JP2005260279A - Polarization method of superconducting magnet device - Google Patents

Abstract

<P>PROBLEM TO BE SOLVED: To provide a polarization method of a superconducting magnet device which generates high magnetic field and can be utilized in various applications and apparatuses. <P>SOLUTION: In a polarizing method of a superconducting magnet device which polarizes a superconducting body 3 by carrying a pulsed current from a pulsed current source 5 to a polarized coil 4 disposed around the superconducting body 3, the superconducting body 3 is cooled to or below its transition temperature of superconductivity, and a pulsed current of which the peak current is determined is carried to the polarization coil 4 such that an applying field in which the minimum value of a magnetic filed entering the superconducting body 3 becomes equal to the maximum value of a magnetic field captured in the superconducting body 3 is generated. <P>COPYRIGHT: (C)2005,JPO&NCIPI

Description

  The present invention relates to a superconducting magnet device, and more particularly to a magnetizing method for a superconducting magnet device used as a magnet by capturing a high magnetic field in a bulk high-temperature superconductor.

  With some high-temperature superconductors such as Y-systems, it has become possible to obtain a large magnetic field exceeding 1 T even at liquid nitrogen temperature, which is impossible with a permanent magnet, by controlling the structure. Further, if it is cooled to a low temperature, a larger magnetic field can be captured, and improvement in characteristics is expected by material development. Therefore, recently, use as a powerful magnet has been studied.

  Well, as a method of making a bulk superconductor into a magnet, a so-called FC that cools below its superconducting transition temperature (Tc) in a state where a magnetic field is applied to the superconductor, and cooling below the superconducting transition temperature of the superconductor. After that, there is a so-called ZFC method in which a magnetic field is applied from the outside to enter the superconductor. In any case, it is necessary to apply a magnetic field equal to or higher than the magnetic field to be captured by the superconductor at one time, and thereafter, to maintain the magnetic field captured by the superconductor, the temperature is maintained below the magnetization temperature. There is a need.

Conventionally, the above-described FC has been generally used as a magnetization method for capturing a magnetic field in a high-temperature superconductor for the purpose of evaluating its characteristics. Japanese Patent Application Laid-Open No. 7-111213 made a superconductor capture a magnetic field by FC and combined a coil and a superconductor into a magnet.
Japanese Patent Laid-Open No. 7-111213

  ZFC, on the other hand, slowly applies an external magnetic field to the superconductor and then slowly decreases it to 0. Since the superconductor is already in a superconducting state due to cooling, a certain amount is applied when an external magnetic field is applied to the superconductor. Since a magnetic field is eliminated, an applied magnetic field larger than the FC is required for magnetization, so when magnetizing using a stationary magnetic field, practically it was performed by FC instead of ZFC. .

Further, as a special method of ZFC, a method of magnetizing with a pulsed magnetic field instead of a stationary magnetic field is disclosed in JP-A-6-168823. This method is effective for magnetizing a superconductor with a simple coil.
JP-A-6-168823

Apart from the method of directly using the above bulk-shaped superconductor as a magnet, JP-A-5-175034 discloses a method of processing a bulk superconductor into a shape equivalent to a coil and energizing it to make a magnet. Is disclosed.
Japanese Patent Laid-Open No. 5-175034

  In the conventional FC described above, a stationary magnetic field must be applied to the superconductor while the superconductor is cooled, but the stationary magnetic field is sufficiently applied because the magnetic field that can be generated by a simple device is small. There is a problem that a magnetic field cannot be obtained, and the magnetic field that can be captured by the superconductor cannot greatly exceed the magnetic field generated by a normal permanent magnet.

  In the above-mentioned conventional FC, the method using a Nb-Ti superconducting coil is a method that can constantly generate a high magnetic field, but this superconducting coil needs to be cooled to a very low temperature, so that the superconductor can capture a high magnetic field. The whole device became a big one. Also, in FC, superconductors are cooled while a magnetic field is applied, so it took a long time to magnetize. Furthermore, since it is necessary to place the superconductor in a place where it is cooled after magnetization, there is also a problem that the places where it can be used are extremely limited. As described above, in the above-described conventional FC, it has been difficult to use the superconductor itself as a strong magnet inside the apparatus or the like.

  In addition, when a stationary magnetic field is used in the conventional ZFC, the same problems as in the FC described above remain as they are, and an applied magnetic field larger than that of the FC is required, which is more difficult than the FC described above. It was.

  In the conventional pulse magnetic field disclosed in JP-A-6-168823, since the coil and the superconductor are both contained in the same refrigerant container, if the magnetizing coil generates heat during magnetization, a large amount of There are problems that the refrigerant evaporates or that the temperature of the superconductor rises and that the magnet performance decreases, and that maintenance of the refrigerant is necessary.

  Furthermore, in the method of processing the above bulk superconductor into a shape equivalent to a coil, it is necessary to perform complicated processing on the superconductor, which is very difficult and costly to process with a high-temperature superconductor made of ceramics. It was. In addition, the material is easily deteriorated during processing, and it is difficult to obtain a material with stable characteristics.

  As described above, in the above prior art, even if there is a bulk-shaped superconductor with good characteristics, it has been difficult to use it in various devices as a magnet for generating a high magnetic field.

  Therefore, the present inventors paid attention to the fact that the characteristics of the superconductor are improved as the temperature is lowered, and that the superconductor can be magnetized with a simple apparatus in pulse magnetization. It is an object of the present invention to capture a high magnetic field that has not been obtained by a simple apparatus and method so that a superconductor can be used as a magnet in various applications and devices.

  In order to solve the above problems, the present inventors have made efforts to improve the method of pulse magnetization. Conventionally, pulse magnetization has the property of excluding the magnetic field invaded by the superconductor when magnetized by applying a magnetic field to a superconductor cooled in a non-magnetized state. It was thought that the space between the magnetic coil and the superconductor had to be as small as possible. However, in order to use the superconductor as a magnet in various devices, it is desirable that the magnetized coil and the superconductor can be arranged more freely. Therefore, the present inventors have made in mind to construct a magnet device of various freely arranged, as a result of earnestly examining the arrangement of the superconductor and the magnetizing coil, the magnitude and application time of the pulse magnetic field, The following technical measures were found to be extremely effective.

The magnetization method of the superconducting magnet device of the present invention (the first invention according to claim 1) is as follows:
A magnetizing method for a superconducting magnet device that magnetizes the superconductor by passing a pulse current through a magnetizing coil disposed around the superconductor,
Cooling the superconductor below the superconducting transition temperature,
A pulse current whose peak value is determined so that an applied magnetic field is generated such that the minimum value of the magnetic field penetrating into the superconductor and the maximum value of the magnetic field trapped in the superconductor are generated, The coil is energized.

The magnetization method of the superconducting magnet device of the present invention (the second invention according to claim 2) is as follows:
In the first invention,
The superconductor is a RE-Ba-Cu-O-based superconductor (RE is Y or a rare earth element and a combination of these elements), and has a large magnetic field that can be captured and is configured to generate a high magnetic field. It is what.

The magnetization method of the superconducting magnet device of the present invention (the third invention according to claim 3) is as follows:
In the second invention,
The superconductor captures a magnetic field exceeding IT.

A superconducting magnet device according to a fourth aspect of the present invention is:
A cold head for cooling disposed in an insulated container;
A superconductor disposed in the container in contact with the cold head;
A magnetizing coil for applying a magnetic field to the superconductor;
The magnetizing coil includes a pulse power source for supplying a pulse current to the magnetizing coil.

The superconducting magnet device according to the fifth aspect of the present invention is:
In the fourth invention,
The cold head is cooled by a refrigerator, and is configured to cool the superconductor to a superconducting transition temperature or lower by heat conduction.

The superconducting magnet device according to the sixth aspect of the present invention is:
In the fifth invention,
The magnetized coil is disposed outside the heat insulating container and insulated from the superconductor.

A superconducting magnet device according to a seventh aspect of the present invention is:
In the sixth aspect of the invention, the pulse power source is configured such that a pulse current is controlled so as to be an applied magnetic field necessary for obtaining a target magnetic field distribution captured in the superconductor.

The superconducting magnet device according to the eighth aspect of the present invention is:
In the seventh invention,
The superconductor is constituted by a bulk superconductor of RE-Ba-Cu-O type (RE is Y or a rare earth element and a combination of these elements).

The superconducting magnet device of the ninth invention of the present invention is
A refrigerant container filled with a refrigerant capable of cooling the superconductor to a superconducting transition temperature or lower;
A superconductor disposed in the refrigerant container;
A magnetizing coil for applying a magnetic field to the superconductor;
It consists of a pulse power supply that supplies a pulse current to the magnetizing coil,
The magnetized coil is outside the refrigerant container and insulated from the superconductor.

The magnetizing method of the superconducting magnet device according to the tenth aspect of the present invention is:
Cooling the superconductor below the superconducting transition temperature,
A pulse current whose peak value is determined is applied to the magnetizing coil so that an applied magnetic field is generated such that the minimum value of the magnetic field penetrating into the superconductor is equal to or greater than the maximum value of the magnetic field trapped in the superconductor. Energize.

The magnetizing method of the superconducting magnet device according to the eleventh aspect of the present invention comprises:
In the tenth invention,
A pulse current whose peak value is determined is applied to the magnetizing coil so that an applied magnetic field is generated such that the maximum value of the magnetic field trapped in the superconductor is equal to the minimum value of the magnetic field penetrating the superconductor. Energize.

The magnetizing method of the superconducting magnet device according to the twelfth aspect of the present invention comprises:
In the tenth invention,
The energizing time of the pulse current energized to the magnetizing coil is controlled to be within a certain time.

  In the magnetizing method of the superconducting magnet device according to the first aspect of the present invention, the minimum value of the magnetic field penetrating into the superconductor cooled below the superconducting transition temperature is equal to the maximum value of the magnetic field trapped in the superconductor. In order to apply a pulse current whose peak value is determined so as to generate an applied magnetic field to the magnetizing coil disposed around the superconductor, only a necessary and sufficient magnetic field is present in the superconductor. Since it does not generate heat due to the penetration of an extra magnetic field, the maximum magnetic field that can be captured from the characteristics of the superconductor can be captured. Furthermore, since the magnetizing coil that can generate the minimum necessary magnetic field is used, there is an effect that the size of the magnetizing coil can be made as small as possible.

  The superconducting magnet apparatus of the second invention having the above-described configuration is the method of magnetizing the superconductor according to the first invention, wherein the superconductor is an RE-Ba-Cu-O system (RE is Y or a rare earth element and a combination of these elements). ), The magnetic field that can be captured is large, and a high magnetic field can be generated.

  The magnetizing method of the superconducting magnet device according to the third aspect of the present invention having the above-described configuration is that, in the second aspect, the superconductor captures a magnetic field exceeding IT, so that a sufficient magnetic field can be captured by the superconductor. There is an effect that it can be captured.

  In the superconducting magnet device according to the fourth aspect of the present invention, a pulse magnetic field generated by the magnetizing coil is disposed in the heat insulating container by applying a pulse current to the magnetizing coil by the pulse power source. It is applied to the superconductor cooled to a superconducting transition temperature or lower by the cold head for cooling, and the magnetic field is captured by the superconductor to function as a magnet. The magnitude of the magnetic field captured by the superconductor can be controlled by the magnitude of the magnetic field generated by the magnetizing coil. In addition, a superconductor can capture a magnetic field if a pulsed magnetic field is applied even once, and the pulse width may be several milliseconds or less. Therefore, in the apparatus of the present invention using pulse magnetization, a small and simple magnetizing coil is used. There is an effect that the superconductor can be magnetized. In addition, since the superconductor is cooled by the cold head, the temperature is not limited as in the case of using a refrigerant, and the superconductor can be used at any operating temperature. Since the superconductor generally has higher characteristics as the temperature is lower, the use of a cold head has an effect of generating a larger magnetic field by lowering the operating temperature.

  The superconducting magnet device according to a fifth aspect of the present invention configured as described above is the structure according to the fourth aspect, wherein the cold head is cooled by a refrigerator, and the superconductor is cooled to a superconducting transition temperature or lower by heat conduction. . In the apparatus of the present invention, since the cold head is cooled by the refrigerator, the temperature of the cold head and the superconductor can be freely and automatically controlled by combining with the heater. Furthermore, there is an effect that the maintenance and management of the refrigerant becomes unnecessary.

  In the superconducting magnet device of the sixth invention having the above-described configuration, in the configuration of the fifth invention, the magnetized coil is disposed outside the heat insulating container and insulated from the superconductor. The superconductor to be magnetized has the effect that it is not affected by the heat generated by the coil when a pulse current is applied to the magnetizing coil during magnetization. That is, since an excessive temperature rise of the superconductor can be avoided, there is an effect that more stable pulse magnetization is possible. Furthermore, since the magnetizing coil is outside the heat insulating container containing the superconductor, after magnetization, the portion of the heat insulating container including the superconductor that captures the magnetic field and functions as a magnet, the magnetizing coil, and the magnetizing There is also an effect that it can be easily separated from the power source, and the magnetic field can be easily used in various applications.

  In the superconducting magnet device of the seventh invention configured as described above, in the configuration of the sixth invention, the pulse current is controlled so as to be an applied magnetic field necessary for obtaining a target magnetic field distribution captured in the superconductor. Thus, there is an effect that a superconductor can capture a necessary magnetic field by one pulse magnetization and the magnetic field can be immediately used for various applications.

  In the superconducting magnet device of the eighth invention having the above-described configuration, in the configuration of the seventh invention, the superconductor is an RE-Ba-Cu-O system (RE is Y or a rare earth element and a combination of these elements). Since it is composed of a bulk superconductor, there is an effect that a large magnetic field can be captured by its strong pinning force.

  The superconducting magnet device of the ninth invention having the above-described configuration is a refrigerant container filled with a refrigerant capable of cooling the superconductor to a superconducting transition temperature or lower, a superconductor disposed in the refrigerant container, and a magnetic field applied to the superconductor. Since the magnetizing coil is outside the refrigerant container and is insulated from the superconductor, the magnetizing coil is applied to the magnetizing coil and a pulse power source for applying a pulse current to the magnetizing coil. The superconductor that is magnetized has the effect that it is not affected by the heat generated by the coil when the magnetized coil is magnetized by applying a pulse current. That is, since an excessive temperature rise of the superconductor can be avoided, there is an effect that more stable pulse magnetization is possible. Furthermore, since the magnetizing coil is outside the refrigerant container containing the superconductor, after magnetization, the portion of the refrigerant container including the superconductor that functions as a magnet by capturing the magnetic field, the magnetizing coil, and the magnetizing There is also an effect that it can be easily separated from the power source, and the magnetic field can be easily used in various applications.

  The method for magnetizing the superconducting magnet device according to the tenth aspect of the present invention comprises cooling the superconductor to a superconducting transition temperature or lower, and the minimum value of the magnetic field penetrating into the superconductor is the maximum value of the magnetic field trapped in the superconductor. In order to apply a pulse current whose peak value is determined to the magnetizing coil so as to generate an applied magnetic field as described above, a magnetic field that is substantially close to the maximum magnetic field that can be captured determined by the characteristics of the superconductor is set. In addition to being able to be captured, there is an effect that a change in the captured magnetic field of the superconducting magnet device is less than immediately after magnetization.

In the magnetizing method of the superconducting magnet device of the eleventh invention having the above-described configuration, the maximum value of the magnetic field trapped in the superconductor is equal to the minimum value of the magnetic field penetrating into the superconductor in the configuration of the tenth invention. Since a pulse current whose peak value is determined is applied to the magnetizing coil so that such an applied magnetic field is generated, only a necessary and sufficient magnetic field penetrates into the superconductor, and heat is generated due to the penetration of an extra magnetic field. Therefore, the maximum magnetic field that can be captured from the characteristics of the superconductor can be captured. Further, since a magnetized coil that can generate a minimum necessary magnetic field is used, there is an effect that the size of the magnetized coil can be made as small as possible.

  The magnetizing method of the superconducting magnet device of the twelfth aspect of the present invention having the above configuration is controlled so that the energization time of the pulse current energized to the magnetizing coil is within a certain time in the configuration of the tenth aspect of the invention. The time required for the magnetizing coil to generate heat during magnetization is short. Therefore, even if a large current is passed through a magnetized coil made of thin wires, the amount of heat generation does not increase and fusing does not occur. Therefore, a simple magnetized coil can easily magnetize a large magnetic field. is there.

  The best mode for carrying out the present invention will be described below with reference to the accompanying drawings.

  As shown in FIG. 1, the superconducting magnet device and the method of magnetizing the superconducting magnet device according to the first embodiment include a cold head 2 disposed in a heat insulating container 1 cooled by a refrigerator 20 and the heat insulating material. A superconductor 3 disposed in contact with the cold head 2 in the container 1 and cooled to a superconducting transition temperature or lower by heat conduction, and a magnetic field applied to the superconductor 3 disposed outside the heat insulating container 1. And a pulse power source 5 for applying a pulse current controlled to be an applied magnetic field in consideration of the magnetic field trapped in the superconductor 3. .

  As shown in FIG. 1, the inside of the heat insulating container 1 is evacuated and has a structure for insulating the superconductor 3 and the cold head 2 from the outside of the heat insulating container.

  The refrigerator 20 is constituted by a GM refrigerator using a regenerative refrigeration cycle developed by Gifford McMahon as shown in FIG. 2, a compressor 21 for compressing gas, and a discharge port of the compressor 21. A high-pressure valve 22 that communicates with the suction port, a low-pressure valve 23 that communicates with the suction port, a displacer 26 as a piston that is inserted in the cylinder 24 and reciprocates by a drive mechanism 25 including a stepping motor and a crank, and the cylinder 24. And a regenerator 27 communicating with the high-pressure valve 22 and the low-pressure valve 23, and a refrigeration unit 28 constituting the cold head 2 formed between the regenerator 27 and one chamber 241 of the cylinder 24. .

  As shown in FIG. 3 showing the principle of operation, the displacer 26 reciprocates within the cylinder 24 by several tens of rpm by the stepping motor, and the high pressure valve 22 and the low pressure valve 23 are synchronized with the reciprocating motion of the displacer 26. Open / close controlled.

  In FIG. 3, when the displacer 26 is at the bottom, the high pressure valve 22 opens and high pressure gas enters the upper space V1 of the displacer 26, and then the displacer 26 rises so that the gas remains at the same pressure. Move to V2. At this time, since the temperature of the lower space is low, the gas contracts and extra gas is replenished.

  When the high-pressure valve 22 is closed and the low-pressure valve 23 is opened at the position where the displacer 26 is almost lifted, the gas is discharged to the low-pressure side and expanded to obtain refrigeration in the lower space V2 having the maximum volume V. Next, after the displacer 26 is lowered and the gas in the lower space V2 is discharged, one cycle is completed by closing the low pressure valve 23 and opening the high pressure valve 22.

  The refrigerator 20 is a one-stage GM refrigerator, the refrigeration output at 80K is 100 W, and the lowest temperature reached by the refrigerator alone is 25K. The lowest temperature reached in the state where the superconductor 3, the coil 4, and the cold head 2 of the present embodiment are attached is 30K.

  As shown in FIG. 1, the superconductor 3 has a copper block 30 having a sufficient thickness placed on the upper surface of the cold head 2 constituted by the freezing unit 28 of the refrigerator 20, and is placed thereon. Placed. Note that a heater wire is wound around the cold head 2, and temperature control is performed using the heater wire so that a desired temperature up to the lowest temperature can be maintained.

  The superconductor 3 is prepared by weighing a fine powder of YBa2Cu3O7-x and Y2BaCuO5 at a molar ratio of 3: 2, and adding 0.5 wt% Pt to this and mixing it sufficiently to form a raw material powder. A Y-based molten bulk having an outer diameter of 35 mm and a thickness of 14 mm obtained by powdering and heat treatment by a so-called melting method was used.

  When this superconductor was cooled and magnetized with liquid nitrogen in a 1 T static magnetic field, it was able to capture a maximum 0.5 T magnetic field.

  The pulse power source 5 discharges the electric charge accumulated in the capacitor 51 and can pass a current only in one direction by rectification by the diode 52. The maximum current that can be generated by this power supply is 10,000 amperes (A).

  The magnetizing coil 4 has 50 turns, a bobbin having an inner diameter of 45 mm and an outer diameter of 60 mm, which is impregnated with resin and fixed, and a terminal 53 of the pulse power source is provided by a current supply line 41 for supplying a pulse current. It is connected to.

  Since the magnetized coil can calculate the generated magnetic field (coil constant) per unit current value of the energized current from its shape, the generated magnetic field can be obtained by examining the current flowing through the coil. When the magnetized coil 4 coil is energized with 10000 amperes (A), a magnetic field of 10 T can be generated in the center of the coil. As shown in FIG. 4, in the pulse magnetization, only a current flows instantaneously through the magnetizing coil, and the current value becomes 0 immediately after reaching the maximum value at the rising time A immediately after the start of energization. That is, the magnetizing coil 4 generates a magnetic field only for a moment when pulse magnetizing is performed, and the generated magnetic field changes with time in accordance with a change in the value of the flowing current. Therefore, the magnetic field generated by the magnetizing coil when the pulse current indicated by the line B in FIG. 4 becomes maximum is defined as the applied magnetic field of the superconductor 3.

  An experiment conducted to determine the optimum applied magnetic field for causing the superconducting 3 to capture a large magnetic field in the first embodiment will be described below. Since the applied magnetic field is determined by the magnitude of the pulse current supplied to the magnetizing coil 4, the magnitude of the pulse current supplied from the pulse power source 5 to the magnetizing coil 4 is changed in various ways to magnetize the superconductor 3. The captured magnetic fields in each case were compared. In this experiment, the temperature of the superconductor was maintained at 77 K, which is the same as the liquid nitrogen temperature.

  FIG. 5 shows the generation of the pulse magnetic field shown in FIG. 4 when the superconductor 3 is magnetized with an applied magnetic field of 0.64 T (A), 1.13 T (B) and 1.86 T (C). The magnetic field distribution inside the superconductor 3 at each time point (1) during rising, (2) during peak, (3) during falling, and (4) after stabilization.

  From FIG. 5 above, the magnetic field applied to the inside of the superconductor is shielded because the applied magnetic field is shielded because the magnetic flux lines entering the inside of the superconductor always receive a force in a direction that prevents its movement during the pulse magnetization process. Indicates that the applied magnetic field applied to the outer surface of the superconductor (that is, the maximum magnetic field generated by the magnetizing coil) needs to be sufficiently increased. That is, in the case of A or B in FIG. 5, since a sufficient magnetic field does not enter the central portion of the superconductor, a magnetic field that can be captured cannot be sufficiently captured from the characteristics of the superconductor.

  Therefore, as is clear from FIG. 5, when an external magnetic field is applied so that a magnetic field larger than the magnetic field that can be captured in the central portion where the captured magnetic field of the superconductor 3 is maximized, that is, from FIG. It can be seen that when a magnetic field of 1.86 T or more is applied, the superconductor can sufficiently capture a magnetic field that can be captured.

  Next, FIG. 6 shows a result of comparison of the trapped magnetic field of the superconductor 3 when a larger magnetic field is applied to the superconductor 3 and when the 1.86 T magnetic field is applied. From this, it can be seen that when a magnetic field larger than necessary is applied to the superconductor 3, the magnetic field that can be captured decreases. This is because when a 4.97 T magnetic field is applied to the superconductor 3, an extra magnetic field penetrates into the superconductor 3 compared to the magnetic field that can be captured, and therefore a large amount of magnetic flux lines move to cause the superconductor 3 to move. This is because heat is generated inside the core, the temperature inside the superconductor 3 increases, and the pinning force of the magnetic flux lines decreases.

The optimum pulse width of the pulse current will be discussed below.
That is, the difference in pulse magnetization characteristics depending on the pulse width and coil shape will be examined. When a large-capacity capacitor is used in the pulse power supply, the magnitude of the generated magnetic field can be controlled by the charge voltage. If the magnetizing coils are the same, increasing the charging voltage will increase the generated pulse magnetic field in proportion to the charging voltage, but the pulse width will hardly change.

  Further, if the number of turns of the magnetizing coil is increased or the inner diameter of the magnetizing coil is increased, the pulse width becomes longer. FIG. 7 shows pulse current waveforms of three typical types of magnetized coils produced. Using these various magnetized coils, the influence on the magnetizing characteristics of the superconductor was investigated.

  As a result, using a magnetized coil with the same inner diameter and different number of turns and magnetizing the superconductor with a pulsed magnetic field with different rise times, the pulse width is within the range of 0.8 msec to 2.4 msec. It was found that there was no difference in the magnetization characteristics due to.

  Even when a superconductor having an outer diameter of 34 mm was magnetized with a magnetizing coil having an inner diameter of 35 mm and 55 mm and the same number of turns, there was no difference in the applied magnetic field dependence of the trapped magnetic field.

  From these results, it was found that the trapping magnetic field of the superconductor by pulse magnetization is determined only by the magnitude of the applied magnetic field applied to the superconductor, regardless of the pulse width and the shape of the magnetizing coil.

  In order to investigate the optimum magnetization conditions in the first embodiment, it was examined how the captured magnetic field distribution changes when the applied magnetic field is changed. In order to compare with the above-mentioned prior art, the trapped magnetic field after magnetization of the same superconductor is measured by changing the applied magnetic field at the liquid nitrogen temperature of 77K with the pulse magnetization of FC, ZFC and the first embodiment. Compared.

  In order to compare the characteristics of the whole sample, a magnetic field sensor was scanned on the surface of the sample, the strength of the magnetic field captured at each point on the sample was measured, and the total amount of magnetic flux captured by the sample was obtained. When the same sample is magnetized with various applied magnetic fields, and the amount of trapped magnetic flux is measured and plotted, the result is as shown in FIG.

  From this, it can be seen that in the case of pulse magnetization, there is an optimum applied magnetic field such as 1.9 T in this sample, and when a magnetic field higher than that is applied, the magnetic field captured by the sample decreases. From this, it was found that when the superconductor is used by capturing a strong magnetic field, it is necessary to investigate the optimum applied magnetic field in advance by measuring the applied magnetic field dependence of the captured magnetic field of the superconductor to be used.

  In some applications, the superconductor is magnetized with an applied magnetic field larger than the applied magnetic field that can capture the largest amount of magnetic field. The trapping magnetic field of the superconductor decreases due to a so-called creep phenomenon that decreases logarithmically at a constant rate immediately after magnetization. When a certain amount of time has passed after magnetization, the amount of decrease will be practically satisfactory.However, if the superconductor is magnetized with an applied magnetic field that is larger than the applied magnetic field that can capture the largest amount of magnetic field by pulse magnetization. Compared to other magnetization methods, the amount of decrease in the magnetic field is less than immediately after magnetization. Therefore, in an application in which stability is more important than the strength of the trapping magnetic field, it is effective to magnetize the superconductor with an applied magnetic field that is larger than the applied magnetic field that can capture the most magnetic field.

The magnetization method of the superconducting magnet device of the first embodiment will be described below.
First, the superconductor 3 is cooled to a superconducting transition temperature or lower by the cold head cooled by the refrigerator 20 through the copper block 30. After the temperature becomes sufficiently steady, a pulsed current similar to that shown in FIG. 4 is applied to the magnetizing coil 4 from the pulse power source 5 and a magnetic field is applied to the superconductor 3.

  By applying a magnetic field, the superconductor 3 captures the magnetic field and becomes a magnet. However, while maintaining a constant temperature, the superconducting magnet has a slight decrease in the generated magnetic field due to a phenomenon called magnetic flux creep. It keeps a substantially constant magnetic field. Thereafter, if necessary, the current supply line 41 can be removed at the terminal 53 to separate the pulse power supply 5 from the superconducting magnet. It is also possible to re-magnetize for the purpose of changing the generated magnetic field.

The characteristics of the superconducting magnet device thus obtained were as follows.
FIG. 9 shows the result of measuring the magnitude of the captured magnetic field with the magnetic field sensor at two locations on the superconductor when the applied magnetic field is sequentially increased. The measurement location is shown in FIG. In this measurement, the superconductor was cooled to 50K.

  From this, when the applied magnetic field is increased, the magnetic field trapped at the periphery of the superconductor first increases first, but when the applied magnetic field exceeds 3T, the magnetic field trapped at the center of the superconductor increases rapidly. , Exceeding the magnetic field trapped at the periphery of the superconductor. Furthermore, it can be seen that when the applied magnetic field exceeds 4T, the captured magnetic field decreases regardless of the location.

  Thus, in the first embodiment, the superconductor 3 can capture a 1.5 T magnetic field by applying a pulse magnetic field of 3.8 T, and a superconducting magnet apparatus with a maximum generated magnetic field of 1.5 T is obtained. At the liquid nitrogen temperature (77K), the magnetic field that can be captured by the superconductor 3 is 0.5T, and the superconducting magnet device of the present embodiment using a refrigerator uses the same superconductor and has a performance three times that of the liquid nitrogen temperature. Is obtained. Further, by using the applied magnetic field dependence data of the trapped magnetic field of the superconductor 3, a superconducting magnet device having an arbitrary generated magnetic field in the range up to the maximum trapped magnetic field at the operating temperature of the superconductor 3 can be obtained. it can.

  Further, when the time change of the trapped magnetic field of the superconductor after magnetization was examined, the result as shown in FIG. 11 was obtained. From this, it was found that when the applied magnetic field exceeds 3.8T, the trapped magnetic field of the superconductor is reduced, but the attenuation after magnetization is considerably reduced. That is, by increasing the applied magnetic field, a superconducting magnet device with a stable generated magnetic field with little attenuation of the generated magnetic field can be obtained.

  The superconducting magnet device according to the first embodiment having the above-described effect is located close to the superconductor 3 in contact with the cold head 2 disposed in the heat insulating container 1 and directly cooled to a low temperature. The magnetizing coil 4 disposed in the magnet captures the magnetic field generated instantaneously by energization of the pulse current as it is to make a magnet, and the superconductor can be easily magnetized to generate a high magnetic field. There is an effect that it can be used in various applications and devices.

  Moreover, since the cold head 2 is cooled by the refrigerator 20 in the superconducting magnet device of the first embodiment, a temperature lower than the temperature of liquid nitrogen used as a refrigerant can be easily realized, and the same superconductor is used. Even if it uses liquid nitrogen for a refrigerant | coolant, there exists an effect that a bigger magnetic field can be generated.

  That is, since the superconductor 3 is cooled by the cold head 2 which is the freezing section of the refrigerator 20 through the copper block 30 having a sufficient capacity, a heater wire is disposed on the cold head 2 and is about 30K. It is possible to magnetize at any operating temperature up to the above, and by controlling the output of the heater wire, the temperature can be automatically maintained and managed, and the low temperature can be used very easily. In the above prior art using a liquid refrigerant, the operating temperature is limited to the temperature of the refrigerant (liquid oxygen 90K, liquid nitrogen 77K, liquid neon 27K, liquid hydrogen 20K, liquid helium 4K). However, only liquid nitrogen can be used easily. Therefore, the device of this embodiment that can operate in a temperature range of 77K or less where the characteristics of the superconductor are increased can easily generate a strong magnetic field even when the same superconductor is used, compared to the case where liquid refrigerant is used. There is an effect.

  In the superconducting magnet device of the first embodiment, since the superconductor 3 is directly cooled by the cold head 2 of the refrigerator 20, the refrigerant container in the prior art becomes unnecessary, and the superconductor 3 is correspondingly reduced. Since the distance to the outside of the vacuum heat insulating container 1 can be shortened, there is an effect that the magnetic field captured by the superconductor can be used more effectively in various applications and devices.

  Furthermore, in the superconducting magnet apparatus of the first embodiment, the magnetizing coil 4 to which a pulse current from the pulse power source 5 is supplied is disposed outside the vacuum heat insulating container 1 and is insulated from the superconductor 3. Therefore, since the superconductor 3 is not affected by the heat generated by the magnetizing coil 4 during magnetization, the performance of the superconducting magnet device is improved.

  Furthermore, in the superconducting magnet device of the first embodiment, the superconductor 3 is constituted by a bulk superconductor of RE-Ba-Cu-O type (RE is Y or a rare earth element and a combination of these elements). Therefore, the magnetic field that can be captured is large, and the effect of generating a high magnetic field is achieved.

  Furthermore, the superconducting magnet magnetization method of the first embodiment is such that an applied magnetic field is generated such that the minimum value of the magnetic field penetrating into the superconductor 3 is equal to or greater than the maximum value of the magnetic field trapped in the superconductor. In addition, since the magnetizing coil 4 is energized with a pulse current whose peak value is determined, a magnetic field substantially close to the maximum magnetic field that can be captured determined by the characteristics of the superconductor can be captured, and the superconducting magnet can be captured immediately after magnetization. The change in the trapped magnetic field of the device is reduced, a stable magnetic field can be generated, and the magnet performance of the superconducting magnet device is improved.

  Further, the superconducting magnet magnetization method of the first embodiment generates an applied magnetic field in which the maximum value of the magnetic field trapped in the superconductor 3 is equal to the minimum value of the magnetic field penetrating into the superconductor 3. As described above, since a pulse current whose peak value is determined is passed through the magnetizing coil 4, only a necessary and sufficient magnetic field penetrates into the superconductor, and heat generation in the superconductor 3 occurs due to the penetration of an extra magnetic field. Therefore, the maximum magnetic field that can be captured from the characteristics of the superconductor 3 can be captured, and the magnet performance of the superconducting magnet device can be improved. Furthermore, by using a magnetizing coil that can generate the minimum necessary magnetic field, the size of the magnetizing coil can be made as small as possible, and an effect is achieved that a simpler superconducting magnet device can be designed.

  Furthermore, the superconducting magnet magnetizing method of the first embodiment is controlled so that the energizing time of the pulse current energized to the magnetizing coil 4 is within a certain time. The calorific value is below a certain level. Therefore, a large current can be passed through a simple coil, and a large applied magnetic field necessary for capturing a large magnetic field in the superconductor 3 can be easily generated.

  As shown in FIG. 12, the superconducting magnet device and the magnetizing method of the superconducting magnet device according to the second embodiment include a refrigerant container 6 filled with a refrigerant capable of cooling the superconductor 3 to a superconducting transition temperature or lower, and the refrigerant. The superconductor 3 disposed in the container 6, a magnetizing coil 4 for applying a magnetic field to the superconductor 3, and a pulse power source 5 for applying a pulse current to the magnetizing coil 4, The magnetic coil 4 is disposed outside the refrigerant container 6.

  The refrigerant container 6 is filled with liquid nitrogen as a refrigerant. The superconductor 3, the magnetizing coil 4, and the pulse power source 5 are the same as those in the first embodiment.

  Also in the second embodiment, the pulse power source 5 obtains the optimum applied magnetic field to be output to the magnetizing coil 4 in order to apply the optimum magnetic field for obtaining a large trapping magnetic field to the superconductor 3. An experiment similar to that in the first embodiment was performed.

  As a result, the trapping magnetic field of the superconductor 3 showed the same applied magnetic field dependence as that performed at 77K in the first embodiment, and the maximum trapping magnetic field was 0.5T. That is, it was confirmed that if the temperature is the same, the trapped magnetic field of the superconductor 3 is the same regardless of the cooling means.

  In the second embodiment, since the magnetizing coil 4 is outside the refrigerant container 6 and insulated from the superconductor 3, the magnetized superconductor 3 applies a pulse current to the magnetizing coil. When magnetized by energization, it is not affected by the heat generated by the coil. In other words, since an excessive temperature rise of the superconductor can be avoided, there is an effect that more stable pulse magnetization is possible.

  Further, in the second embodiment, since the magnetizing coil is outside the refrigerant container 6 containing the superconductor, after the magnetization, the refrigerant container including the superconductor functioning as a magnet by capturing the magnetic field is used. The portion can be easily separated from the magnetizing coil and the magnetizing power source. Therefore, after magnetizing, the magnetizing coil and the magnetizing power source, which are required only when magnetizing, are separated from the part of the refrigerant container containing the superconductor, and only the functional part that generates the magnetic field of the superconducting magnet device is The effect is that it can be used in applications and devices.

  In a magnetizing method of a superconducting magnet device that magnetizes the superconductor by passing a pulse current through a magnetizing coil disposed around the superconductor, the superconductor is cooled to a superconducting transition temperature or less, and the superconductor The magnetizing coil is energized with a pulse current whose peak value has been determined so that an applied magnetic field is generated such that the minimum value of the magnetic field penetrating the magnetic field and the maximum value of the magnetic field trapped in the superconductor are generated. In addition to generating a high magnetic field, the present invention can be applied to various uses and uses that enable use in equipment.

It is a block diagram which shows the fundamental structure of the superconducting magnet apparatus of 1st Example of this invention, and its magnetization method. It is a block diagram which shows the refrigerator in the 1st Example. It is a block diagram for demonstrating the operating principle of the refrigerator in this 1st Example. It is a diagram which shows an example of the current waveform with which the magnetizing coil in a 1st Example is energized, and is a diagram for defining an applied magnetic field. It is a diagram which shows the magnetic field distribution inside a superconductor in each time of the pulse magnetization process of the superconductor in a 1st Example. It is a diagram which shows the relationship between the applied magnetic field in this 1st Example, and the capture | acquisition magnetic field of a superconductor. It is a diagram which shows the relationship between the winding number of the magnetizing coil in this 1st Example, and the rise time of a pulse current. FIG. 4 is a diagram showing an applied magnetic field and a trapped magnetic flux amount of the superconductor (total amount of trapped magnetic field) in the first embodiment. It is a diagram which shows the applied magnetic field dependence of the trapped magnetic flux amount which is the total amount of the trapped magnetic field of the superconductor in the 1st Example. It is explanatory drawing which shows arrangement | positioning of the magnetic field sensor which measures the capture magnetic field of the superconductor in a 1st Example. It is a diagram which shows the result investigated by the various applied magnetic fields of the time change of the capture magnetic field after the magnetization of the superconductor in a 1st Example. It is a block diagram which shows the basic composition of the superconducting magnet apparatus of 2nd Example of this invention, and its magnetization method.

Explanation of symbols

DESCRIPTION OF SYMBOLS 1 Thermal insulation container 2 Cold head 20 Refrigerator 3 Superconductor 4 Magnetization coil 5 Pulse power supply 6 Refrigerant container

Claims (3)

A magnetizing method for a superconducting magnet device that magnetizes the superconductor by passing a pulse current through a magnetizing coil disposed around the superconductor,
Cooling the superconductor below the superconducting transition temperature,
A pulse current whose peak value is determined so that an applied magnetic field is generated such that the minimum value of the magnetic field penetrating into the superconductor and the maximum value of the magnetic field trapped in the superconductor are generated, A magnetizing method for a superconducting magnet device, wherein a coil is energized. In claim 1,
The superconductor is a RE-Ba-Cu-O-based superconductor (RE is Y or a rare earth element and a combination of these elements), and has a large magnetic field that can be captured and is configured to generate a high magnetic field. A magnetizing method for a superconducting magnet device. In claim 2,
A superconducting magnet apparatus magnetizing method, wherein the superconductor captures a magnetic field exceeding IT.

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