JP2007178718A5 - - Google Patents

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JP2007178718A5
JP2007178718A5 JP2005377072A JP2005377072A JP2007178718A5 JP 2007178718 A5 JP2007178718 A5 JP 2007178718A5 JP 2005377072 A JP2005377072 A JP 2005377072A JP 2005377072 A JP2005377072 A JP 2005377072A JP 2007178718 A5 JP2007178718 A5 JP 2007178718A5
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Prior art keywords
rotor
toner
pulverization step
mechanical pulverizer
stator
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JP2005377072A
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JP4777063B2 (en
JP2007178718A (en
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Claims (10)

少なくとも結着樹脂及び着色剤を含有する組成物を溶融混練し、得られた混練物を冷却固化し、冷却固化物を粗粉砕して粗粉砕物を得る粗粉砕工程、得られた粗粉砕物を微粉砕して重量平均粒径3乃至8μm微粉砕物を得る微粉砕工程を有するトナーの製造方法において、
該微粉砕工程が、機械式粉砕機を用いて行われ、該機械式粉砕機は、少なくとも固定子と、中心回転軸に取り付けられた回転子とを有し、該固定子は該回転子を内包しており、該固定子の表面と該回転子の表面とは所定の間隙を有するように回転子は配置されて粉砕ゾーンを形成しており、粉砕ゾーンにおいて、該回転子の回転に伴って粗粉砕物が微粉砕され、
該機械式粉砕機の回転子の外周面及び固定子の内周面は、複数の凸部と、該凸部と該凸部との間に形成される凹部とを有し、
該機械式粉砕機の回転子の凸部と凸部との繰り返し距離をRa、該固定子の凸部と凸部との繰り返し距離をLaとしたとき、
RaとLaとが異なる範囲が存在するよう回転子及び固定子の構成を設定し、
該機械式粉砕機の回転子において、該凸部と該凸部との繰り返し距離Raが異なる範囲が存在するよう回転子の構成を設定する
ことを特徴とするトナーの製造方法。
A coarse pulverization step for obtaining a coarse pulverized product by melt-kneading a composition containing at least a binder resin and a colorant, cooling and solidifying the obtained kneaded product, and coarsely pulverizing the cooled solidified product, and the obtained coarse pulverized product In a method for producing a toner having a fine pulverization step of pulverizing the toner to obtain a finely pulverized product having a weight average particle diameter of 3 to 8 μm,
The fine pulverization step is performed using a mechanical pulverizer, and the mechanical pulverizer includes at least a stator and a rotor attached to a central rotating shaft, and the stator removes the rotor. The rotor is arranged so as to have a predetermined gap between the surface of the stator and the surface of the rotor to form a pulverization zone, and in the pulverization zone, the rotor rotates. The coarsely pulverized product is pulverized,
The outer peripheral surface of the rotor of the mechanical pulverizer and the inner peripheral surface of the stator have a plurality of convex portions and concave portions formed between the convex portions and the convex portions,
When the repetition distance between the convex part and the convex part of the rotor of the mechanical pulverizer is Ra, and the repetition distance between the convex part and the convex part of the stator is La,
Set the rotor and stator configurations so that there is a range where Ra and La are different,
A method for producing a toner, characterized in that, in the rotor of the mechanical pulverizer, the configuration of the rotor is set so that there is a range in which the repetition distance Ra between the convex portion and the convex portion is different.
該機械式粉砕機の固定子は、該凸部と該凸部との繰り返し距離Laが3.5mm未満であり、
該回転子の該凸部と該凸部との繰り返し距離Raが3.5mm以上のゾーンをLRa、該凸部と該凸部との繰り返し距離Raが3.5mm未満のゾーンをSRaとしたとき、LRa/SRaが0.1以上7.0以下であることを特徴とする請求項1に記載のトナーの製造方法。
The stator of the mechanical pulverizer has a repetition distance La between the convex portion and the convex portion of less than 3.5 mm,
When the zone where the repetition distance Ra between the projections of the rotor is 3.5 mm or more is LRa, and the zone where the repetition distance Ra between the projections and the projection is less than 3.5 mm is SRa The toner production method according to claim 1, wherein LRa / SRa is 0.1 or more and 7.0 or less.
該トナー粒子に使用される該結着樹脂は、少なくともポリエステルユニットを有する樹脂であることを特徴とする請求項1又は2に記載のトナーの製造方法。   3. The toner production method according to claim 1, wherein the binder resin used for the toner particles is a resin having at least a polyester unit. 該機械式粉砕機の固定子に、邪魔板リングを設け、該邪魔板リングと該回転子の間隔が0.3mm以上0.8mm以下であることを特徴とする請求項1乃至3のいずれかに記載のトナーの製造方法。   4. A baffle plate ring is provided on a stator of the mechanical pulverizer, and a distance between the baffle plate ring and the rotor is 0.3 mm or more and 0.8 mm or less. 2. A method for producing the toner according to 1. 該微粉砕工程の前に中粉砕工程があり、該中粉砕工程が、少なくとも機械式粉砕機を用いて行われ、得られた中粉砕物の重量平均粒径が50乃至500μmであることを特徴とする請求項1乃至4のいずれかに記載のトナーの製造方法。   There is an intermediate pulverization step before the fine pulverization step, the intermediate pulverization step is performed at least using a mechanical pulverizer, and the weight average particle size of the obtained intermediate pulverized product is 50 to 500 μm. The method for producing a toner according to any one of claims 1 to 4. 該中粉砕工程で使用する機械式粉砕機の回転子及び、該微粉砕工程で使用する機械式粉砕機の回転子は、外部から冷媒を、回転子軸端部の回転体継手より回転軸内部の通冷媒経路を介して端回転子から導入し、除熱した後に逆の端回転子から再び回転軸の通冷媒経路に戻す冷媒循環を設けていることを特徴とする請求項5に記載のトナーの製造方法。 The rotor of the mechanical pulverizer used in the intermediate pulverization step and the rotor of the mechanical pulverizer used in the fine pulverization step are configured so that the refrigerant is supplied from the outside to the inside of the rotary shaft from the rotor joint at the end of the rotor shaft. 6. The refrigerant circulation according to claim 5, further comprising: a refrigerant circulation which is introduced from the end rotor through the refrigerant passage and is removed from heat and then returned to the refrigerant passage of the rotating shaft from the opposite end rotor. Toner manufacturing method. 該微粉砕工程の後工程に、該微粉砕工程で使用する機械式粉砕機により得られた微粉砕物の粗粒分を分級するための分級工程を有し、粗粒分を粉砕工程に戻すシステムであることを特徴とする請求項1乃至6のいずれかに記載のトナーの製造方法。   There is a classification step for classifying the coarse particles of the finely pulverized product obtained by the mechanical pulverizer used in the fine pulverization step after the fine pulverization step, and the coarse particles are returned to the pulverization step. The toner manufacturing method according to claim 1, wherein the toner manufacturing method is a system. 該微粉砕工程の後工程、或いは該分級工程の後工程に、得られたトナー粒子を表面改質して表面改質粒子を得る表面改質工程を有することを特徴とする請求項7に記載のトナーの製造方法。 8. The method according to claim 7, further comprising a surface modification step for obtaining surface modified particles by modifying the surface of the obtained toner particles in a step subsequent to the fine pulverization step or a step subsequent to the classification step. Toner production method. 該表面改質工程が、回分式の表面改質装置を用いて行われ、該回分式の表面改質装置には、少なくとも所定粒径以下の微粉を装置外へ連続的に排出除去する分級手段と、機械式衝撃力を用いる表面改質手段と、該分級手段と該表面改質手段との間の空間を第一の空間と第二の空間とに二分する案内手段を有することを特徴とする請求項に記載のトナーの製造方法。 The surface modification step is performed using a batch type surface modification device, and the batch type surface modification device has a classification means for continuously discharging and removing at least fine powder having a predetermined particle size or less from the device. When a surface modification means using a mechanical impact force, to have a guide means you bisects the space between the classifying means and the surface modification means into a first space and the second space The method for producing a toner according to claim 8 , wherein the toner is a toner. 該回分式の表面改質装置において、表面改質粒子を得る際、トナー粒子を第一の空間に導入し、該分級手段により所定粒径以下の微粉を装置外へ連続的に排出除去しながら、第二の空間を経由して、機械式衝撃力を用いる該表面改質手段へ導入して表面改質処理を行い、再び第一の空間へ循環させることにより、一定時間分級と表面改質処理を繰り返すことを特徴とする請求項に記載のトナーの製造方法。 In the batch type surface modification device, when obtaining the surface modified particles, the toner particles are introduced into the first space, and fine particles having a predetermined particle diameter or less are continuously discharged and removed by the classification means to the outside of the device. via the second space, performs surface modification treatment is introduced into the surface modifying means using a mechanical impact force, by circulating back to the first space, a fixed time, classification and surface modification method for producing a toner according to claim 9, characterized that you repeat the quality process.
JP2005377072A 2005-12-28 2005-12-28 Toner production method Active JP4777063B2 (en)

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JP2007178718A JP2007178718A (en) 2007-07-12
JP2007178718A5 true JP2007178718A5 (en) 2009-02-19
JP4777063B2 JP4777063B2 (en) 2011-09-21

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4966813B2 (en) * 2007-10-19 2012-07-04 シャープ株式会社 Toner, developer, developing device, and image forming apparatus
JP5235442B2 (en) * 2008-02-12 2013-07-10 キヤノン株式会社 Toner production method
JP2009223011A (en) * 2008-03-17 2009-10-01 Canon Inc Method of manufacturing toner
JP2010066545A (en) * 2008-09-11 2010-03-25 Kyocera Mita Corp Toner for two-component developer and image forming apparatus
JP5472612B2 (en) 2009-01-07 2014-04-16 株式会社リコー Toner manufacturing method
JP5611410B2 (en) * 2013-04-30 2014-10-22 キヤノン株式会社 Toner production method

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