXIEUFW-UHFFFAOYSA-N 0.000 claims 1
- BMVXCPBXGZKUPN-UHFFFAOYSA-N 1-hexanamine Chemical compound CCCCCCN BMVXCPBXGZKUPN-UHFFFAOYSA-N 0.000 claims 1
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 claims 1
- LTHNHFOGQMKPOV-UHFFFAOYSA-N 2-ethylhexan-1-amine Chemical compound CCCCC(CC)CN LTHNHFOGQMKPOV-UHFFFAOYSA-N 0.000 claims 1
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims 1
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims 1
- WUGQZFFCHPXWKQ-UHFFFAOYSA-N Propanolamine Chemical compound NCCCO WUGQZFFCHPXWKQ-UHFFFAOYSA-N 0.000 claims 1
- 125000003282 alkyl amino group Chemical group 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- HQABUPZFAYXKJW-UHFFFAOYSA-N butan-1-amine Chemical compound CCCCN HQABUPZFAYXKJW-UHFFFAOYSA-N 0.000 claims 1
- 150000004770 chalcogenides Chemical class 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- IOQPZZOEVPZRBK-UHFFFAOYSA-N octan-1-amine Chemical compound CCCCCCCCN IOQPZZOEVPZRBK-UHFFFAOYSA-N 0.000 claims 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 150000003573 thiols Chemical class 0.000 claims 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/509,847 US8308973B2 (en) | 2009-07-27 | 2009-07-27 | Dichalcogenide selenium ink and methods of making and using same |
| US12/509,847 | 2009-07-27 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011052206A JP2011052206A (ja) | 2011-03-17 |
| JP2011052206A5 true JP2011052206A5 (enExample) | 2013-07-11 |
| JP5666836B2 JP5666836B2 (ja) | 2015-02-12 |
Family
ID=43447156
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010145553A Active JP5666836B2 (ja) | 2009-07-27 | 2010-06-25 | ジカルコゲナイドセレンインク、並びにその製造方法および使用方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US8308973B2 (enExample) |
| EP (1) | EP2287115B1 (enExample) |
| JP (1) | JP5666836B2 (enExample) |
| KR (1) | KR101199033B1 (enExample) |
| CN (1) | CN101967637A (enExample) |
| TW (1) | TWI432533B (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110137061A1 (en) * | 2009-12-09 | 2011-06-09 | Chi-Jie Wang | Nanoink for forming absorber layer of thin film solar cell and method of producing the same |
| US8709917B2 (en) * | 2010-05-18 | 2014-04-29 | Rohm And Haas Electronic Materials Llc | Selenium/group 3A ink and methods of making and using same |
| US8119506B2 (en) * | 2010-05-18 | 2012-02-21 | Rohm And Haas Electronic Materials Llc | Group 6a/group 3a ink and methods of making and using same |
| WO2011146115A1 (en) | 2010-05-21 | 2011-11-24 | Heliovolt Corporation | Liquid precursor for deposition of copper selenide and method of preparing the same |
| US9142408B2 (en) | 2010-08-16 | 2015-09-22 | Alliance For Sustainable Energy, Llc | Liquid precursor for deposition of indium selenide and method of preparing the same |
| US8883550B2 (en) * | 2010-09-15 | 2014-11-11 | Precursor Energetics, Inc. | Deposition processes for photovoltaic devices |
| US8282995B2 (en) * | 2010-09-30 | 2012-10-09 | Rohm And Haas Electronic Materials Llc | Selenium/group 1b/group 3a ink and methods of making and using same |
| US8343267B2 (en) * | 2011-02-18 | 2013-01-01 | Rohm And Haas Electronic Materials Llc | Gallium formulated ink and methods of making and using same |
| US9105797B2 (en) * | 2012-05-31 | 2015-08-11 | Alliance For Sustainable Energy, Llc | Liquid precursor inks for deposition of In—Se, Ga—Se and In—Ga—Se |
| US9842733B2 (en) * | 2013-06-11 | 2017-12-12 | Imec Vzw | Method for dissolving chalcogen elements and metal chalcogenides in non-hazardous solvents |
| TWI527821B (zh) | 2013-10-16 | 2016-04-01 | 國立中山大學 | 銀化合物、銀墨水及可撓式基板之噴印方法 |
| EP3068729A1 (en) * | 2013-11-15 | 2016-09-21 | Nanoco Technologies Ltd | Preparation of copper-rich copper indium (gallium) diselenide/disulfide nanoparticles |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4520010A (en) | 1983-06-02 | 1985-05-28 | Xerox Corporation | Process for modifying the electrical properties of selenium, and selenium alloys |
| WO1993004212A1 (en) | 1991-08-26 | 1993-03-04 | Eastman Kodak Company | Preparation of group iii element-group vi element compound films |
| WO2001037324A1 (en) | 1999-11-16 | 2001-05-25 | Midwest Research Institute | A NOVEL PROCESSING APPROACH TOWARDS THE FORMATION OF THIN-FILM Cu(In,Ga)Se¿2? |
| CN100490205C (zh) | 2003-07-10 | 2009-05-20 | 国际商业机器公司 | 淀积金属硫族化物膜的方法和制备场效应晶体管的方法 |
| US6875661B2 (en) | 2003-07-10 | 2005-04-05 | International Business Machines Corporation | Solution deposition of chalcogenide films |
| US7163835B2 (en) | 2003-09-26 | 2007-01-16 | E. I. Du Pont De Nemours And Company | Method for producing thin semiconductor films by deposition from solution |
| US7115304B2 (en) | 2004-02-19 | 2006-10-03 | Nanosolar, Inc. | High throughput surface treatment on coiled flexible substrates |
| US7306823B2 (en) | 2004-09-18 | 2007-12-11 | Nanosolar, Inc. | Coated nanoparticles and quantum dots for solution-based fabrication of photovoltaic cells |
| US20070166453A1 (en) | 2004-02-19 | 2007-07-19 | Nanosolar, Inc. | High-throughput printing of chalcogen layer |
| US20080124831A1 (en) | 2004-02-19 | 2008-05-29 | Robinson Matthew R | High-throughput printing of semiconductor precursor layer from chalcogenide particles |
| US20070163640A1 (en) | 2004-02-19 | 2007-07-19 | Nanosolar, Inc. | High-throughput printing of semiconductor precursor layer by use of chalcogen-rich chalcogenides |
| EP1992010A2 (en) * | 2006-02-23 | 2008-11-19 | Van Duren, Jeroen K.J. | High-throughput printing of chalcogen layer and the use of an inter-metallic material |
| US7494841B2 (en) | 2006-05-12 | 2009-02-24 | International Business Machines Corporation | Solution-based deposition process for metal chalcogenides |
| EP2101931B1 (en) | 2006-11-09 | 2015-05-13 | Alliance for Sustainable Energy, LLC | Precursors for formation of copper selenide, indium selenide, copper indium diselenide, and/or copper indium gallium diselenide films |
| WO2008057119A1 (en) | 2006-11-09 | 2008-05-15 | Midwest Research Institue | Formation of copper-indium-selenide and/or copper-indium-gallium-selenide films from indium selenide and copper selenide precursors |
| EP2115783A2 (en) | 2007-01-31 | 2009-11-11 | Jeroen K.J. Van Duren | Solar cell absorber layer formed from metal ion precursors |
| US20080264479A1 (en) * | 2007-04-25 | 2008-10-30 | Nanoco Technologies Limited | Hybrid Photovoltaic Cells and Related Methods |
| JP5566901B2 (ja) * | 2007-11-30 | 2014-08-06 | ナノコ テクノロジーズ リミテッド | ナノ粒子材料の調製 |
| US8613973B2 (en) | 2007-12-06 | 2013-12-24 | International Business Machines Corporation | Photovoltaic device with solution-processed chalcogenide absorber layer |
| US20120060928A1 (en) * | 2009-05-21 | 2012-03-15 | E.I. Du Pont De Nemours And Company | Processes for preparing copper tin sulfide and copper zinc tin sulfide films |
| US8277894B2 (en) * | 2009-07-16 | 2012-10-02 | Rohm And Haas Electronic Materials Llc | Selenium ink and methods of making and using same |
| US20110076798A1 (en) * | 2009-09-28 | 2011-03-31 | Rohm And Haas Electronic Materials Llc | Dichalcogenide ink containing selenium and methods of making and using same |
-
2009
- 2009-07-27 US US12/509,847 patent/US8308973B2/en active Active
-
2010
- 2010-06-21 EP EP10166692.3A patent/EP2287115B1/en active Active
- 2010-06-25 JP JP2010145553A patent/JP5666836B2/ja active Active
- 2010-07-08 TW TW099122440A patent/TWI432533B/zh active
- 2010-07-14 CN CN2010102358183A patent/CN101967637A/zh active Pending
- 2010-07-15 KR KR1020100068560A patent/KR101199033B1/ko active Active
-
2012
- 2012-10-12 US US13/650,574 patent/US8513052B2/en active Active
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