JP2000178206A - Lubricant containing plant fat and oil - Google Patents

Lubricant containing plant fat and oil

Info

Publication number
JP2000178206A
JP2000178206A JP36075198A JP36075198A JP2000178206A JP 2000178206 A JP2000178206 A JP 2000178206A JP 36075198 A JP36075198 A JP 36075198A JP 36075198 A JP36075198 A JP 36075198A JP 2000178206 A JP2000178206 A JP 2000178206A
Authority
JP
Japan
Prior art keywords
lubricant
oil
tablets
fat
vegetable oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP36075198A
Other languages
Japanese (ja)
Inventor
Kentarou Ohari
健太郎 小治
Sukeyuki Teramoto
祐之 寺本
Kenichi Ishiwatari
健一 石渡
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fancl Corp
Original Assignee
Fancl Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fancl Corp filed Critical Fancl Corp
Priority to JP36075198A priority Critical patent/JP2000178206A/en
Publication of JP2000178206A publication Critical patent/JP2000178206A/en
Pending legal-status Critical Current

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  • Confectionery (AREA)
  • Medicinal Preparation (AREA)

Abstract

PROBLEM TO BE SOLVED: To obtain the subject lubricant that can inhibit the tablets from capping, sticking and binding, when tablets and table cakes are formed, by using a specific vegetable fat and oil powder. SOLUTION: This lubricant is prepared by adding (A) protein and (B) saccharide (C) vegetable fat and oil and pulverizing the mixture into particles, preferably fine particles with an average particle size of <=250 μm. In a preferred embodiment, the lubricant is produced by formulating the components (A), (B) and (C) into an emulsion and spray-drying the emulsion. As a component A, are cited the coconut oil from copra, palm oil collected from the fruit flesh and palm kernel oil collected from the fruit kernel and the amounts of the components B and C are 8-12 pts.wt., and 30-40 parts per 100 pts.wt. of the component (A), respectively.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は滑沢剤、及びそれを
用いた錠剤及び錠菓に関するものである。更に詳細に
は、植物性油脂を主成分とし、打錠の際のキャッピン
グ、スティッキング及びバインディング等を起こさない
滑沢剤、及びそれを用いた錠剤及び錠菓に関する。
TECHNICAL FIELD The present invention relates to a lubricant, and tablets and confections using the same. More specifically, the present invention relates to a lubricant containing a vegetable fat as a main component and not causing capping, sticking, binding and the like at the time of tableting, and to tablets and confections using the same.

【0002】[0002]

【従来の技術】錠剤、錠菓の製造において、粉末や粉状
の原料を打錠する必要がある。打錠においては、脱型の
際に錠剤の上杵側が帽子状に薄くはがれるキャッピン
グ、打錠中に粉が杵に付着し杵離れが悪く、錠剤表面に
傷がつくスティッキング、錠剤と臼の摩擦が大きく打錠
後の錠剤の排出性が悪くなるバインディングを生じるこ
とがあり、これがひどくなるとスムースに打錠できなく
なる。
2. Description of the Related Art In the production of tablets and confectionery, it is necessary to compress powder or powdery raw materials. In tableting, capping of the upper punch side of the tablet peels off thinly in the form of a hat when demolding, sticking that the powder adheres to the punch during tableting and peels off poorly, scratches the tablet surface, and friction between the tablet and the die In some cases, the binding of the tablet may become poor after tableting, and the tablet may not be discharged smoothly.

【0003】そこで、打錠においては滑沢剤を使用する
ことにより、原料粉体の流動性を向上させ、打錠機の臼
に一定量が充填されるようにすると同時に、打錠の際の
キャッピング、スティッキング及びバインディング等を
防止し、打錠の表面に光沢を与える。そのために従来か
ら精製タルク、ステアリン酸マグネシウム、ショ糖脂肪
酸エステル、ポリグリセリン脂肪酸エステル、植物硬化
油等が滑沢剤として使用されてきた。
[0003] Therefore, in tableting, a lubricant is used to improve the fluidity of the raw material powder so that a certain amount is filled in a die of a tableting machine, and at the same time, a tableting machine is used. Prevents capping, sticking, binding, etc. and imparts gloss to the tableting surface. For this purpose, purified talc, magnesium stearate, sucrose fatty acid esters, polyglycerin fatty acid esters, hardened vegetable oils, and the like have been conventionally used as lubricants.

【0004】その内、ショ糖脂肪酸エステルは多くが一
度塊状にしたものを粉砕して得られるため形状が球状で
なく、そのために近年の錠剤の形状の複雑化に伴い、添
加量が増加しコスト等に問題が生じてきた。ポリグリセ
リン脂肪酸エステルはその効果が小さいため、充分な効
果を期待するためには多量添加をしなくてはならず、ま
た、そのために錠剤の硬度低下や風味を悪くしたりする
問題があった。また、ステアリン酸マグネシウムの場合
は、少量の使用で滑沢剤としての効果を出すことができ
るが、食品添加物として認められていないためその用途
が医薬品に限定される。植物硬化油は滑沢剤としての効
果が小さく、且つ夏場での倉庫等の保管においてブロッ
キングを起こしやすい。また、近年、欧米諸国において
トランス脂肪酸の血清コレステロール濃度、癌との関係
が取りざたされている。更に、精製タルクは、食品への
使用量に制限があり、且つ滑沢剤としての効果も小さい
ためあまり用いられていない。
Among them, most of sucrose fatty acid esters are obtained by pulverizing a lump of lumps once and thus are not spherical in shape. And so on. Since polyglycerin fatty acid ester has a small effect, it has to be added in a large amount in order to expect a sufficient effect, and there is a problem that the hardness of the tablet is lowered and the flavor is deteriorated. In the case of magnesium stearate, the effect as a lubricant can be obtained by using a small amount, but its use is limited to pharmaceuticals because it is not recognized as a food additive. The hardened vegetable oil has a small effect as a lubricant and tends to cause blocking in storage in a warehouse or the like in summer. In recent years, relations between serum cholesterol levels of trans fatty acids and cancer have been taken up in Western countries. Further, purified talc is not used much because it has a limited amount of use in foods and has a small effect as a lubricant.

【0005】[0005]

【発明が解決しようとする課題】本発明は従来の技術の
課題を解決すべくなされたもので、錠剤、錠菓を打錠す
る際のキャッピング、スティッキング及びバインディン
グを防止する滑沢剤を提供することを目的とする。
SUMMARY OF THE INVENTION The present invention has been made to solve the problems of the prior art, and provides a lubricant which prevents capping, sticking and binding when compressing tablets and confections. The purpose is to:

【0006】[0006]

【課題を解決するための手段】本発明者は前記課題を解
決すべく鋭意研究を重ねた結果、植物性油脂を主成分と
する植物性油脂粉末を使用することによって、キャッピ
ング、スティッキング及びバインディングを起こさない
錠剤、錠菓を得られることを見出し、本発明に至った。
即ち、本発明は植物性油脂に蛋白質及び糖質を添加して
粉末化した植物性油脂粉末よりなることを特徴とする錠
剤又は錠菓用滑沢剤、及びかかる滑沢剤を添加してなる
ことを特徴とする錠剤又は錠菓である。好ましくは、植
物性油脂粉末中に植物性油脂を50重量%以上含み、植
物性油脂に蛋白質及び糖質を配合して乳化させ噴霧乾燥
することによって作られ、且つ平均粒子径250μm以
下の微粉末よりなる滑沢剤、及びかかる滑沢剤を添加し
てなる錠剤又は錠菓である。
Means for Solving the Problems As a result of intensive studies to solve the above problems, the present inventor has found that capping, sticking and binding can be achieved by using a vegetable oil powder containing a vegetable oil as a main component. The present inventors have found that tablets and confections that do not wake up can be obtained, and have led to the present invention.
That is, the present invention comprises a lubricant for tablets or tablet confections, comprising a vegetable oil or fat powder obtained by adding protein and sugar to vegetable oil or fat, and adding such a lubricant. A tablet or tablet confection characterized by the above. Preferably, a fine powder having a vegetable oil fat content of 50% by weight or more in the vegetable oil fat powder, blending the vegetable oil with the protein and saccharide, emulsifying and spray-drying the powder, and having an average particle diameter of 250 μm or less. And tablets or tablet confections to which such a lubricant is added.

【0007】[0007]

【発明の実施の形態】以下に本発明を詳細に説明する。
本発明における植物性油脂は、コプラから採油されるや
し油、アブラヤシの果肉部及び果実の核から採油される
パーム油及びパーム核油、カカオの種子から採油される
カカオ脂等常温で半固形状の油脂が適するが、これらの
みに限定されるものではない。また、蛋白質はカゼイン
ソーダが適し、糖質としては乳糖、デキストリンが適す
るが、これらのみに限定されるものではない。また必要
に応じてグリセリン脂肪酸エステル、リン酸塩といった
食品添加物を加えても構わない。
DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention will be described below in detail.
Vegetable oils and fats according to the present invention are semi-solid at room temperature such as palm oil extracted from copra, palm oil and palm kernel oil extracted from the pulp and fruit kernels of oil palm, and cocoa butter extracted from cocoa seeds. Fats and oils in shape are suitable, but are not limited thereto. In addition, casein soda is suitable as a protein, and lactose and dextrin are suitable as carbohydrates, but are not limited thereto. Food additives such as glycerin fatty acid esters and phosphates may be added as needed.

【0008】本発明に用いられる植物性油脂粉末は微粉
末の形態で使用され、その平均粒子径は250μm以下
であることが好ましい。特に好ましくは100〜150
μmである。即ち、滑沢効果は滑沢化しようとする粉末
または顆粒に比べ、その粒子径が小さいほど粉体粒子の
被覆力が大きいため、滑沢剤の粒子径はその性能に大き
く影響する。ここで、平均粒子径とは2種以上の粒径を
もつ粒子群の代表径のことをいい、比表面積測定法によ
る中央累積値として求める。
The vegetable oil powder used in the present invention is used in the form of a fine powder, and its average particle size is preferably 250 μm or less. Particularly preferably, 100 to 150
μm. In other words, the lubricating effect is such that the smaller the particle size, the greater the covering power of the powder particles, as compared with the powder or granules to be lubricated, so that the particle size of the lubricant greatly affects its performance. Here, the average particle diameter refers to a representative diameter of a particle group having two or more kinds of particle diameters, and is determined as a central cumulative value by a specific surface area measurement method.

【0009】このような植物性油脂粉末は植物性油脂に
蛋白質と糖質を配合して乳化させ噴霧乾燥することによ
って製造することができる。具体的には適量の水に植物
性油脂と植物性油脂100重量部に対して蛋白質8〜1
2重量部、糖質30〜40重量部、及び必要に応じて前
記食品添加物を配合して乳化させ、噴霧乾燥によって粉
末化することができる。
[0009] Such a vegetable oil and fat powder can be produced by blending a vegetable oil and fat with a protein and a carbohydrate, emulsifying and spray drying. Specifically, protein 8 to 1 to 100 parts by weight of vegetable oil and fat and vegetable oil and fat in an appropriate amount of water.
2 parts by weight, 30 to 40 parts by weight of carbohydrate and, if necessary, the above-mentioned food additive are blended and emulsified, and powdered by spray drying.

【0010】本発明における植物性油脂粉末は植物性油
脂を主成分とするものであり、植物性油脂の特徴、利点
を損なわない範囲で、崩壊剤、賦形剤、吸収剤と配合し
て使用することができる。例えばリン酸カルシウム、炭
酸カルシウム等があげられる。また、ステアリン酸マグ
ネシウム、精製タルク、ショ糖脂肪酸エステル、ポリグ
リセリン脂肪酸エステル、フマル酸といった従来の滑沢
剤も併用できる。
The vegetable oil powder of the present invention is mainly composed of vegetable oils and fats, and is used in combination with disintegrants, excipients and absorbents as long as the characteristics and advantages of the vegetable oils and fats are not impaired. can do. For example, calcium phosphate, calcium carbonate and the like can be mentioned. Conventional lubricants such as magnesium stearate, purified talc, sucrose fatty acid ester, polyglycerin fatty acid ester and fumaric acid can also be used in combination.

【0011】錠剤、錠菓の製造過程は、圧縮成型するた
めの粉末または顆粒を製造する造粒プロセスと、圧縮成
型する打錠プロセスに分けられるが、本発明に係る滑沢
剤は一般に造粒プロセス後に添加される。添加量は0.
2〜5重量%であるが、要求される機能によって添加量
はその限りではない。また、本発明に用いられる滑沢剤
は直接錠剤製造法、湿式錠剤製造法のどちらでも用いる
ことができる。
The manufacturing process of tablets and confectionery is divided into a granulation process for producing powder or granules for compression molding and a tableting process for compression molding. The lubricant according to the present invention is generally used for granulation. Added after process. The addition amount is 0.
The content is 2 to 5% by weight, but the addition amount is not limited depending on the required function. The lubricant used in the present invention can be used in either a direct tablet production method or a wet tablet production method.

【0012】[0012]

【実施例】以下に本発明の実施例を示すが、本発明はこ
れらのみに限定されるものではない。 製造例1 60℃の温水4.0kgに乳糖1.2kg、デキストリ
ン1.2kg及びカゼインソーダ0.6kgを添加して
10分間撹拌する。次に7.0kg食用パーム油を65
℃に加熱溶解し、上記水溶液に徐々に添加して乳化し
た。得られたエマルジョンを噴霧乾燥して粉末油脂を作
成した。この粉末油脂の平均粒子径は約230μmだっ
た。
EXAMPLES Examples of the present invention will be shown below, but the present invention is not limited only to these. Production Example 1 1.2 kg of lactose, 1.2 kg of dextrin and 0.6 kg of casein soda were added to 4.0 kg of warm water at 60 ° C., and the mixture was stirred for 10 minutes. Next, add 7.0 kg of edible palm oil to 65
The mixture was heated and dissolved at ℃, and gradually added to the aqueous solution to emulsify. The obtained emulsion was spray-dried to prepare a powdered fat. The average particle size of the powdered fat was about 230 μm.

【0013】実施例1〜2、比較例1〜4 無水結晶ブドウ糖85重量%、デキストリン15重量%
を造粒した後に表1に示す滑沢剤を全体に対して所定量
になるように混合し、この混合物を打錠径=5mm、打
錠圧=1200kgfで打錠を行った。これらの評価結
果を表1に併せて示す。なお、評価は肉眼観察により行
った。
Examples 1-2, Comparative Examples 1-4 Anhydrous crystalline glucose 85% by weight, dextrin 15% by weight
Was granulated, and the lubricants shown in Table 1 were mixed in a predetermined amount with respect to the whole, and the mixture was tableted at a tablet diameter of 5 mm and a tablet pressure of 1200 kgf. The evaluation results are shown in Table 1. In addition, evaluation was performed by visual observation.

【0014】[0014]

【表1】 [Table 1]

【0015】実施例3〜4、比較例5〜8 還元麦芽糖48.5重量%、還元乳糖21.4重量%、
アスコルビン酸12.8重量%、アスコルビン酸ナトリ
ウム6.5重量%、グァガム5.8重量%、エリスリト
ール5.0重量%を造粒した後に表1に示す滑沢剤を全
体に対して所定量になるように混合し、この混合物を打
錠径=5mm、打錠圧=1200kgfで打錠を行っ
た。これらの評価結果を表2に併せて示す。
Examples 3-4, Comparative Examples 5-8 Reduced maltose 48.5% by weight, reduced lactose 21.4% by weight,
After granulating 12.8% by weight of ascorbic acid, 6.5% by weight of sodium ascorbate, 5.8% by weight of guar gum, and 5.0% by weight of erythritol, the lubricant shown in Table 1 was added to a predetermined amount with respect to the whole. The resulting mixture was tableted at a tablet diameter of 5 mm and a tablet pressure of 1200 kgf. These evaluation results are also shown in Table 2.

【0016】[0016]

【表2】 [Table 2]

【0017】[0017]

【発明の効果】本発明に係る植物性油脂粉末は従来の滑
沢剤よりも天然の植物成分より抽出したものなので極め
て安全性が高い。また、表1,2の評価結果に示した如
く、油脂を蛋白質、糖質を用いて乳化し、噴霧乾燥させ
ることで保存安定性に優れた油脂粉末が得られ、少量の
添加量でキャッピング、スティッキング及びバインディ
ングを起こさない、結着性のよい、硬い錠剤、錠菓が得
られる。
The vegetable oil and fat powder according to the present invention is extremely safe because it is extracted from natural plant components more than conventional lubricants. In addition, as shown in the evaluation results of Tables 1 and 2, fats and oils are emulsified using proteins and carbohydrates, and a fat and oil powder having excellent storage stability is obtained by spray drying. Hard tablets and confections which do not cause sticking and binding and have good binding properties are obtained.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 石渡 健一 神奈川県横浜市栄区飯島町53番地 株式会 社ファンケル内 Fターム(参考) 4B014 GB08 GG12 GG14 GK12 GL10 GP23 GQ07 4C076 AA36 CC40 DD38 DD59 DD67 EE38 EE41 EE53 EE58 FF09 FF36 FF67 GG14 GG50  ────────────────────────────────────────────────── ─── Continued on the front page (72) Inventor Kenichi Ishiwatari F-term in FANCL, 53 53 Iijimacho, Sakae-ku, Yokohama-shi, Kanagawa 4B014 GB08 GG12 GG14 GK12 GL10 GP23 GQ07 4C076 AA36 CC40 DD38 DD59 DD67 EE38 EE41 EE53 EE58 FF09 FF36 FF67 GG14 GG50

Claims (4)

【特許請求の範囲】[Claims] 【請求項1】 植物性油脂に蛋白質及び糖質を添加して
粉末化した植物性油脂粉末よりなることを特徴とする錠
剤又は錠菓用滑沢剤。
1. A lubricating agent for tablets or confections, comprising a vegetable oil or fat powder obtained by adding protein and sugar to vegetable oil or fat.
【請求項2】 植物性油脂粉末が平均粒子径250μm
以下の微粉末であることを特徴とする請求項1記載の錠
剤又は錠菓用滑沢剤。
2. The vegetable oil powder has an average particle diameter of 250 μm.
The lubricating agent for tablets or confections according to claim 1, which is the following fine powder.
【請求項3】 植物性油脂に蛋白質及び糖質を配合して
乳化させ噴霧乾燥することによって作られることを特徴
とする請求項1又は2記載の錠剤又は錠菓用滑沢剤。
3. The lubricant for tablets or confections according to claim 1, wherein the lubricant is prepared by blending a vegetable oil or fat with a protein and a carbohydrate, emulsifying and spray-drying.
【請求項4】 請求項1〜3のいずれか1項の滑沢剤を
添加してなることを特徴とする錠剤又は錠菓。
4. A tablet or confection comprising the lubricant according to claim 1 added thereto.
JP36075198A 1998-12-18 1998-12-18 Lubricant containing plant fat and oil Pending JP2000178206A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP36075198A JP2000178206A (en) 1998-12-18 1998-12-18 Lubricant containing plant fat and oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP36075198A JP2000178206A (en) 1998-12-18 1998-12-18 Lubricant containing plant fat and oil

Publications (1)

Publication Number Publication Date
JP2000178206A true JP2000178206A (en) 2000-06-27

Family

ID=18470768

Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Status (1)

Country Link
JP (1) JP2000178206A (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002188095A (en) * 2000-12-21 2002-07-05 Fancl Corp Vegetable oil and fat powder and food composition containing the powder
JP2002326961A (en) * 2001-04-27 2002-11-15 Taiyo Kagaku Co Ltd Lubricant for making tablet
JP2003073691A (en) * 2001-08-30 2003-03-12 Nof Corp Protein-free powdered fat composition and its use
WO2008130883A1 (en) * 2007-04-16 2008-10-30 Wyeth Embedded liquid lubricants for tableting
WO2017005889A1 (en) * 2015-07-07 2017-01-12 Perora Gmbh Edible particles comprising a polysaccharide and a lipid
WO2017005890A1 (en) * 2015-07-07 2017-01-12 Perora Gmbh Method of inducing satiety
WO2017140902A1 (en) * 2016-02-18 2017-08-24 Perora Gmbh Kits comprising satiety-inducing formulations
US11311570B2 (en) 2014-08-11 2022-04-26 Perora Gmbh Method of inducing satiety
US11504330B2 (en) 2014-08-11 2022-11-22 Perora Gmbh Formulation comprising particles containing a water-swellable or water-soluble polymeric component and a lipid component

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002188095A (en) * 2000-12-21 2002-07-05 Fancl Corp Vegetable oil and fat powder and food composition containing the powder
JP2002326961A (en) * 2001-04-27 2002-11-15 Taiyo Kagaku Co Ltd Lubricant for making tablet
JP2003073691A (en) * 2001-08-30 2003-03-12 Nof Corp Protein-free powdered fat composition and its use
US11013251B2 (en) 2007-04-16 2021-05-25 PF Consumer Healthcare 1, LLC Embedded liquid lubricants for tableting
WO2008130883A1 (en) * 2007-04-16 2008-10-30 Wyeth Embedded liquid lubricants for tableting
AU2008242256B2 (en) * 2007-04-16 2011-11-03 Pf Consumer Healthcare 1 Llc Embedded liquid lubricants for tableting
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