IT1003183B - Solventi per la spettroscopia di risonanza nucleare - Google Patents

Solventi per la spettroscopia di risonanza nucleare

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Publication number
IT1003183B
IT1003183B IT30249/73A IT3024973A IT1003183B IT 1003183 B IT1003183 B IT 1003183B IT 30249/73 A IT30249/73 A IT 30249/73A IT 3024973 A IT3024973 A IT 3024973A IT 1003183 B IT1003183 B IT 1003183B
Authority
IT
Italy
Prior art keywords
solvents
resonance spectroscopy
nuclear resonance
nuclear
spectroscopy
Prior art date
Application number
IT30249/73A
Other languages
English (en)
Italian (it)
Original Assignee
Merck Patent Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Merck Patent Gmbh filed Critical Merck Patent Gmbh
Application granted granted Critical
Publication of IT1003183B publication Critical patent/IT1003183B/it

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C317/00Sulfones; Sulfoxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00Carbonates of sodium, potassium or alkali metals in general
    • C01D7/07Preparation from the hydroxides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02Monocyclic hydrocarbons
    • C07C15/04Benzene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/10Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/16Preparation of halogenated hydrocarbons by replacement by halogens of hydroxyl groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/01Acyclic saturated compounds containing halogen atoms containing chlorine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/01Acyclic saturated compounds containing halogen atoms containing chlorine
    • C07C19/03Chloromethanes
    • C07C19/04Chloroform
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/01Acyclic saturated compounds containing halogen atoms containing chlorine
    • C07C19/03Chloromethanes
    • C07C19/041Carbon tetrachloride
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00Carboxylic acid nitriles
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C275/00Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C275/04Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups bound to acyclic carbon atoms
    • C07C275/06Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups bound to acyclic carbon atoms of an acyclic and saturated carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C07C29/151Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02Monohydroxylic acyclic alcohols
    • C07C31/04Methanol
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02Monohydroxylic acyclic alcohols
    • C07C31/08Ethanol
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C321/00Thiols, sulfides, hydropolysulfides or polysulfides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00Ethers; Compounds having groups, groups or groups
    • C07C43/02Ethers
    • C07C43/03Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04Saturated ethers
    • C07C43/06Diethyl ether
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/04Saturated compounds containing keto groups bound to acyclic carbon atoms
    • C07C49/08Acetone
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/15Preparation of carboxylic acids or their salts, halides or anhydrides by reaction of organic compounds with carbon dioxide, e.g. Kolbe-Schmitt synthesis
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/363Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/02Formic acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/15Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen containing halogen
    • C07C53/16Halogenated acetic acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/12Acetic acid esters
    • C07C69/14Acetic acid esters of monohydroxylic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/06Phosphorus compounds without P—C bonds
    • C07F9/22Amides of acids of phosphorus
    • C07F9/224Phosphorus triamides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00Indexing scheme relating to specific properties of organic compounds
    • C07B2200/05Isotopically modified compounds, e.g. labelled
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00Chemistry: analytical and immunological testing
    • Y10T436/24Nuclear magnetic resonance, electron spin resonance or other spin effects or mass spectrometry

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
IT30249/73A 1972-11-21 1973-10-18 Solventi per la spettroscopia di risonanza nucleare IT1003183B (it)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2257005A DE2257005A1 (de) 1972-11-21 1972-11-21 Loesungsmittel fuer die kernresonanzspektroskopie

Publications (1)

Publication Number Publication Date
IT1003183B true IT1003183B (it) 1976-06-10

Family

ID=5862323

Family Applications (1)

Application Number Title Priority Date Filing Date
IT30249/73A IT1003183B (it) 1972-11-21 1973-10-18 Solventi per la spettroscopia di risonanza nucleare

Country Status (9)

Country Link
US (1) US3954410A (en:Method)
JP (1) JPS4989592A (en:Method)
BE (1) BE807386A (en:Method)
CH (1) CH589291A5 (en:Method)
DE (1) DE2257005A1 (en:Method)
FR (1) FR2207101B1 (en:Method)
GB (1) GB1405970A (en:Method)
IT (1) IT1003183B (en:Method)
NL (1) NL7312574A (en:Method)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4532218A (en) * 1981-06-29 1985-07-30 Mobil Oil Corporation Identification of carbon-containing ions adsorbed on ion-exchange resins by nuclear magnetic resonance spectroscopy
JP5782038B2 (ja) * 2009-10-09 2015-09-24 ダウ グローバル テクノロジーズ エルエルシー 等温多管式反応器及び該反応器を組み込んだプロセス
BR112012007913A2 (pt) * 2009-10-09 2019-09-24 Dow Global Technologies Llc reator adiabático de fluxo pistonado, processo para produzir um prpeno clorado ou fluorado, processo para preparar um produto a jusante e processo para preparar 2,3,3,3-tetrafluoroprop-1-eno (hfo-123yf) ou 1,3,3,3-tetrafluoroprop-1-eno (hfo-123ze)
WO2011044536A1 (en) * 2009-10-09 2011-04-14 Dow Global Technologies, Inc Process for the production of chlorinated and/or fluorinated propenes and higher alkenes
JP5706432B2 (ja) * 2009-10-09 2015-04-22 ダウ グローバル テクノロジーズ エルエルシー 塩素化及び/又はフッ素化プロペンの製造方法
CA2836493A1 (en) 2011-05-31 2012-12-06 Max Markus Tirtowidjojo Process for the production of chlorinated propenes
JP5918358B2 (ja) 2011-05-31 2016-05-18 ブルー キューブ アイピー エルエルシー 塩素化プロペンの製造方法
CA2837956C (en) 2011-06-08 2016-06-28 Dow Agrosciences, Llc Process for the production of chlorinated and/or fluorinated propenes
CA2844319A1 (en) 2011-08-07 2013-02-14 Dow Global Technologies Llc Process for the production of chlorinated propenes
CA2844207A1 (en) 2011-08-07 2013-02-14 Max Markus Tirtowidjojo Process for the production of chlorinated propenes
US9067855B2 (en) 2011-11-21 2015-06-30 Dow Global Technologies Llc Process for the production of chlorinated alkanes
EP2785671B1 (en) 2011-12-02 2017-03-01 Blue Cube IP LLC Process for the production of chlorinated propanes
US9199899B2 (en) 2011-12-02 2015-12-01 Blue Cube Ip Llc Process for the production of chlorinated alkanes
JP6170068B2 (ja) 2011-12-13 2017-07-26 ブルー キューブ アイピー エルエルシー 塩素化プロパン及びプロペンの製造方法
EP2794528B1 (en) 2011-12-22 2020-02-26 Blue Cube IP LLC Process for the production of tetrachloromethane
WO2013096706A1 (en) 2011-12-23 2013-06-27 Dow Global Technologies, Llc Process for the production of alkenes and/or aromatic compounds
CA2884435A1 (en) 2012-09-20 2014-03-27 Dow Global Technologies Llc Process for the production of chlorinated propenes
WO2014046970A1 (en) 2012-09-20 2014-03-27 Dow Global Technologies, Llc Process for the production of chlorinated propenes
IN2015DN03119A (en:Method) 2012-09-30 2015-10-02 Dow Global Technologies Llc
IN2015DN03949A (en:Method) 2012-10-26 2015-10-02 Dow Global Technologies Llc
EP2935165A1 (en) 2012-12-18 2015-10-28 Blue Cube IP LLC Process for the production of chlorinated propenes
EP2935166A1 (en) 2012-12-19 2015-10-28 Blue Cube IP LLC Process for the production of chlorinated propenes
CN104981449B (zh) 2013-02-27 2016-12-28 蓝立方知识产权有限责任公司 用于生产氯化丙烯的方法
JP6449791B2 (ja) 2013-03-09 2019-01-09 ブルー キューブ アイピー エルエルシー クロロアルカンの製造方法
CN109415281B (zh) 2016-07-05 2022-04-26 西方化学股份有限公司 氯仿光氯化为四氯化碳
CN108047050B (zh) * 2017-11-15 2020-06-26 成都海创药业有限公司 一种以卤代氘代甲烷合成氘代二甲胺盐的方法
JP7520850B2 (ja) 2019-01-10 2024-07-23 オキシデンタル ケミカル コーポレーション 部分的に塩素化されたクロロメタンから四塩化炭素への光塩素化
CN118271152B (zh) * 2024-05-31 2024-08-09 安徽泽升科技股份有限公司 一种氘代碘甲烷的连续合成方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1475608A (fr) * 1964-04-30 1967-04-07 Inst Francais Du Petrole Procédé de détection des hydrocarbures
FR94310E (fr) * 1964-04-30 1969-08-01 Inst Francais Du Petrole Procédé de détection des hydrocarbures.
BE756934R (fr) * 1969-10-15 1971-03-16 Commissariat Energie Atomique Nouveau procede de polarisation dynamique des noyaux atomiques d'un solvant, notamment d'un solvant hydrogene, et magnetometres pourla mesure de l'intensite des champs magnetiques faibles notamment du champ magnetique terrestre, mettant en oeuvre ce procede
US3700410A (en) * 1971-09-24 1972-10-24 Robert E Sievers Rare earth complexes as nuclear magnetic resonance shift reagents
US3846333A (en) * 1971-09-24 1974-11-05 R Sievers Rare earth complexes as nuclear magnetic resonance shift reagents
US3730687A (en) * 1971-09-28 1973-05-01 Us Air Force Spectral separation and analysis of isomeric azoxybenzenes
US3756779A (en) * 1971-11-16 1973-09-04 Us Air Force Spectral analysis of ketoximes

Also Published As

Publication number Publication date
US3954410A (en) 1976-05-04
GB1405970A (en) 1975-09-10
DE2257005A1 (de) 1974-05-22
NL7312574A (en:Method) 1974-05-24
FR2207101B1 (en:Method) 1977-06-10
JPS4989592A (en:Method) 1974-08-27
BE807386A (fr) 1974-05-16
CH589291A5 (en:Method) 1977-06-30
FR2207101A1 (en:Method) 1974-06-14

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