JP2005200369A - 化粧料 - Google Patents
化粧料 Download PDFInfo
- Publication number
- JP2005200369A JP2005200369A JP2004009305A JP2004009305A JP2005200369A JP 2005200369 A JP2005200369 A JP 2005200369A JP 2004009305 A JP2004009305 A JP 2004009305A JP 2004009305 A JP2004009305 A JP 2004009305A JP 2005200369 A JP2005200369 A JP 2005200369A
- Authority
- JP
- Japan
- Prior art keywords
- cosmetic
- crosslinked
- silicone oil
- silica
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002537 cosmetic Substances 0.000 title claims abstract description 35
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 59
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 44
- 229920002545 silicone oil Polymers 0.000 claims abstract description 29
- 229920000642 polymer Polymers 0.000 claims abstract description 28
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 24
- 239000000470 constituent Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 4
- 125000005375 organosiloxane group Chemical group 0.000 abstract 1
- 229920000223 polyglycerol Polymers 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 18
- 229910002012 Aerosil® Inorganic materials 0.000 description 13
- 239000000203 mixture Substances 0.000 description 9
- -1 fructooligosaccharide fatty acid ester Chemical class 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 6
- 239000004205 dimethyl polysiloxane Substances 0.000 description 6
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 6
- 238000009472 formulation Methods 0.000 description 6
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000006071 cream Substances 0.000 description 4
- 235000014113 dietary fatty acids Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000004945 emulsification Methods 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- 239000000194 fatty acid Substances 0.000 description 4
- 229930195729 fatty acid Natural products 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 description 3
- 229940107187 fructooligosaccharide Drugs 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000002304 perfume Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 2
- 229910002014 Aerosil® 130 Inorganic materials 0.000 description 2
- 229910002016 Aerosil® 200 Inorganic materials 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 2
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- 239000002734 clay mineral Substances 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 125000004122 cyclic group Chemical group 0.000 description 2
- 239000003349 gelling agent Substances 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 230000005660 hydrophilic surface Effects 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- FPLYNRPOIZEADP-UHFFFAOYSA-N octylsilane Chemical compound CCCCCCCC[SiH3] FPLYNRPOIZEADP-UHFFFAOYSA-N 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- 229910002018 Aerosil® 300 Inorganic materials 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- IUMSDRXLFWAGNT-UHFFFAOYSA-N Dodecamethylcyclohexasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 IUMSDRXLFWAGNT-UHFFFAOYSA-N 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 229920001202 Inulin Polymers 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000012644 addition polymerization Methods 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 239000011346 highly viscous material Substances 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 230000005661 hydrophobic surface Effects 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 description 1
- 229940029339 inulin Drugs 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- HMMGMWAXVFQUOA-UHFFFAOYSA-N octamethylcyclotetrasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 HMMGMWAXVFQUOA-UHFFFAOYSA-N 0.000 description 1
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229920006136 organohydrogenpolysiloxane Polymers 0.000 description 1
- 239000008385 outer phase Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 125000005372 silanol group Chemical group 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- QPQANCNBWQXGTQ-UHFFFAOYSA-N trihydroxy(trimethylsilylperoxy)silane Chemical compound C[Si](C)(C)OO[Si](O)(O)O QPQANCNBWQXGTQ-UHFFFAOYSA-N 0.000 description 1
- 125000000026 trimethylsilyl group Chemical group [H]C([H])([H])[Si]([*])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
【解決手段】構成成分として、(A)架橋部分がオルガノポリシロキサン及び/又はポリグリセリンからなる架橋型オルガノポリシロキサン重合物を1〜50重量%と、(B)シリカを0.1〜5重量%と、(C)25℃における粘度が350cSt以下であるシリコーン油を含有する油性ゲルを配合する。
Description
[製造方法]
フラクトオリゴ糖脂肪酸エステル誘導体である成分9を除く油相成分を三本ローラーで混練し、油性ゲルを形成させる。成分9を添加する場合は、これを加熱溶解して加える。さらに成分10〜13を加え、ディスパーミルにて混合撹拌する。これに成分14〜17を溶解して加え、ディスパーミルにて混合撹拌し、乳化ファンデーションを得た。
得られた乳化ファンデーションに対し、下記の項目について評価を行い、表1にその結果を示す。
伸びの良さ、さっぱりとした使用感:10人の専門パネラーにより官能評価を行い、下記で示した基準でまとめた。
○・・・8人以上が良好と評価
△・・・4人〜7人が良好と評価
×・・・3人以下が良好と評価
化粧料の安定性:40℃で1ヶ月保存後の乳化ファンデーションについて、下記で示した基準でまとめた。
○・・・油分の離漿なし、粘度変化なし
△・・・油分の離漿なし、粘度低下
×・・・油分の離漿あり、粘度低下
*2:AEROSIL R972(日本アエロジル社製)
*3:ベントン38V(エレメンティススペシャリティーズ社製)
*4:KSG−210(架橋部分ポリオキシアルキレン、信越化学工業社製、架橋型
オルガノポリシロキサン重合物約27%、ジメチルポリシロキサン(6cSt
)約73%換算)
*5:レオパールISK(千葉製粉社製)
成分 重量% (油性ゲル中)
1.架橋型オルガノポリシロキサン重合物(※6) 10 (14.7 )
2.シリカ(※7) 0.5( 0.7 )
3.ジメチルポリシロキサン(6cSt) 15
4.デカメチルシクロペンタシロキサン(6cSt) 37.5
5.トリメチルシロキシケイ酸 5
6.雲母チタン 25
7.ポリアクリル酸アルキル 5
8.窒化ホウ素 2
9.香料 適量
※6:KSG−16(架橋部分オルガノポリシロキサン、信越化学工業社製、架橋型
オルガノポリシロキサン重合物約25%、ジメチルポリシロキサン(6cSt
)約75%換算)
※7:AEROSIL R976(日本アエロジル社製)
[製造方法]
成分1〜5を三本ローラーで混練し、油性ゲルを形成させる。これに成分6〜9を加え、プラネタリーミキサーにて混合撹拌し、アイシャドウを得た。
成分 重量% (油性ゲル中)
1.架橋型オルガノポリシロキサン重合物(※8) 5 ( 8.6 )
2.シリカ(※9) 1 ( 1.7 )
3.メチルフェニルポリシロキサン(15cSt) 42
4.デカメチルシクロペンタシロキサン(6cSt) 10
5.シリコーン処理酸化チタン 18
6.シリコーン処理酸化鉄(黄、赤、黒) 3
7.シリコーン処理セリサイト 14
8.窒化ホウ素 5
9.ナイロン末 2
10.香料 適量
※8:KSG−18(架橋部分オルガノポリシロキサン、信越化学工業社製、架橋型
オルガノポリシロキサン重合物約15%、メチルフェニルポリシロキサン(1
5cSt)約85%換算)
※9:AEROSIL 200(日本アエロジル社製)
[製造方法]
成分1〜4を三本ローラーで混練し、油性ゲルを形成させる。これに成分5〜10を加え、三本ローラーで混練し、油性ファンデーションを得た。
成分 重量% (油性ゲル中)
1.架橋型オルガノポリシロキサン重合物(※10) 3 ( 7.6 )
2.シリカ(※11) 0.2( 0.5 )
3.ジメチルポリシロキサン(6cSt) 15
4.オクタメチルトリシロキサン(1cSt) 20
5.ポリエーテル変性ポリシロキサン 0.5
6.トリイソステアリン酸ポリオキシエチレン硬化ヒマシ油 1
7.ポリアクリル酸アルキル 3
8.精製水 44.1
9.グリセリン 10
10.エタノール 3
11.防腐剤 0.2
12.香料 適量
※10:KSG−710(架橋部分ポリグリセリン、信越化学工業社製、架橋型オル
ガノポリシロキサン重合物約25%、ジメチルポリシロキサン(6cSt)
約75%換算)
※11:AEROSIL 130(日本アエロジル社製)
[製造方法]
実施例1と同様にして(油性ゲルは成分1〜6)、W/O型クリームを得た。
Claims (2)
- 構成成分として、(A)架橋部分がオルガノポリシロキサン及び/又はポリグリセリンからなる架橋型オルガノポリシロキサン重合物を1〜50重量%と、(B)シリカを0.1〜5重量%と、(C)25℃における粘度が350cSt以下であるシリコーン油を含有する油性ゲルを配合した化粧料。
- 請求項1において構成成分(A)の架橋部分がオルガノポリシロキサンからなる架橋型オルガノポリシロキサン重合物を含有する油性ゲルを配合した化粧料。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2004009305A JP4250093B2 (ja) | 2004-01-16 | 2004-01-16 | 化粧料 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2004009305A JP4250093B2 (ja) | 2004-01-16 | 2004-01-16 | 化粧料 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2005200369A true JP2005200369A (ja) | 2005-07-28 |
JP4250093B2 JP4250093B2 (ja) | 2009-04-08 |
Family
ID=34822387
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2004009305A Expired - Lifetime JP4250093B2 (ja) | 2004-01-16 | 2004-01-16 | 化粧料 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP4250093B2 (ja) |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006057054A (ja) * | 2004-08-23 | 2006-03-02 | Shiseido Co Ltd | ゲル状組成物及びそれを含む化粧料 |
JP2007182391A (ja) * | 2006-01-04 | 2007-07-19 | Noevir Co Ltd | 油中水型乳化化粧料 |
JP2008273942A (ja) * | 2007-03-30 | 2008-11-13 | Kose Corp | 弾性ゲル状油性化粧料 |
WO2009038712A1 (en) * | 2007-09-20 | 2009-03-26 | Momentive Performance Materials Inc. | Boron nitride-containing silicone gel composition |
JP2009528377A (ja) * | 2006-03-01 | 2009-08-06 | イーエルシー マネージメント エルエルシー | 透明なサンスクリーンジェル及びその使用方法 |
JP2010006777A (ja) * | 2008-06-30 | 2010-01-14 | Kowa Co | 離液抑制方法 |
JP2010163370A (ja) * | 2009-01-13 | 2010-07-29 | Kao Corp | 凹凸補正用油性化粧料 |
JP2011126808A (ja) * | 2009-12-16 | 2011-06-30 | Kao Corp | 油中水型乳化化粧料 |
JP2013032345A (ja) * | 2011-06-30 | 2013-02-14 | Rohto Pharmaceutical Co Ltd | 外用組成物 |
KR20130120405A (ko) * | 2012-04-25 | 2013-11-04 | 신에쓰 가가꾸 고교 가부시끼가이샤 | 유성 메이크업 화장료 |
US20210220231A1 (en) * | 2018-05-22 | 2021-07-22 | Shiseido Company, Ltd. | Two-layered oil-based cosmetic |
-
2004
- 2004-01-16 JP JP2004009305A patent/JP4250093B2/ja not_active Expired - Lifetime
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006057054A (ja) * | 2004-08-23 | 2006-03-02 | Shiseido Co Ltd | ゲル状組成物及びそれを含む化粧料 |
JP2007182391A (ja) * | 2006-01-04 | 2007-07-19 | Noevir Co Ltd | 油中水型乳化化粧料 |
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