JP2003523969A5 - - Google Patents
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- Publication number
- JP2003523969A5 JP2003523969A5 JP2001555041A JP2001555041A JP2003523969A5 JP 2003523969 A5 JP2003523969 A5 JP 2003523969A5 JP 2001555041 A JP2001555041 A JP 2001555041A JP 2001555041 A JP2001555041 A JP 2001555041A JP 2003523969 A5 JP2003523969 A5 JP 2003523969A5
- Authority
- JP
- Japan
- Prior art keywords
- nitroguanidine
- value
- methylammonium salt
- methylamine
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical class NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 claims 6
- 238000000034 method Methods 0.000 claims 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- IDCPFAYURAQKDZ-UHFFFAOYSA-N 1-nitroguanidine Chemical compound NC(=N)N[N+]([O-])=O IDCPFAYURAQKDZ-UHFFFAOYSA-N 0.000 claims 2
- XCXKNNGWSDYMMS-UHFFFAOYSA-N 2-methyl-1-nitroguanidine Chemical compound CNC(N)=N[N+]([O-])=O XCXKNNGWSDYMMS-UHFFFAOYSA-N 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 1
- 229910002651 NO3 Inorganic materials 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 125000000250 methylamino group Chemical group [H]N(*)C([H])([H])[H] 0.000 claims 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
- 239000010452 phosphate Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10003834.4 | 2000-01-28 | ||
| DE10003834A DE10003834A1 (de) | 2000-01-28 | 2000-01-28 | Verfahren zur Herstellung von 1-Methyl-3-nitroguanidin |
| PCT/EP2001/000351 WO2001055099A1 (de) | 2000-01-28 | 2001-01-12 | Verfahren zur herstellung von 1-methyl-3-nitroguanidin |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2003523969A JP2003523969A (ja) | 2003-08-12 |
| JP2003523969A5 true JP2003523969A5 (https=) | 2005-07-07 |
| JP4758584B2 JP4758584B2 (ja) | 2011-08-31 |
Family
ID=7629122
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2001555041A Expired - Fee Related JP4758584B2 (ja) | 2000-01-28 | 2001-01-12 | １−メチル−３−ニトログアニジンの製造方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6486348B1 (https=) |
| EP (1) | EP1261581B1 (https=) |
| JP (1) | JP4758584B2 (https=) |
| AT (1) | ATE327218T1 (https=) |
| DE (2) | DE10003834A1 (https=) |
| ES (1) | ES2261374T3 (https=) |
| WO (1) | WO2001055099A1 (https=) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10000891A1 (de) * | 2000-01-12 | 2001-07-19 | Bayer Ag | Verfahren zur Herstellung von N-Methyl-N'-nitroguanidin |
| CN101565392A (zh) * | 2008-04-21 | 2009-10-28 | 南通天泽化工有限公司 | 一种甲基硝基胍及其制备方法 |
| CN106986790A (zh) * | 2017-05-25 | 2017-07-28 | 宁夏贝利特生物科技有限公司 | 用生产硝基胍后的稀硫酸生产n‑甲基‑n′‑硝基胍的方法 |
| CN107698466A (zh) * | 2017-11-09 | 2018-02-16 | 宁夏贝利特生物科技有限公司 | 一种n‑甲基‑n′‑硝基胍的制备方法 |
| CN109053498A (zh) * | 2018-09-27 | 2018-12-21 | 南通天泽化工有限公司 | 一种1-甲基-1,2-二硝基胍的制备方法 |
| CN117986160A (zh) * | 2023-12-11 | 2024-05-07 | 福诺(宁夏)化工科技有限公司 | 一种甲基硝基胍的制备方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW198724B (https=) * | 1990-10-24 | 1993-01-21 | Ciba Geigy Ag | |
| DE19611654A1 (de) | 1996-03-25 | 1997-10-02 | Bayer Ag | Verfahren zur Herstellung von N-Methyl-N'-nitroguanidin |
| JPH107645A (ja) * | 1996-06-19 | 1998-01-13 | Mitsui Petrochem Ind Ltd | アルキルニトログアニジン誘導体の製造方法 |
| DE19712885A1 (de) * | 1997-03-27 | 1998-10-01 | Bayer Ag | Verfahren zur Herstellung von N-Alkyl-N'-nitroguanidinen |
| CN1207279C (zh) * | 1998-11-25 | 2005-06-22 | 狄纳米特诺贝尔爆炸材料和系统技术股份有限公司 | 制备n－烷基－n′－硝基胍的方法 |
| DE10000891A1 (de) * | 2000-01-12 | 2001-07-19 | Bayer Ag | Verfahren zur Herstellung von N-Methyl-N'-nitroguanidin |
-
2000
- 2000-01-28 DE DE10003834A patent/DE10003834A1/de not_active Withdrawn
-
2001
- 2001-01-12 DE DE50109873T patent/DE50109873D1/de not_active Expired - Lifetime
- 2001-01-12 EP EP01901150A patent/EP1261581B1/de not_active Expired - Lifetime
- 2001-01-12 ES ES01901150T patent/ES2261374T3/es not_active Expired - Lifetime
- 2001-01-12 WO PCT/EP2001/000351 patent/WO2001055099A1/de not_active Ceased
- 2001-01-12 JP JP2001555041A patent/JP4758584B2/ja not_active Expired - Fee Related
- 2001-01-12 AT AT01901150T patent/ATE327218T1/de active
-
2002
- 2002-06-05 US US10/161,619 patent/US6486348B1/en not_active Expired - Lifetime
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