JP2009198331A - 試料成分の分離方法及び分析方法 - Google Patents
試料成分の分離方法及び分析方法 Download PDFInfo
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Abstract
【解決手段】プレートとカバープレートの隙間に配置した試料溶液の溶媒を気化させ、カバープレートの周縁部に試料成分を析出させる。試料溶液はプレートとカバープレートの隙間に試料を配置し溶媒を導入して得られ、或いは、予め調製したものをプレートとカバープレートの隙間に導入する。好ましくは、プレート上に配置した試料又はスペーサの上にカバープレートを載置することでカバープレートに傾斜をつけ、プレートとカバープレートの最大隙間付近から毛細現象を利用して溶媒を導入する。試料成分をプレート上で析出した状態のままマイクロプローブを使用して分析する。
【選択図】図1
Description
津田孝雄著「クロマトグラフィー」丸善1995年
Claims (8)
- プレートとカバープレートの隙間に配置した試料溶液の溶媒を気化させ、前記カバープレートの周縁部に試料成分を析出させることを特徴とする試料成分の分離方法。
- 前記試料溶液は、前記プレートと前記カバープレートの隙間に試料を配置し溶媒を導入して得られたものであることを特徴とする請求項1記載の試料成分の分離方法。
- 前記カバープレートの一端側から前記溶媒を導入することを特徴とする請求項2記載の試料成分の分離方法。
- 前記プレート上に配置した前記試料の上に前記カバープレートを載置することで前記カバープレートに傾斜をつけ、前記プレートと前記カバープレートの最大隙間付近から毛細現象を利用して前記溶媒を導入することを特徴とする請求項3記載の試料成分の分離方法。
- 前記試料溶液は、予め調製したものを前記プレートと前記カバープレートの隙間に導入したものであることを特徴とする請求項1記載の試料成分の分離方法。
- 前記カバープレートの一端側から前記試料溶液を導入することを特徴とする請求項5記載の試料成分の分離方法。
- 前記プレート上に配置したスペーサの上に前記カバープレートを載置することで前記カバープレートに傾斜をつけ、前記プレートと前記カバープレートの最大隙間付近から毛細現象を利用して前記試料溶液を導入することを特徴とする請求項6記載の試料成分の分離方法。
- 前記請求項1〜7のいずれか1項記載の試料成分の分離方法を用いて前記カバープレートの周縁部に析出させた試料成分を、前記プレート上で析出した状態のままマイクロプローブを使用して分析することを特徴とする試料成分の分析方法。
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JP2009198331A true JP2009198331A (ja) | 2009-09-03 |
JP5028595B2 JP5028595B2 (ja) | 2012-09-19 |
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2002516982A (ja) * | 1998-03-07 | 2002-06-11 | ウォードロウ、スチーブン、シー | 抗凝固全血静止サンプルの分析 |
JP2004198388A (ja) * | 2002-10-25 | 2004-07-15 | Asahi Kasei Corp | 混合物の分離分析方法 |
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Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2002516982A (ja) * | 1998-03-07 | 2002-06-11 | ウォードロウ、スチーブン、シー | 抗凝固全血静止サンプルの分析 |
JP2004198388A (ja) * | 2002-10-25 | 2004-07-15 | Asahi Kasei Corp | 混合物の分離分析方法 |
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