JP2011046680A - Hair cosmetics containing erucic acid-rich rape-seed oil - Google Patents
Hair cosmetics containing erucic acid-rich rape-seed oil Download PDFInfo
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本願発明は、毛髪化粧料、特にパーマネントウエーブ剤、ストレートパーマ剤、ヘアリンス、ヘアトリートメント、酸化染毛剤、及びヘアブリーチ剤に関する。 The present invention relates to a hair cosmetic, particularly a permanent wave agent, a straight permanent agent, a hair rinse, a hair treatment, an oxidative hair dye, and a hair bleaching agent.
ダメージヘアは、一般に毛髪表面がザラつき滑らかでなく、毛髪の感触(滑り感、サラサラ感等)や指・櫛通りが悪く、また艶が無いといった問題を有する。 Damaged hair generally has the problem that the hair surface is not smooth and smooth, the hair feel (smoothness, smoothness, etc.), the fingers and combs are not good, and the hair is not glossy.
そこで、従来、毛髪表面を滑らかにするため、各種成分(シリコンラバー、アミノ変性シリコーン、高重合シリコーン、非イオン性高分子、カチオン化高分子、アニオン化高分子等)を配合した毛髪化粧料が提案されている。 Therefore, conventionally, hair cosmetics containing various components (silicon rubber, amino-modified silicone, highly polymerized silicone, nonionic polymer, cationized polymer, anionized polymer, etc.) to smooth the hair surface have been prepared. Proposed.
しかし、このような毛髪化粧料を繰り返し使用していくと、次第に上記配合成分が毛髪表面上に蓄積され、その結果、毛髪が硬くなりボソつきやカリつきが生じてくる、毛髪にボリュームが出過ぎて纏まらない、毛髪に艶が無くなる等、といったダメージヘアと同じような問題が出てきた。 However, when such hair cosmetics are used repeatedly, the above ingredients are gradually accumulated on the hair surface. As a result, the hair becomes stiff and bulges and becomes crisp, resulting in excessive volume in the hair. The same problems as damaged hair, such as losing luster and losing luster on the hair.
一方、毛髪の感触・風合いを向上させるため、植物油(オリーブ油、リノールサラダ油、椿油、アボカド油、小麦胚芽油、ヒマシ油、ホホバ油等)を配合した毛髪化粧料も知られている。 On the other hand, hair cosmetics containing vegetable oils (olive oil, linole salad oil, cocoon oil, avocado oil, wheat germ oil, castor oil, jojoba oil, etc.) for improving the feel and texture of hair are also known.
しかし、このような毛髪化粧料は、毛髪に油性感は付与できても、吸着したコーティング感は付与できず、そのため滑り感やサラサラ感、指・櫛通り等を向上させることはできなかった。 However, even though such a hair cosmetic can impart an oily feeling to the hair, it cannot impart an adsorbed coating feeling, and therefore it has not been possible to improve the slipping feeling, smooth feeling, finger / comb passage, and the like.
上記事情に鑑み、本願発明は、毛髪(特にダメージヘア)に優れたコーティング感を付与することにより毛髪表面を滑らかにし且つザラつきを無くし、その結果、健康毛のような優れた滑り感、サラサラ感、指・櫛通り、艶等を付与でき、更に長期間、繰り返し使用しても配合成分が毛髪表面上に蓄積されず、その結果、毛髪にボソつきやカリつきが生じず、毛髪の纏まり・艶を優れた状態に維持できる、毛髪化粧料を提供することを目的とする。 In view of the above circumstances, the present invention smoothes the hair surface and eliminates roughness by imparting an excellent coating feeling to hair (particularly damaged hair). Feeling, finger / comb, gloss, etc. can be given, and even if used repeatedly for a long time, the compounding ingredients do not accumulate on the hair surface, so that the hair does not become sticky or clogged, and the hair is bundled -It aims at providing the hair cosmetics which can maintain glossiness in the outstanding state.
上記目的を達成するため、本願発明者が鋭意、検討した結果、以下の本願発明を成すに到った。 In order to achieve the above object, the inventor of the present application diligently studied, and as a result, has reached the following present invention.
即ち、本願第1発明は、高エルカ酸品種菜種油を、0.1〜30重量%含有することを特徴とする毛髪化粧料を提供する。 That is, the first invention of the present application provides a hair cosmetic characterized by containing 0.1 to 30% by weight of a high erucic acid variety rapeseed oil.
本願第2発明は、高エルカ酸品種菜種油がエルカ酸を40.0〜65.0重量%含有することを特徴とする本願第1発明の毛髪化粧料を提供する。 The second invention of the present application provides the hair cosmetic composition of the first invention of the present application, wherein the high erucic acid variety rapeseed oil contains 40.0 to 65.0% by weight of erucic acid.
本願第3発明は、毛髪化粧料が、パーマネントウエーブ剤、ストレートパーマ剤、ヘアリンス、ヘアトリートメント、酸化染毛剤、又はブリーチ剤であることを特徴とする本願第1発明又は第2発明の毛髪化粧料を提供する。 The third aspect of the present invention is the hair cosmetic composition according to the first or second aspect of the present invention, wherein the hair cosmetic is a permanent wave agent, a straight permanent agent, a hair rinse, a hair treatment, an oxidative hair dye, or a bleaching agent. Provide a fee.
本願第4発明は、本願第1発明〜第3発明の何れかの毛髪化粧料の調製に用いられる高エルカ酸品種菜種油を提供する。 The fourth invention of the present application provides a high erucic acid variety rapeseed oil used for the preparation of the hair cosmetic composition of any one of the first to third inventions of the present application.
本願発明により、毛髪(特にダメージヘア)に優れたコーティング感を付与することにより毛髪表面を滑らかにし且つザラつきを無くし、その結果、健康毛のような優れた滑り感、サラサラ感、指・櫛通り、艶等を付与でき、更に長期間、繰り返し使用しても配合成分が毛髪表面上に蓄積されず、その結果、毛髪にボソつきやカリつきが生じず、毛髪の纏まり・艶を優れた状態に維持できる、毛髪化粧料を提供することができる。 According to the present invention, the hair surface (especially damaged hair) is imparted with an excellent coating feeling to make the hair surface smooth and free from roughness. As a result, excellent slipperiness, smoothness, finger / comb like healthy hair As a result, even if it is used repeatedly for a long period of time, the blended components will not accumulate on the hair surface, and as a result, the hair will not be crumpled or crisp, and the hair will have excellent lump and gloss A hair cosmetic that can be maintained in a state can be provided.
以下、本願発明を、最良の実施形態について、詳述する。
本願発明の毛髪化粧料には、高エルカ酸品種菜種油を含有する。高エルカ酸品種菜種油は、エルカ酸含量の高い菜種品種より採油された菜種油である。高エルカ酸品種菜種油中、エルカ酸は40.0〜65.0(好ましくは43.0〜60.0)重量%含有するのが好ましい。そのような高エルカ酸品種菜種油としては、具体的には、サミット製油株式会社製「ハイエルシン菜種白絞油」等が挙げられる。Hereinafter, the present invention will be described in detail with respect to the best mode.
The hair cosmetic composition of the present invention contains a high erucic acid variety rapeseed oil. High erucic acid rapeseed oil is rapeseed oil extracted from rapeseed varieties having a high erucic acid content. The erucic acid is preferably contained in 40.0 to 65.0 (preferably 43.0 to 60.0) wt% in the high erucic acid rapeseed oil. Specific examples of such high erucic acid variety rapeseed oil include “Hielsin rapeseed white squeezed oil” manufactured by Summit Oil Co., Ltd.
本願発明の毛髪化粧料には、添加成分として、炭化水素類[(流動)パラフィン、スクワラン等]、シリコーン類(好ましくは粘度が200cs以下のもの)[メチルポリシロキサン等]、油脂類[オリーブ油、リノールサラダ油、ホホバ油等]、ロウ類[カルナウバロウ、キャンデリラロウ等]、エステル油類[脂肪酸エステル(ミリスチン酸イソプロピル、ミリスチン酸2−オクチルドデシル等)、リンゴ酸ジイソステアリル等]、脂肪酸類[ラウリン酸、ステアリン酸、ベヘニン酸等]、アルコール類[高級アルコール(セチルアルコール、(イソ)ステアリルアルコール、2−オクチルドデカノール等)、多価アルコール(エチレングリコール、グリセリン等)]、エーテル油類[バチルアルコール、キミルアルコール、ジオクチルエーテル等]、アミン類[ジメチルステアリルアミン等]、アミドアミン類[ステアラミドプロピルジメチルアミン等]、カチオン界面活性剤[C12〜C22トリメチル型(塩化C12〜C22アルキルトリメチルアンモニウム等)、ジC12〜C22アルキル型(塩化ジC12〜C22アルキルジメチルアンモニウム等)]、アニオン界面活性剤[C12〜C16硫酸Na型(アルキル硫酸エステル塩、POEアルキルエーテル硫酸塩等)、アミノ酸系(N−アシルアミノ酸塩等)]、非イオン界面活性剤[ソルビタン系(ソルビタン高級脂肪酸エステル等)、POEアルキルエーテル等]を含有してよい。 In the hair cosmetic composition of the present invention, as additives, hydrocarbons [(liquid) paraffin, squalane, etc.], silicones (preferably those having a viscosity of 200 cs or less) [methyl polysiloxane etc.], fats and oils [olive oil, Linole salad oil, jojoba oil, etc.], waxes [carnauba wax, candelilla wax, etc.], ester oils [fatty acid esters (isopropyl myristate, 2-octyldodecyl myristate, etc.), diisostearyl malate, etc.], fatty acids [ Lauric acid, stearic acid, behenic acid, etc.], alcohols [higher alcohols (cetyl alcohol, (iso) stearyl alcohol, 2-octyldodecanol, etc.), polyhydric alcohols (ethylene glycol, glycerin, etc.)], ether oils [ Batyl alcohol, chimyl alcohol, dioctyl Ether, etc.], amines [dimethylstearylamine, etc.], amidoamines [stearamidopropyldimethylamine, etc.], cationic surfactants [C12-C22 trimethyl type (C12-C22 alkyltrimethylammonium chloride, etc.), di-C12-C22 alkyl Type (di-C12-C22 alkyldimethylammonium chloride, etc.)], anionic surfactant [C12-C16 sulfuric acid Na type (alkyl sulfate ester salt, POE alkyl ether sulfate, etc.), amino acid system (N-acyl amino acid salt, etc.)] , Nonionic surfactants [sorbitans (such as higher sorbitan fatty acid esters), POE alkyl ethers, etc.] may be contained.
本願発明の毛髪化粧料の組成において、高エルカ酸品種菜種油を0.1〜30.0(好ましくは0.5〜20.0)重量%含有するのが好ましい。高エルカ酸品種菜種油が多過ぎると、吸着が多く重く、スベリ、滑らかさが悪くなることがある。 In the composition of the hair cosmetic composition of the present invention, it is preferable to contain 0.1 to 30.0 (preferably 0.5 to 20.0)% by weight of high erucic acid variety rapeseed oil. If there is too much high erucic acid rapeseed oil, the amount of adsorption will be heavy and the smoothness and smoothness may be poor.
本願発明の毛髪化粧料としては、例えばパーマネントウエーブ剤(第I剤及び/又は第II剤)、ストレートパーマ剤(第I剤及び/又は第II剤)、ヘアリンス、ヘアトリートメント、酸化染毛剤(第I剤及び/又は第II剤)、又はブリーチ剤(第I剤)等が挙げられる。 Examples of the hair cosmetic composition of the present invention include permanent wave agents (I and / or II agents), straight permanent agents (I and / or II agents), hair rinses, hair treatments, oxidative hair dyes ( (I agent and / or II agent), bleach agent (I agent), etc. are mentioned.
<毛髪化粧料の調製>
表1〜17に示す配合組成に従って、それぞれパーマネントウエーブ剤第I剤[実施例1−(1)〜1−(8)、及び比較例1−(1)〜1−(10)]、パーマネントウエーブ剤第II剤[実施例2−(1)〜2−(8)、及び比較例2−(1)〜2−(10)]、ストレートパーマ剤第I剤[実施例3−(1)〜3−(9)、及び比較例3−(1)〜3−(3)]、ストレートパーマ剤第II剤[実施例4−(1)〜4−(9)、及び比較例4−(1)〜4−(3)]、ヘアリンス又はヘアトリートメント[実施例5−(1)〜5−(13)、及び比較例5−(1)〜5−(14)]、酸化染毛剤第I剤[実施例6−(1)〜6−(15)、及び比較例6−(1)〜6−(15)]、酸化染毛剤第II剤[実施例7−(1)〜7−(15)、及び比較例7−(1)〜7−(15)]、並びにヘアブリーチ剤第I剤[実施例8−(1)〜8−(15)、及び比較例8−(1)〜8−(15)]を調製した。<Preparation of hair cosmetics>
According to the composition shown in Tables 1 to 17, permanent wave agent I (Examples 1- (1) to 1- (8) and Comparative Examples 1- (1) to 1- (10)), permanent wave, respectively. Agent II Agent [Example 2- (1) to 2- (8) and Comparative Example 2- (1) to 2- (10)], Straight Perm Agent I Agent [Example 3- (1) to 3- (9) and Comparative Examples 3- (1) to 3- (3)], Straight Perm Agent II Agent [Examples 4- (1) to 4- (9), and Comparative Example 4- (1) ) To 4- (3)], hair rinse or hair treatment [Examples 5- (1) to 5- (13) and Comparative Examples 5- (1) to 5- (14)], Oxidative hair dye No. I Agents [Examples 6- (1) to 6- (15) and Comparative Examples 6- (1) to 6- (15)], Oxidative hair dye II agent [Examples 7- (1) to 7- (15 And Comparative Examples 7- (1) to 7- (15)], and hair bleaching agent I [Examples 8- (1) to 8- (15) and Comparative Examples 8- (1) to 8-- (15)] was prepared.
尚、「高エルカ酸品種菜種油」としてサミット製油株式会社製「ハイエルシン菜種白絞油」、「低エルカ酸品種菜種油」としてキャノーラ油[味の素株式会社製「1番絞りキャノーラ油」]を、それぞれ用いた。 In addition, “High Elsin rapeseed white squeezed oil” manufactured by Summit Oil Co., Ltd. as “high erucic acid rapeseed oil”, and canola oil [“No. 1 squeezed canola oil” manufactured by Ajinomoto Co., Inc.] as “low erucic acid rapeseed oil”, respectively. It was.
<毛髪化粧料の各種評価試験>
上記で調製された各毛髪化粧料について、下記の方法にて、各種評価試験を行った。
評価結果を、それぞれ表1〜17に示す。<Various evaluation tests for hair cosmetics>
Each hair cosmetic prepared as described above was subjected to various evaluation tests by the following methods.
The evaluation results are shown in Tables 1 to 17, respectively.
・パーマネントウエーブ剤第I剤についての評価試験
毛髪全体に第I剤を塗布し、ロットを巻き、ロットの上より再度、第I剤を全体に対し塗布した。その後、キャップを被せ、10分間、放置した。10分経過後、キャップを外し、中間水洗し、タオルドライを行った。次いで、第II剤(添加剤なしの6%ブロム酸ナトリウム水溶液)を上記処理毛髪に塗布し、7分放置後、再度第II剤を塗布し、7分放置した。7分経過後、ロットを外し、水洗、タオルドライ、乾燥後、毛髪表面の滑らかさについて官能評価した。-Evaluation test for permanent wave agent I The agent I was applied to the entire hair, the lot was wound, and the agent I was applied again over the lot. Thereafter, the cap was put on and left for 10 minutes. After 10 minutes, the cap was removed, the water was washed with water, and towel drying was performed. Next, the second agent (6% sodium bromate aqueous solution without additives) was applied to the treated hair, allowed to stand for 7 minutes, and then the second agent was applied again and left for 7 minutes. After 7 minutes, the lot was removed, washed with water, towel-dried, dried, and then subjected to sensory evaluation on the smoothness of the hair surface.
評価基準(毛髪表面の滑らかさ)
「×(a)」:毛髪表面がザラつき、滑らかさ無し。
「×(b):ザラつきは無いが、表面に付き過ぎ、重く滑らかとは言えない。
「○」:吸着し、表面が滑らか。
「◎」:吸着し、表面が非常に滑らか。Evaluation criteria (smoothness of hair surface)
“× (a)”: The hair surface is rough and smooth.
“× (b): There is no roughness, but it is too sticky on the surface and cannot be said to be heavy and smooth.
“O”: Adsorbed and smooth surface.
“◎”: Adsorbed and the surface is very smooth.
・パーマネントウエーブ剤第II剤についての評価試験
第I剤として(7%5mlのチオグリコール酸アンモニウム、アンモニア水処方、添加剤無し水溶液)を用い、第II剤として各実施例又は比較例のものを用いた以外は、パーマネントウエーブ剤第I剤と同様にして、毛髪表面の滑らかさについて官能評価した。・ Evaluation test for permanent wave agent II agent (7% 5 ml ammonium thioglycolate, aqueous ammonia formulation, aqueous solution without additives) as agent I, and those of each example or comparative example as agent II Sensory evaluation was performed on the smoothness of the hair surface in the same manner as in the permanent wave agent I, except that it was used.
・ストレートパーマ剤第I剤についての評価試験
未処理毛髪全体に第I剤を塗布し、キャップを被せ、15分間、放置後、濯ぎ・乾燥した。乾燥後、アイロン処理した。次いで、第II剤(添加剤なしの6%ブロム酸ナトリウム水溶液)を塗布した後、15分間、放置した。その後、濯ぎ、タオルドライ、乾燥後、毛髪表面の滑らかさ及びストレートパーマ剤としての機能について官能評価した。・ Evaluation test for straight permanent agent No. I The No. I agent was applied to the whole untreated hair, covered with a cap, allowed to stand for 15 minutes, rinsed and dried. After drying, it was ironed. Next, after applying the second agent (6% aqueous solution of sodium bromate without additives), the mixture was allowed to stand for 15 minutes. Then, after rinsing, towel drying, and drying, sensory evaluation was performed for the smoothness of the hair surface and the function as a straight permanent agent.
評価基準(毛髪表面の滑らかさ)
「×(a)」:毛髪表面がザラつき、滑らかさ無し。
「×(b):ザラつきは無いが、表面に付き過ぎ、重く滑らかとは言えない。
「△」:処理前(未処理)毛髪と変わらず。
「○」:吸着し、表面が滑らか。
「◎」:吸着し、表面が非常に滑らか。Evaluation criteria (smoothness of hair surface)
“× (a)”: The hair surface is rough and smooth.
“× (b): There is no roughness, but it is too sticky on the surface and cannot be said to be heavy and smooth.
“Δ”: unchanged from untreated (untreated) hair.
“O”: Adsorbed and smooth surface.
“◎”: Adsorbed and the surface is very smooth.
評価基準(機能=粘度、クリームの伸び)
「×(c)」:粘度が低過ぎ、垂れる。
「×(d):粘度が高過ぎ、塗布時クリームの伸びが悪い。
「△」:粘度がやや低い。
「○」:粘度、伸び共に適度。
「◎」:粘度、伸び共に最適。Evaluation criteria (function = viscosity, cream elongation)
“× (c)”: Viscosity is too low and dripping.
“× (d): Viscosity is too high and the elongation of the cream is poor when applied.
“Δ”: Viscosity is slightly low.
"O": Both viscosity and elongation are moderate.
“◎”: Optimum in both viscosity and elongation.
・ストレートパーマ剤第II剤についての評価試験
第I剤として(7%5mlのチオグリコール酸アンモニウム・アンモニア水・モノエタノールアミン水・添加剤なし水溶液)を用い、第II剤として各実施例又は比較例のものを用いた以外は、ストレートパーマ剤第I剤と同様にして、毛髪表面の滑らかさ及びストレートパーマ剤としての機能について官能評価した。・ Evaluation test for straight permanent agent II agent (7% 5 ml ammonium thioglycolate, ammonia water, monoethanolamine water, aqueous solution without additives) as agent I, and each example or comparison as agent II Sensory evaluation was performed on the smoothness of the hair surface and the function as a straight perm agent in the same manner as the straight perm agent No. I except that the example was used.
・ヘアリンス又はヘアトリートメントについての評価試験
毛髪をシャンプー後、ヘアリンス又はヘアトリートメントを塗布し、濯ぎ、乾燥後、毛髪表面の滑らかさについて官能評価した。また、上記処理を1日1回、計5日間、行い、蓄積性について官能評価した。Evaluation test for hair rinse or hair treatment After shampooing the hair, the hair rinse or hair treatment was applied, rinsed, dried, and sensory evaluated for the smoothness of the hair surface. Moreover, the said process was performed once a day for a total of 5 days, and sensory evaluation was carried out about accumulation property.
評価基準(毛髪表面の滑らかさ)
「△(a)」:吸着しているが、滑らかとは言えない。
「△(b)」:吸着が多く重い、また滑らかとは言えない。
「○」:滑らか。
「◎」:非常に滑らか。Evaluation criteria (smoothness of hair surface)
“Δ (a)”: adsorbed but not smooth.
“Δ (b)”: Heavy adsorption and heavy and cannot be said to be smooth.
“○”: Smooth.
“◎”: Very smooth.
評価基準(蓄積性)
「×」:ボソつき・カリつき有り。
「○」:ボソつき・カリつき無し。Evaluation criteria (accumulation)
“×”: with bulge and potash.
“○”: with a bulge and no crisp.
・酸化染毛剤第I剤についての評価試験
第I剤と第II剤を、1:1の割合で混合し、これを毛髪全体に塗布し、キャップを被せた。20分間、放置した後、濯ぎ、シャンプー、濯ぎ、タオルドライ、乾燥した。その後、毛髪表面の滑らかさについて官能評価した。尚、第II剤として、実施例7−(2)において「高エルカ酸品種菜種油」を除いたもの、を用いた。-Evaluation test about oxidation hair dye 1st agent The 1st agent and the 2nd agent were mixed in the ratio of 1: 1, this was applied to the whole hair, and the cap was put on. After standing for 20 minutes, it was rinsed, shampooed, rinsed, towel dried and dried. Then, sensory evaluation was carried out about the smoothness of the hair surface. As the II agent, the one obtained by removing “high erucic acid variety rapeseed oil” in Example 7- (2) was used.
評価基準(毛髪表面の滑らかさ)
「×(a)」:毛髪表面がザラつき、滑らかさ無し。
「×(b):ザラつきは無いが、表面に付き過ぎ、重く滑らかとは言えない。
「○」:吸着し、表面が滑らか。
「◎」:吸着し、表面が非常に滑らか。Evaluation criteria (smoothness of hair surface)
“× (a)”: The hair surface is rough and smooth.
“× (b): There is no roughness, but it is too sticky on the surface and cannot be said to be heavy and smooth.
“O”: Adsorbed and smooth surface.
“◎”: Adsorbed and the surface is very smooth.
・酸化染毛剤第II剤についての評価試験
第I剤として、実施例6−(2)において「高エルカ酸品種菜種油」を除いたもの、を用い、第II剤として各実施例又は比較例のものを用いた以外は、酸化染毛剤第I剤と同様にして、毛髪表面の滑らかさについて官能評価した。・ Evaluation test for oxidative hair dye No. II agent As the I agent, except for “high erucic acid variety rapeseed oil” in Example 6- (2), each Example or Comparative Example as the II agent The hair surface was subjected to a sensory evaluation on the smoothness of the hair surface in the same manner as the oxidation hair dye No. I, except that
・ヘアブリーチ剤第I剤についての評価試験
酸化染毛剤第I剤と同様にして、毛髪表面の滑らかさについて官能評価した。尚、ヘアブリーチ剤第II剤として、実施例7−(2)において「高エルカ酸品種菜種油」を除いたもの、を用いた。-Evaluation test about hair bleaching agent 1st agent The sensory evaluation was carried out about the smoothness of the hair surface like the oxidation hair dye 1st agent. As the hair bleaching agent II, the one obtained by removing “high erucic acid variety rapeseed oil” in Example 7- (2) was used.
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