JP2010235493A - 歯磨組成物の製造方法 - Google Patents
歯磨組成物の製造方法 Download PDFInfo
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- JP2010235493A JP2010235493A JP2009084203A JP2009084203A JP2010235493A JP 2010235493 A JP2010235493 A JP 2010235493A JP 2009084203 A JP2009084203 A JP 2009084203A JP 2009084203 A JP2009084203 A JP 2009084203A JP 2010235493 A JP2010235493 A JP 2010235493A
- Authority
- JP
- Japan
- Prior art keywords
- silica
- dentifrice composition
- sodium chloride
- mass
- sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 61
- 239000000551 dentifrice Substances 0.000 title claims abstract description 58
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 21
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 97
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 74
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims abstract description 56
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 48
- 239000011780 sodium chloride Substances 0.000 claims abstract description 37
- 239000011775 sodium fluoride Substances 0.000 claims abstract description 28
- 235000013024 sodium fluoride Nutrition 0.000 claims abstract description 28
- 238000013329 compounding Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 10
- 230000007935 neutral effect Effects 0.000 abstract description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000008213 purified water Substances 0.000 description 7
- 239000013078 crystal Substances 0.000 description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000002411 adverse Effects 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229910052731 fluorine Inorganic materials 0.000 description 3
- 239000011737 fluorine Substances 0.000 description 3
- 238000005498 polishing Methods 0.000 description 3
- 230000008719 thickening Effects 0.000 description 3
- XGRSAFKZAGGXJV-UHFFFAOYSA-N 3-azaniumyl-3-cyclohexylpropanoate Chemical compound OC(=O)CC(N)C1CCCCC1 XGRSAFKZAGGXJV-UHFFFAOYSA-N 0.000 description 2
- CUFNKYGDVFVPHO-UHFFFAOYSA-N azulene Chemical compound C1=CC=CC2=CC=CC2=C1 CUFNKYGDVFVPHO-UHFFFAOYSA-N 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 229940043430 calcium compound Drugs 0.000 description 2
- 150000001674 calcium compounds Chemical class 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 208000002925 dental caries Diseases 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 150000002222 fluorine compounds Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 208000028169 periodontal disease Diseases 0.000 description 2
- 229960004711 sodium monofluorophosphate Drugs 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 235000011010 calcium phosphates Nutrition 0.000 description 1
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 1
- 235000005487 catechin Nutrition 0.000 description 1
- 229950001002 cianidanol Drugs 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 208000007565 gingivitis Diseases 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 201000001245 periodontitis Diseases 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- YUOWTJMRMWQJDA-UHFFFAOYSA-J tin(iv) fluoride Chemical compound [F-].[F-].[F-].[F-].[Sn+4] YUOWTJMRMWQJDA-UHFFFAOYSA-J 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 150000003752 zinc compounds Chemical class 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
【解決手段】塩化ナトリウムやシリカが存在しない条件下でフッ化ナトリウムを溶解し、塩化ナトリウムやシリカと配合することにより中性付近の歯磨組成物を効率的に得ることができる製造方法。塩化ナトリウムの含有量が、歯磨組成物全量に対して5〜35質量%であり、またシリカは研磨性シリカであり、さらにその配合量が、5〜35質量%であることが好ましい。
【選択図】なし
Description
項1.結晶状態の塩化ナトリウム、フッ化ナトリウム及びシリカを含有する歯磨組成物において、塩化ナトリウム及びシリカが存在しない条件下でフッ化ナトリウムを溶解させることを特徴とする歯磨組成物の製造方法。
項2.フッ化ナトリウムを溶解した後に、溶解した組成物に塩化ナトリウムやシリカを混合することを特徴とする項1に記載の歯磨組成物の製造方法。
項3.塩化ナトリウムの含有量が、歯磨組成物全量に対して5〜35質量%であることを特徴とする項1または項2の何れかに記載の歯磨組成物の製造方法。項4.シリカが研磨性シリカであることを特徴とする項1〜3の何れかに記載の歯磨組成物の製造方法。項5.シリカの配合量が、5〜35質量%であることを特徴とする項1〜4の何れかに記載の歯磨組成物の製造方法。
Claims (5)
- 結晶状態の塩化ナトリウム、フッ化ナトリウム及びシリカを含有する歯磨組成物において、塩化ナトリウム及びシリカが存在しない条件下でフッ化ナトリウムを溶解させることを特徴とする歯磨組成物の製造方法。
- フッ化ナトリウムを溶解した後に、溶解した組成物に塩化ナトリウムやシリカを混合することを特徴とする請求項1に記載の歯磨組成物の製造方法。
- 塩化ナトリウムの含有量が、歯磨組成物全量に対して5〜35質量%であることを特徴とする請求項1または2の何れかに記載の歯磨組成物の製造方法。
- シリカが研磨性シリカであることを特徴とする請求項1〜3の何れかに記載の歯磨組成物の製造方法。
- シリカの配合量が、5〜35質量%であることを特徴とする請求項1〜4の何れかに記載の歯磨組成物の製造方法。
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JP2009084203A JP5552251B2 (ja) | 2009-03-31 | 2009-03-31 | 歯磨組成物の製造方法 |
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JP2009084203A JP5552251B2 (ja) | 2009-03-31 | 2009-03-31 | 歯磨組成物の製造方法 |
Publications (2)
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JP2010235493A true JP2010235493A (ja) | 2010-10-21 |
JP5552251B2 JP5552251B2 (ja) | 2014-07-16 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2021160978A (ja) * | 2020-03-31 | 2021-10-11 | 三井化学株式会社 | アルカリモノフルオロホスフェート組成物の製造方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH04234807A (ja) * | 1990-01-08 | 1992-08-24 | Unilever Nv | 口腔用組成物 |
JP2003183141A (ja) * | 2001-12-18 | 2003-07-03 | Lion Corp | 歯磨組成物 |
JP2008013528A (ja) * | 2006-07-10 | 2008-01-24 | Kao Corp | 歯磨き組成物 |
-
2009
- 2009-03-31 JP JP2009084203A patent/JP5552251B2/ja active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH04234807A (ja) * | 1990-01-08 | 1992-08-24 | Unilever Nv | 口腔用組成物 |
JP2003183141A (ja) * | 2001-12-18 | 2003-07-03 | Lion Corp | 歯磨組成物 |
JP2008013528A (ja) * | 2006-07-10 | 2008-01-24 | Kao Corp | 歯磨き組成物 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2021160978A (ja) * | 2020-03-31 | 2021-10-11 | 三井化学株式会社 | アルカリモノフルオロホスフェート組成物の製造方法 |
JP7449141B2 (ja) | 2020-03-31 | 2024-03-13 | 三井化学株式会社 | アルカリモノフルオロホスフェート組成物の製造方法 |
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JP5552251B2 (ja) | 2014-07-16 |
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