JP2009298803A5 - - Google Patents
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- Publication number
- JP2009298803A5 JP2009298803A5 JP2009188092A JP2009188092A JP2009298803A5 JP 2009298803 A5 JP2009298803 A5 JP 2009298803A5 JP 2009188092 A JP2009188092 A JP 2009188092A JP 2009188092 A JP2009188092 A JP 2009188092A JP 2009298803 A5 JP2009298803 A5 JP 2009298803A5
- Authority
- JP
- Japan
- Prior art keywords
- sucralose
- crystals
- maintain
- range
- water content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- BAQAVOSOZGMPRM-JVFSCRHWSA-N (2R,3R,4R,5R,6R)-2-[(2S,3R,4R,5R)-2,5-bis(chloromethyl)-3,4-dihydroxyoxolan-2-yl]oxy-5-chloro-6-(hydroxymethyl)oxane-3,4-diol Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@]1(CCl)[C@H](O)[C@@H](O)[C@H](CCl)O1 BAQAVOSOZGMPRM-JVFSCRHWSA-N 0.000 claims 3
- 239000004376 Sucralose Substances 0.000 claims 3
- 235000019408 sucralose Nutrition 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Claims (1)
- pHが5.5乃至8.5の範囲に保持するように調整されたスクラロース水溶液から結晶化されたスクラロース結晶であって、0.5重量%乃至10重量%の残留水分量を含むことを特徴とする、スクラロース結晶。
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US24978200P | 2000-11-17 | 2000-11-17 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2002543503A Division JP4560637B2 (ja) | 2000-11-17 | 2001-11-16 | 改良されたスクラロース組成物およびその結晶化の方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2009298803A JP2009298803A (ja) | 2009-12-24 |
JP2009298803A5 true JP2009298803A5 (ja) | 2010-10-28 |
Family
ID=22944966
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2002543503A Expired - Fee Related JP4560637B2 (ja) | 2000-11-17 | 2001-11-16 | 改良されたスクラロース組成物およびその結晶化の方法 |
JP2009188092A Pending JP2009298803A (ja) | 2000-11-17 | 2009-08-14 | 改良されたスクラロース組成物およびその結晶化の方法 |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2002543503A Expired - Fee Related JP4560637B2 (ja) | 2000-11-17 | 2001-11-16 | 改良されたスクラロース組成物およびその結晶化の方法 |
Country Status (11)
Country | Link |
---|---|
US (4) | US6646121B2 (ja) |
EP (1) | EP1339728B1 (ja) |
JP (2) | JP4560637B2 (ja) |
KR (1) | KR100854528B1 (ja) |
CN (1) | CN1294139C (ja) |
AU (2) | AU2691802A (ja) |
BR (1) | BR0115482B1 (ja) |
CA (1) | CA2429228C (ja) |
MX (1) | MXPA03004402A (ja) |
RU (1) | RU2279437C2 (ja) |
WO (1) | WO2002040495A2 (ja) |
Families Citing this family (55)
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US6921026B2 (en) * | 2002-02-05 | 2005-07-26 | Albert L. Saari | Preservation of intermediate moisture foods by controlling humidity and inhibition of mold growth |
US6998480B2 (en) * | 2002-03-08 | 2006-02-14 | Tate & Lyle Public Limited Company | Process for improving sucralose purity and yield |
US6984732B2 (en) * | 2003-03-31 | 2006-01-10 | Mcneil-Ppc, Inc. | High-intensity sweetener composition and delivery of same |
US6943248B2 (en) * | 2003-04-30 | 2005-09-13 | Tate & Lyle Public Limited Company | Crystalline form of sucralose, and method for producing it |
US20040258822A1 (en) * | 2003-06-16 | 2004-12-23 | Shyhyuan Liao | Chilsonated sucralose product |
US20040258818A1 (en) * | 2003-06-20 | 2004-12-23 | Kraft Foods Holdings, Inc. | Reduced acidic flavor in acidified starch products |
MXPA06010665A (es) * | 2004-03-19 | 2007-03-28 | Pharmed Medicare Pvt Ltd | Un proceso mejorado para producir sacarosa clorada. |
US20070020330A1 (en) | 2004-11-24 | 2007-01-25 | Medpointe Healthcare Inc. | Compositions comprising azelastine and methods of use thereof |
WO2006058022A1 (en) | 2004-11-24 | 2006-06-01 | Medpointe Healthcare Inc. | Compositions comprising azelastine and methods of use thereof |
US8758816B2 (en) | 2004-11-24 | 2014-06-24 | Meda Pharmaceuticals Inc. | Compositions comprising azelastine and methods of use thereof |
JP4737977B2 (ja) * | 2004-11-30 | 2011-08-03 | 株式会社ケーヒン | 燃料電池用弁装置 |
KR101102803B1 (ko) * | 2004-12-28 | 2012-01-05 | 니혼 텐사이 세이토 가부시키가이샤 | 디프룩토스 2무수물 ⅲ 결정 제조 방법 |
US7750146B2 (en) * | 2005-03-18 | 2010-07-06 | Tate & Lyle Plc | Granular sucralose |
US20060247180A1 (en) * | 2005-04-29 | 2006-11-02 | Bergey James L | Purgative composition and uses thereof |
US20060276639A1 (en) * | 2005-06-01 | 2006-12-07 | Healthy Brands, Llc | Conversion of sucralose-6-ester to sucralose |
DE202005019910U1 (de) * | 2005-12-19 | 2007-04-19 | Mann + Hummel Gmbh | Filter |
US7741477B2 (en) * | 2006-01-10 | 2010-06-22 | Alembic Limited | Process for purification of sucralose |
US20070264403A1 (en) * | 2006-05-11 | 2007-11-15 | Nehmer Warren L | Sparkling agglomerated sweetener, and method of making it |
US8791253B2 (en) * | 2006-06-19 | 2014-07-29 | The Coca-Cola Company | Rebaudioside A composition and method for purifying rebaudioside A |
US9012626B2 (en) * | 2006-06-19 | 2015-04-21 | The Coca-Cola Company | Rebaudioside a composition and method for purifying rebaudioside a |
US20090312538A1 (en) * | 2006-07-06 | 2009-12-17 | Alembic Limited | process for the preparation of sucralose of high purity |
GB0702857D0 (en) * | 2007-01-19 | 2007-03-28 | Tate & Lyle Plc | Improved sucralose production method |
CN101260127B (zh) * | 2007-03-06 | 2011-04-20 | 盐城捷康三氯蔗糖制造有限公司 | 由三氯蔗糖-6-乙酯脱乙酰基合成三氯蔗糖的方法 |
US8030481B2 (en) | 2007-05-21 | 2011-10-04 | The Coca-Cola Company | Stevioside polymorphic and amorphous forms, methods for their formulation, and uses |
US20080299277A1 (en) * | 2007-06-01 | 2008-12-04 | Yaohai Chao | Sweetening Compositions |
AR070082A1 (es) * | 2008-01-04 | 2010-03-10 | Tate & Lyle Technology Ltd | Metodo para la produccion de sucralosa |
EP2254677A1 (en) * | 2008-03-20 | 2010-12-01 | Tate & Lyle Technology Limited | Removal of acids from tertiary amide solvents |
US8436157B2 (en) * | 2008-03-26 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
US8497367B2 (en) * | 2008-04-03 | 2013-07-30 | Tate & Lyle Technology Limited | Sucralose purification process |
AR071134A1 (es) * | 2008-04-03 | 2010-05-26 | Tate & Lyle Technology Ltd | Cristalizacion de sucralosa a partir de chorros que contienen sucralosa |
US20090259036A1 (en) * | 2008-04-03 | 2009-10-15 | Tate & Lyle Technology Limited | Extraction of less polar impurities from sucralose containing aqueous feed streams |
TW200946683A (en) * | 2008-04-03 | 2009-11-16 | Tate & Lyle Technology Ltd | A process for the purification of aqueous feed streams containing sucralose extraction efficiency |
WO2009140345A2 (en) * | 2008-05-15 | 2009-11-19 | Tate & Lyle Technology Ltd | Buffer rinsed sucralose crystals |
GB2468936B (en) | 2009-03-27 | 2011-09-07 | Mohamad Rami Radwan Jaber | Chlorination of sucrose-6-esters |
GB2469157B (en) | 2009-03-30 | 2011-07-06 | John Kerr | Process for removing dimethylamine during sucralose production |
GB2469158B (en) | 2009-03-31 | 2011-09-28 | Peter J Seaberg | Base-assisted formation of tin-sucrose adducts |
WO2011024199A1 (en) * | 2009-08-25 | 2011-03-03 | V.B. Medicare Pvt. Ltd. | Liquid sucralose sweetener composition |
GB2474310B (en) * | 2009-10-12 | 2012-02-29 | Tate & Lyle Technology Ltd | Process for the production of sucrose-6-ester |
GB2474311B (en) | 2009-10-12 | 2012-10-17 | Tate & Lyle Technology Ltd | Low temperature, single solvent process for the production of sucrose-6-ester |
GB201110520D0 (en) | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
CN102391319B (zh) * | 2011-10-14 | 2015-01-07 | 山东三和维信生物科技有限公司 | 三氯蔗糖的结晶方法 |
CN102391320B (zh) * | 2011-12-23 | 2014-03-19 | 盐城捷康三氯蔗糖制造有限公司 | 溶剂热回流纯化三氯蔗糖的方法 |
GB2503644A (en) * | 2012-05-03 | 2014-01-08 | British American Tobacco Co | Filter |
CN102977157A (zh) * | 2012-12-05 | 2013-03-20 | 溧阳维信生物科技有限公司 | 一种三氯蔗糖的结晶方法 |
CN103242384B (zh) * | 2013-05-27 | 2015-12-02 | 南通市常海食品添加剂有限公司 | 三氯蔗糖母液萃取工艺 |
US10227367B2 (en) | 2013-12-16 | 2019-03-12 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
WO2016020635A1 (en) | 2014-08-08 | 2016-02-11 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
GB2536480B (en) | 2015-03-17 | 2019-09-04 | Tate & Lyle Tech Ltd | DMF Distillation |
US9750811B2 (en) | 2015-09-15 | 2017-09-05 | Boveda, Inc. | Devices and methods for controlling headspace humidity and oxygen levels |
GB2551591B (en) | 2016-06-23 | 2019-08-07 | Tate & Lyle Tech Ltd | Liquid-liquid extraction of DMF |
BR112019007417A2 (pt) | 2016-10-12 | 2019-07-02 | Boveda Inc | conjunto de recipiente e fechamento com umidade predeterminada e método relacionado |
US12098015B2 (en) | 2016-10-12 | 2024-09-24 | Boveda Inc. | Device for controlling headspace humidity and methods for making the same |
CN109762030A (zh) * | 2019-03-06 | 2019-05-17 | 福州大学 | 一种三氯蔗糖的结晶方法 |
CN112574258A (zh) * | 2020-12-02 | 2021-03-30 | 安徽金禾实业股份有限公司 | 一种控制三氯蔗糖酸味的方法 |
Family Cites Families (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2065646B (en) | 1979-12-18 | 1983-10-05 | Tate & Lyle Ltd | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxygalactosucrose |
ZA807578B (en) * | 1979-12-18 | 1981-11-25 | Tate & Lyle Patent Holdings | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
EP0030804B1 (en) | 1979-12-18 | 1983-10-19 | TATE & LYLE PUBLIC LIMITED COMPANY | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
DE3062467D1 (en) | 1979-12-20 | 1983-04-28 | Tate & Lyle Plc | Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
ATE9355T1 (de) * | 1980-07-08 | 1984-09-15 | Tate & Lyle Public Limited Company | Verfahren zur herstellung von 4,1',6'-trichlor4,1',6'-trideoxygalactosucrose (tgs). |
GB8500862D0 (en) * | 1985-01-14 | 1985-02-20 | Tate & Lyle Plc | Composition |
GB8525953D0 (en) | 1985-10-21 | 1985-11-27 | Mcneilab Inc | Preparation of galactopyranoside |
GB8525954D0 (en) | 1985-10-21 | 1985-11-27 | Mcneilab Inc | Chlorination of carbohydrates &c alcohols |
DE3602090A1 (de) | 1986-01-24 | 1987-07-30 | Basf Ag | Verfahren zur herstellung von aromatischen block-copolyethern |
GB8617222D0 (en) * | 1986-07-15 | 1986-08-20 | Tate & Lyle Plc | Sweetener |
GB8627139D0 (en) * | 1986-11-13 | 1986-12-10 | Tate & Lyle Plc | Sweetening composition |
US4950746A (en) | 1988-07-18 | 1990-08-21 | Noramco, Inc. | Process for synthesizing sucrose derivatives by regioselective reaction |
GB8818430D0 (en) | 1988-08-03 | 1988-09-07 | Tate & Lyle Plc | Process |
GB8822674D0 (en) | 1988-09-27 | 1988-11-02 | Tate & Lyle Plc | Preparation of acylated sucrose derivatives |
US4980463A (en) * | 1989-07-18 | 1990-12-25 | Noramco, Inc. | Sucrose-6-ester chlorination |
US5034551A (en) * | 1990-04-23 | 1991-07-23 | Noramco, Inc. | Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds |
US5470969A (en) | 1990-08-27 | 1995-11-28 | Mcneil-Ppc, Inc. | Catalyzed sucrose-6-ester process |
JPH06155682A (ja) * | 1992-11-25 | 1994-06-03 | Kumagaya:Kk | 包装体 |
US5298611A (en) | 1993-03-12 | 1994-03-29 | Mcneil-Ppc, Inc. | Sucralose pentaester production |
US5498709A (en) | 1994-10-17 | 1996-03-12 | Mcneil-Ppc, Inc. | Production of sucralose without intermediate isolation of crystalline sucralose-6-ester |
US5874155A (en) * | 1995-06-07 | 1999-02-23 | American National Can Company | Easy-opening flexible packaging laminates and packaging materials made therefrom |
GB9517281D0 (en) * | 1995-08-23 | 1995-10-25 | Tate & Lyle Plc | Solid sucralose |
JP2000142799A (ja) * | 1998-11-12 | 2000-05-23 | Ma Packaging:Kk | 易開封袋 |
JP2000272060A (ja) * | 1999-03-25 | 2000-10-03 | Toyo Aluminium Kk | 化学製品包装用積層体と蓋材および袋 |
-
2001
- 2001-11-16 RU RU2003117710/04A patent/RU2279437C2/ru not_active IP Right Cessation
- 2001-11-16 MX MXPA03004402A patent/MXPA03004402A/es active IP Right Grant
- 2001-11-16 WO PCT/US2001/043491 patent/WO2002040495A2/en active Application Filing
- 2001-11-16 AU AU2691802A patent/AU2691802A/xx active Pending
- 2001-11-16 EP EP01995868A patent/EP1339728B1/en not_active Expired - Lifetime
- 2001-11-16 KR KR1020037006731A patent/KR100854528B1/ko not_active IP Right Cessation
- 2001-11-16 US US09/991,123 patent/US6646121B2/en not_active Expired - Lifetime
- 2001-11-16 JP JP2002543503A patent/JP4560637B2/ja not_active Expired - Fee Related
- 2001-11-16 CN CNB018220258A patent/CN1294139C/zh not_active Expired - Lifetime
- 2001-11-16 CA CA002429228A patent/CA2429228C/en not_active Expired - Fee Related
- 2001-11-16 BR BRPI0115482-6A patent/BR0115482B1/pt not_active IP Right Cessation
- 2001-11-16 AU AU2002226918A patent/AU2002226918B2/en not_active Ceased
-
2003
- 2003-08-01 US US10/632,876 patent/US6809198B2/en not_active Expired - Lifetime
-
2004
- 2004-08-17 US US10/919,656 patent/US20050013922A1/en not_active Abandoned
-
2006
- 2006-09-18 US US11/522,566 patent/US8017767B2/en not_active Expired - Fee Related
-
2009
- 2009-08-14 JP JP2009188092A patent/JP2009298803A/ja active Pending
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