JP2005089615A - Method for producing humic acid liquid - Google Patents
Method for producing humic acid liquid Download PDFInfo
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- JP2005089615A JP2005089615A JP2003325581A JP2003325581A JP2005089615A JP 2005089615 A JP2005089615 A JP 2005089615A JP 2003325581 A JP2003325581 A JP 2003325581A JP 2003325581 A JP2003325581 A JP 2003325581A JP 2005089615 A JP2005089615 A JP 2005089615A
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本発明は、土壌改良材及び肥料として有用な腐植酸液の製造方法に関する。 The present invention relates to a method for producing a humic acid solution useful as a soil conditioner and a fertilizer.
腐植酸はフミン酸とも呼ばれ、土壌有機物の中核をなすものであり、作物の成長促進や根の活性化のほか、土壌自体の物理性改善、肥沃化、微生物の増殖化、多様化など、土壌の総合的な健全化に大きな役割を果たしている。このため、従来普通肥料として腐植酸アンモニア肥料、腐植酸カリ肥料、腐植酸苦土肥料、腐植酸りん肥等があり、又、土壌改良材として各種の腐植酸質資材が供給されている。 Humic acid, also known as humic acid, is the core of soil organic matter. In addition to promoting the growth of crops and activating the roots, physical improvement of the soil itself, fertilization, microbial growth, diversification, etc. It plays a major role in comprehensive soil health. For this reason, conventional humic acid fertilizers include humic acid ammonia fertilizer, humic acid potassium fertilizer, humic acid bitter fertilizer, humic acid phosphorus fertilizer and the like, and various humic acid materials are supplied as soil improvement materials.
これらの普通肥料、土壌改良材で使用されている腐植酸は、通常、石炭又は亜炭を硝酸又は硝酸及び硫酸で分解して生成しているのでニトロフミン酸とも呼ばれている(下記特許文献参照)。しかしながら、このような酸分解物では本来腐植酸が内包する有用物質である糖やアミノ酸類が少なからず分解されてしまうという欠点がある。
本発明は、上記欠点を解消させ、本来腐植酸が内包する有用物質の分解を防ぐことのできる腐植酸液の製造方法を提供することを目的とする。 An object of this invention is to provide the manufacturing method of the humic acid liquid which can eliminate the said fault and can prevent decomposition | disassembly of the useful substance which humic acid inherently contains.
本発明は、泥炭に水とアルカリ水溶液を加えて、攪拌し、液体と沈殿物とを分離することを特徴とする。 The present invention is characterized in that water and an aqueous alkaline solution are added to peat and stirred to separate the liquid and the precipitate.
本発明では腐植酸液を得るのに硝酸又は硝酸及び硫酸を使用しないので、本来腐植酸が内包する有用物質である糖やアミノ酸類の分解を防ぐことができる。 In the present invention, since nitric acid or nitric acid and sulfuric acid are not used to obtain a humic acid solution, it is possible to prevent the decomposition of sugars and amino acids, which are inherently useful substances contained in humic acid.
以下本発明を詳細に説明する。 The present invention will be described in detail below.
泥炭(ピート類)は寒冷な湖沼地帯に生育したヨシ、スゲ、ミズゴケなどが腐朽堆積し、低温、嫌気的条件下で分解したものである。泥炭の形成が最も盛んに行われたのは、氷河後退期から温暖期に移行するころであり、その頃は湿地帯にヨシ、スゲ、ミズゴケなどが大群生し、活発な泥炭化が進行していたと推定されている。その後、気温が上昇し乾燥した地帯ではさらに分解が進んで腐食化し黒泥となったが、寒冷湿潤な地帯では泥炭のまま残っている。 Peat (peats) is a product of reeds, reeds, sphagnum, etc. grown in cold lakes and decomposed under low temperature and anaerobic conditions. The formation of peat was most prominent during the transition from the glacial retreat to the warm season, when reeds, sedges, and sphagnum were swarming in the wetlands, and active peat carbonization was progressing. It is estimated that After that, in the dry zone where the temperature rose, it further decomposed and became corroded and became black mud, but it remained peat in the cold and humid zone.
現在では、泥炭層は北緯45°〜65°の間の地帯に分布し、カナダ、ロシア、中国、アラスカ、北欧などに広がっている。 At present, the peat layer is distributed in the region between 45 ° and 65 ° north latitude, and extends to Canada, Russia, China, Alaska, Northern Europe and so on.
泥炭には、生成過程の違いによって低位泥炭、中位泥炭、高位泥炭の3種類に分けられる。本発明ではいずれも使用可能である。特に、中国東北地方で産出される高位泥炭である松花江炭(登録商標)が最も好ましい。
(1)低位泥炭
浅い湖沼の岸近くにヨシ、スゲが茂り、その遺体が水中に堆積し泥炭化したもので分解が進み、黒褐色で泥に近い。弱酸性で無機成分が比較的多い。
(2)中位泥炭
低位泥炭が水面上に隆起するとその上に樹木が侵入するようになり、落ち葉や落枝が堆積して中位泥炭が形成された。低位泥炭ほどは分解が進まず、褐色で泥状の部分は少ない。やや酸性を呈し無機成分はあまり多くない。
(3)高位泥炭
中位泥炭地帯の森林化が進むと、湿潤な土地の上にミズゴケが繁雑し、ついには森林を圧倒して丘状のミズゴケ堆積層が形成され泥炭化して高位泥炭ができる。分解はあまり進んでおらず、淡褐色で繊維が多く、弾力性に富み、強酸性で無機成分に乏しい。
There are three types of peat, low peat, medium peat and high peat, depending on the production process. Any of them can be used in the present invention. In particular, Songhuajiang Charcoal (registered trademark), which is a high-ranking peat produced in Northeast China, is most preferred.
(1) Low-rank peat Reeds and sedges grow near the shores of shallow lakes, and their bodies accumulate in the water and are charred. Weakly acidic and contains a relatively large amount of inorganic components.
(2) Middle peat When the lower peat rises above the surface of the water, trees begin to invade it, and fallen leaves and twigs accumulate to form middle peat. The lower the peat, the less the decomposition, the less brown and muddy. It is slightly acidic and contains few inorganic components.
(3) Higher peat If the forestation of the middle peat zone progresses, sphagnum moss on the wet land, eventually overwhelming the forest to form a hill-shaped sphagnum sedimentary layer and peat carbonize to produce higher peat. . Decomposition has not progressed much, light brown, rich in fibers, rich in elasticity, strongly acidic and poor in inorganic components.
一般にピートと呼ばれているものは、中、高位泥炭で、特にミズゴケ泥炭(ピートモス)は園芸用土の改良材として使われている。 What is commonly called peat is middle and high peat, and sphagnum peat (peet moss) is used as an improvement material for horticultural soil.
アルカリ水溶液としては、水酸化ナトリウム、水酸化カリウム、消石灰、アンモニア等が使用できるが、特に水酸化カリウムが好ましい。 As the alkaline aqueous solution, sodium hydroxide, potassium hydroxide, slaked lime, ammonia and the like can be used, and potassium hydroxide is particularly preferable.
泥炭と水とアルカリ水溶液の混合比率は、水100重量部に対して、泥炭10〜30重量部、アルカリ水溶液1〜3重量部が好ましい。攪拌は、常温で行われ20分〜40分程度で十分である。分離された液体及び沈殿物を濾過して得られた腐植酸液の濃度は5〜8%である。 The mixing ratio of peat, water, and aqueous alkaline solution is preferably 10 to 30 parts by weight of peat and 1 to 3 parts by weight of aqueous alkaline solution with respect to 100 parts by weight of water. Stirring is performed at room temperature, and about 20 to 40 minutes is sufficient. The concentration of the humic acid solution obtained by filtering the separated liquid and the precipitate is 5 to 8%.
このようにして得られた腐植酸液は単独又は液状複合肥料と混和して灌水施用される。 The humic acid solution thus obtained is applied alone or mixed with a liquid composite fertilizer for irrigation.
この腐植酸液を作物に対して使用することにより、次のような効果が得られる。
1.土の耐水性団粒を形成し、透水性、保水性、排水性をよくし、酸素吸収能力を高める。
2.土のりん酸吸収係数を低下させ、りん酸の有効性を高める。
3.土の微量要素をキレート結合させることにより植物に吸収されやすい形にする。
4.土の陽イオン交換容量を増大する。
5.土のpH緩衝能力を高め、酸、アルカリの障害を除去する。
6.土の微生物の代謝活性を高め、多様な生態環境を作り、連作障害を軽減する。
7.植物の成長点を刺激して、強力に発根を促進する。
8.ppm単位(百万分の一)の量で、植物に活性を与える有機触媒のような働きがあり、植物酵素の活動を刺激して、若々しく健全な作物を作る。
The following effects can be obtained by using this humic acid solution on crops.
1. Forms water-resistant aggregates of soil, improves water permeability, water retention, drainage, and increases oxygen absorption capacity.
2. Reduces the phosphate absorption coefficient of soil and increases the effectiveness of phosphoric acid.
3. Forms that are easily absorbed by plants by chelating the minor elements of the soil.
Four. Increase soil cation exchange capacity.
Five. Increase the pH buffering capacity of the soil and remove the obstacles of acid and alkali.
6. Increase the metabolic activity of soil microorganisms, create a diverse ecological environment, and reduce continuous cropping obstacles.
7. Stimulates plant growth points and strongly promotes rooting.
8. In ppm (parts per million), it acts as an organic catalyst that gives activity to plants and stimulates the activities of plant enzymes to produce youthful and healthy crops.
水1000リットルに中国東北地方で産出される高位泥炭である松花江炭(登録商標)200kgと水酸化カリウム18kgを加えて常温で30分間攪拌し、液体と沈殿物とに分離させ、液体部分から腐植酸液を得るとともに、沈殿物はさらに濾過して腐植酸液を得た。完成した腐植酸液の濃度は8%であった。水酸化カリウムの濃度は1.5%であった。
To 1000 liters of water, add 200 kg of Songhuajiang Charcoal (registered trademark), a high-grade peat produced in Northeast China, and 18 kg of potassium hydroxide. While obtaining a humic acid solution, the precipitate was further filtered to obtain a humic acid solution. The concentration of the finished humic acid solution was 8%. The concentration of potassium hydroxide was 1.5%.
Claims (4)
The method according to claim 1, wherein the peat is Songhuajiang charcoal (registered trademark) produced in Northeast China.
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JP2003325581A JP2005089615A (en) | 2003-09-18 | 2003-09-18 | Method for producing humic acid liquid |
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Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102336915A (en) * | 2011-08-12 | 2012-02-01 | 祁长喜 | Method for producing humate from base waste liquid |
RU2446201C1 (en) * | 2010-09-24 | 2012-03-27 | Государственное образовательное учреждение высшего профессионального образования "Югорский государственный университет" | Peat carboxymethylation method |
JP2012509316A (en) * | 2008-11-20 | 2012-04-19 | ジョ,クォンホ | Method for producing plant growth promoter using peat moss |
CN102584457A (en) * | 2012-02-28 | 2012-07-18 | 管庆文 | Organic fertilizer for treating little-leaf disease and chlorosis of apple trees and hairy leaf disease of cherry trees and preparation method of organic fertilizer |
RU2469994C1 (en) * | 2011-07-19 | 2012-12-20 | Владимир Ильич Кормилицын | Granular fertiliser based on peat |
KR101492811B1 (en) | 2013-04-23 | 2015-02-13 | 김영민 | Method for Germanium Humic Acid |
KR101535163B1 (en) * | 2013-08-27 | 2015-07-09 | 김영민 | Method of Growing Crops with Germanium Humic acid |
KR20160147878A (en) * | 2014-04-23 | 2016-12-23 | 블라디미르 페트로비치 세바스티야노프 | Method for comprehensively processing brown coal and leonardite into humic fertilizers and preparations and into fuel briquettes, and mechanochemical reactor for processing highly-viscous media |
CN108484330A (en) * | 2018-05-28 | 2018-09-04 | 张桂芳 | A kind of environmental protection SOLID ORGANIC fertilizer formula |
RU2686807C1 (en) * | 2017-12-08 | 2019-04-30 | федеральное государственное бюджетное образовательное учреждение высшего образования "Югорский государственный университет" | Method of producing compound liquid humic fertilizers from peat |
CN115073241A (en) * | 2022-07-08 | 2022-09-20 | 安徽农业大学 | Preparation method and application of humic acid phosphate fertilizer for improving phosphorus effectiveness |
RU2790724C1 (en) * | 2021-10-11 | 2023-02-28 | Сямиуллин Заир Сайярович | Method for obtaining humic preparation containing humic acids and peat mineral components |
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2003
- 2003-09-18 JP JP2003325581A patent/JP2005089615A/en active Pending
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2012509316A (en) * | 2008-11-20 | 2012-04-19 | ジョ,クォンホ | Method for producing plant growth promoter using peat moss |
RU2446201C1 (en) * | 2010-09-24 | 2012-03-27 | Государственное образовательное учреждение высшего профессионального образования "Югорский государственный университет" | Peat carboxymethylation method |
RU2469994C1 (en) * | 2011-07-19 | 2012-12-20 | Владимир Ильич Кормилицын | Granular fertiliser based on peat |
CN102336915A (en) * | 2011-08-12 | 2012-02-01 | 祁长喜 | Method for producing humate from base waste liquid |
CN102584457A (en) * | 2012-02-28 | 2012-07-18 | 管庆文 | Organic fertilizer for treating little-leaf disease and chlorosis of apple trees and hairy leaf disease of cherry trees and preparation method of organic fertilizer |
CN102584457B (en) * | 2012-02-28 | 2013-11-20 | 管庆文 | Organic fertilizer for treating little-leaf disease and chlorosis of apple trees and hairy leaf disease of cherry trees and preparation method of organic fertilizer |
KR101492811B1 (en) | 2013-04-23 | 2015-02-13 | 김영민 | Method for Germanium Humic Acid |
KR101535163B1 (en) * | 2013-08-27 | 2015-07-09 | 김영민 | Method of Growing Crops with Germanium Humic acid |
KR20160147878A (en) * | 2014-04-23 | 2016-12-23 | 블라디미르 페트로비치 세바스티야노프 | Method for comprehensively processing brown coal and leonardite into humic fertilizers and preparations and into fuel briquettes, and mechanochemical reactor for processing highly-viscous media |
JP2017518248A (en) * | 2014-04-23 | 2017-07-06 | ウラジミール・ペトロヴィッチ・セヴァスチヤノフ | Comprehensive conversion method of lignite and leonardite to humus fertilizer, preparation to briquette fuel, and mechanochemical reactor for high viscosity medium conversion |
KR102306975B1 (en) | 2014-04-23 | 2021-09-30 | 블라디미르 페트로비치 세바스티야노프 | Method for comprehensively processing brown coal and leonardite into humic fertilizers and preparations and into fuel briquettes, and mechanochemical reactor for processing highly-viscous media |
RU2686807C1 (en) * | 2017-12-08 | 2019-04-30 | федеральное государственное бюджетное образовательное учреждение высшего образования "Югорский государственный университет" | Method of producing compound liquid humic fertilizers from peat |
CN108484330A (en) * | 2018-05-28 | 2018-09-04 | 张桂芳 | A kind of environmental protection SOLID ORGANIC fertilizer formula |
RU2790724C1 (en) * | 2021-10-11 | 2023-02-28 | Сямиуллин Заир Сайярович | Method for obtaining humic preparation containing humic acids and peat mineral components |
CN115073241A (en) * | 2022-07-08 | 2022-09-20 | 安徽农业大学 | Preparation method and application of humic acid phosphate fertilizer for improving phosphorus effectiveness |
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