IN2015KN00624A - - Google Patents
Info
- Publication number
- IN2015KN00624A IN2015KN00624A IN624KON2015A IN2015KN00624A IN 2015KN00624 A IN2015KN00624 A IN 2015KN00624A IN 624KON2015 A IN624KON2015 A IN 624KON2015A IN 2015KN00624 A IN2015KN00624 A IN 2015KN00624A
- Authority
- IN
- India
- Prior art keywords
- crystallizer
- recycle
- crystals
- potassium
- aqueous solution
- Prior art date
Links
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 abstract 4
- 239000013078 crystal Substances 0.000 abstract 4
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 abstract 3
- 229910052939 potassium sulfate Inorganic materials 0.000 abstract 3
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 229910052943 magnesium sulfate Inorganic materials 0.000 abstract 2
- 235000019341 magnesium sulphate Nutrition 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 235000011151 potassium sulphates Nutrition 0.000 abstract 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract 1
- 239000012267 brine Substances 0.000 abstract 1
- 239000012530 fluid Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000011591 potassium Substances 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/12—Preparation of double sulfates of magnesium with sodium or potassium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/02—Crystallisation from solutions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/06—Preparation of sulfates by double decomposition
- C01D5/10—Preparation of sulfates by double decomposition with sulfates of magnesium, calcium, strontium, or barium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/16—Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
- Seasonings (AREA)
- Fodder In General (AREA)
- Fertilizers (AREA)
- Removal Of Specific Substances (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201261699917P | 2012-09-12 | 2012-09-12 | |
PCT/US2013/059040 WO2014043118A1 (en) | 2012-09-12 | 2013-09-10 | Methods of processing potassium sulfate and magnesium sulfate, and related systems |
Publications (1)
Publication Number | Publication Date |
---|---|
IN2015KN00624A true IN2015KN00624A (cs) | 2015-07-17 |
Family
ID=50233481
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IN624KON2015 IN2015KN00624A (cs) | 2012-09-12 | 2013-09-10 |
Country Status (6)
Country | Link |
---|---|
US (2) | US8802048B2 (cs) |
EP (1) | EP2895427A4 (cs) |
CN (1) | CN104755426B (cs) |
CA (1) | CA2883806C (cs) |
IN (1) | IN2015KN00624A (cs) |
WO (1) | WO2014043118A1 (cs) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014043118A1 (en) * | 2012-09-12 | 2014-03-20 | Intercontinental Potash Corporation | Methods of processing potassium sulfate and magnesium sulfate, and related systems |
GB2522492B (en) | 2014-06-02 | 2020-07-15 | York Potash Ltd | Dry powder processing |
CA2860275C (en) | 2014-06-02 | 2016-10-25 | Veolia Water Solutions & Technologies North America, Inc. | Oil recovery process including a high solids crystallizer for treating evaporator blowdown |
GB2530757B (en) * | 2014-09-30 | 2019-04-24 | York Potash Ltd | Pelletising process |
CN105036156A (zh) * | 2015-08-27 | 2015-11-11 | 莫红兵 | 一种硫酸钾晶体生长促进剂及其应用 |
US11059756B1 (en) | 2015-09-29 | 2021-07-13 | Intrepid Potash, Inc. | Pelletized fertilizer and methods of preparing pelletized fertilizer |
EP3222584A1 (en) | 2016-03-21 | 2017-09-27 | Tessenderlo Chemie NV | Method for producing soluble potassium sulfate |
CN106379917B (zh) * | 2016-08-29 | 2017-11-24 | 化工部长沙设计研究院 | 一种用杂卤石制备硫酸钾的工艺 |
CA3076265C (en) * | 2017-10-13 | 2021-05-25 | Novopro Projects Inc. | Systems and methods of producing potassium sulfate |
US11326088B2 (en) | 2019-06-07 | 2022-05-10 | Lyondellbasell Advanced Polymers Inc. | Low temperature diversion in well completion operations using natural mineral compound |
CN111908535B (zh) * | 2020-08-20 | 2022-04-29 | 江苏迈安德节能蒸发设备有限公司 | 硫酸镁生产废水零排放资源化处理系统及处理方法 |
Family Cites Families (74)
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US1812497A (en) | 1927-06-22 | 1931-06-30 | Humble Oil & Refining Company | Recovery of potassium sulphate from polyhalite |
US2020322A (en) | 1927-08-11 | 1935-11-12 | Rita Vinay | Process of treatment of complex materials containing potassium salts |
US1794552A (en) | 1928-12-29 | 1931-03-03 | Eugene P Schoch | Process of recovering salts from minerals |
US1924519A (en) | 1930-09-03 | 1933-08-29 | Eugene P Schoch | Treatment of minerals |
US1939174A (en) * | 1931-09-01 | 1933-12-12 | Kaselitz Oskar | Production of alkali metal sulphates |
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US2809093A (en) * | 1955-05-03 | 1957-10-08 | Int Minerals & Chem Corp | Production of potassium sulfate from langbeinite |
US2862788A (en) | 1955-05-03 | 1958-12-02 | Int Minerals & Chem Corp | Process for purifying impure solid-phase kainite |
US2860951A (en) | 1955-07-28 | 1958-11-18 | Horizons Inc | Recovery of values in naturally occurring alkali metal sulfate minerals |
US3004826A (en) | 1957-07-22 | 1961-10-17 | Montedison Spa | Process for obtaining schoenite by direct treatment of kainite containing sodium chloride as an impurity |
US3058806A (en) | 1959-01-16 | 1962-10-16 | Metallgesellschaft Ag | Method of preparing potassium sulfate from kainite |
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US3110561A (en) | 1960-03-19 | 1963-11-12 | Wintershall Ag | Process for the production of potassium sulfate |
DE1159414B (de) | 1961-05-05 | 1963-12-19 | Wintershall Ag | Verfahren zur Herstellung von Kaliumsulfat |
US3271106A (en) | 1963-10-09 | 1966-09-06 | Int Minerals & Chem Corp | Production of potassium sulfate and potassium chloride |
US3285025A (en) * | 1963-12-20 | 1966-11-15 | Phillips Petroleum Co | Multi-stage crystallization process |
CH431576A (de) | 1964-01-07 | 1967-03-15 | Inventa Ag | Verfahren zum Granulieren von stickstoffhaltigen Düngemitteln |
US3396086A (en) | 1964-12-23 | 1968-08-06 | Applied Res And Engineering Lt | Recompression evaporators |
US3528767A (en) | 1966-03-16 | 1970-09-15 | Donald E Garrett | Production of potassium chloride,potassium sulfate and sodium sulfate from brines and the like containing potassium,chloride and sulfate |
GB1183938A (en) | 1966-09-21 | 1970-03-11 | Fisons Ltd | Prilling |
US3547597A (en) * | 1967-05-22 | 1970-12-15 | Phillips Petroleum Co | Method for producing high-purity crystals using serially connected crystallization zones |
US3630713A (en) | 1968-07-22 | 1971-12-28 | Duval Corp | Method of producing fertilizer granules |
US3634041A (en) | 1969-02-14 | 1972-01-11 | Great Salt Lake Minerals | Method for the production of potassium sulfate from potassium-containing double salts of magnesium sulfate |
US3617243A (en) | 1970-03-23 | 1971-11-02 | Great Salt Lake Minerals | Process for the production of anhydrous potassium magnesium sulfate material with low hygroscopicity from hydrated potassium magnesium sulfate material |
US3843772A (en) | 1972-09-14 | 1974-10-22 | Int Minerals & Chem Corp | Production of white potassium sulfate crystals |
US3926609A (en) | 1974-04-18 | 1975-12-16 | Kali & Salz Ag | Granular mgo-containing potassium salt fertilizers and process for their manufacture |
US3998935A (en) | 1975-01-30 | 1976-12-21 | Pennzoil Company | Manufacture of potassium sulfate |
US4026696A (en) | 1975-02-24 | 1977-05-31 | Union Oil Company Of California | Particulate multicomponent soil additive |
US4045335A (en) | 1976-03-10 | 1977-08-30 | Duval Corporation | Beneficiation of kieserite and langbeinite from a langbeinite ore |
US4183738A (en) | 1977-05-09 | 1980-01-15 | International Fertilizer Development Center | Granulation process and products produced thereby |
US4306880A (en) | 1978-09-22 | 1981-12-22 | Garrett Donald E | Recovering by-products from sea water brines and the like |
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US4246019A (en) | 1979-02-21 | 1981-01-20 | Sokolov Igor D | Method of producing a complex mineral fertilizer |
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IT1140901B (it) * | 1979-07-05 | 1986-10-10 | Ind Sali Potassici Ed Affini S | Procedimento per la produzione di solfato potassico partendo da un minerale contenente polialite, langbeinite ed altri sali di potassio |
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DE3332250C1 (de) | 1983-09-07 | 1984-10-25 | Kali Und Salz Ag, 3500 Kassel | Verwendung einer Langbeinit-Trübe als Bindemittel |
US4554151A (en) | 1983-09-27 | 1985-11-19 | Prodeco, Inc. | Process for producing K3 H(SO4)2 crystals and potassium sulfate crystals |
DE3435124C2 (de) | 1984-09-25 | 1987-03-05 | Kali Und Salz Ag, 3500 Kassel | Verfahren zur Herstellung von Kaliumchlorid mit über 55 Gew.-%K↓2↓O aus dem Feinzersetzungssalz der Carnallitzersetzung |
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US5078779A (en) | 1988-12-01 | 1992-01-07 | Martin Marietta Magnesia Specialties Inc. | Binder for the granulation of fertilizers such as ammonium sulfate |
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US5298050A (en) * | 1992-10-09 | 1994-03-29 | Great Salt Lake Minerals Corporation | High water solubility potassium sulfate and method of producing same |
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FI981490A7 (fi) | 1998-06-29 | 1999-12-30 | Kemira Agro Oy | Menetelmä seoslannoitteiden valmistamiseksi |
US6143271A (en) * | 1998-09-14 | 2000-11-07 | Dead Sea Works | Process for producing potassium sulfate from potash and sodium sulfate |
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CA2542289A1 (en) | 2005-04-07 | 2006-10-07 | The Mosaic Company | Use of urea-formaldehyde resin in potash ore processing |
CN100360693C (zh) * | 2005-09-08 | 2008-01-09 | 成都理工大学 | 对杂卤石矿中钾的溶浸开采方法 |
DE102005045055A1 (de) * | 2005-09-21 | 2007-03-22 | Kali-Umwelttechnik Gmbh | Verfahren zur Kaliumsulfatherstellung aus Kaliumchlorid und Schwefelsäure ohne Anfall von Chlorwasserstoff |
CN1789129B (zh) * | 2005-12-12 | 2010-10-06 | 中国科学院青海盐湖研究所 | 利用硫酸镁亚型含钾盐湖卤水提取硫酸钾的方法 |
FI118598B (fi) | 2006-05-17 | 2008-01-15 | Kemira Growhow Oyj | Lannoiterae ja menetelmä sen valmistamiseksi |
CN100484883C (zh) * | 2007-04-24 | 2009-05-06 | 天津长芦海晶集团有限公司 | 以制盐废液为原料生产精制盐的制备工艺 |
US7604792B2 (en) * | 2007-10-17 | 2009-10-20 | Searles Valley Minerals Operations Inc. | Separation of purified potassium sulfate from glaserite |
DE102007058666B4 (de) * | 2007-12-19 | 2010-11-25 | K-Utec Ag Salt Technologies | Verfahren zur Verarbeitung von Polyhalit zum Zweck der Herstellung von Langbeinit, Kaliumsulfat und Flüssigdünger |
ATE488140T1 (de) * | 2009-02-20 | 2010-12-15 | Christoph Mahnkopp | Verfahren zur verwertung von backwaren und anlage dazu |
US8388916B2 (en) | 2009-06-25 | 2013-03-05 | Imi Tami Institute For Research And Development | Process for production of commercial quality potassium nitrate from polyhalite |
IN2014CN03665A (cs) * | 2011-11-14 | 2015-07-03 | Intercontinental Potash Corp Usa | |
WO2014043118A1 (en) * | 2012-09-12 | 2014-03-20 | Intercontinental Potash Corporation | Methods of processing potassium sulfate and magnesium sulfate, and related systems |
-
2013
- 2013-09-10 WO PCT/US2013/059040 patent/WO2014043118A1/en unknown
- 2013-09-10 EP EP13837230.5A patent/EP2895427A4/en not_active Withdrawn
- 2013-09-10 IN IN624KON2015 patent/IN2015KN00624A/en unknown
- 2013-09-10 CN CN201380056997.6A patent/CN104755426B/zh active Active
- 2013-09-10 CA CA2883806A patent/CA2883806C/en active Active
- 2013-09-10 US US14/023,347 patent/US8802048B2/en active Active
-
2014
- 2014-07-25 US US14/341,644 patent/US9139446B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
US9139446B2 (en) | 2015-09-22 |
US8802048B2 (en) | 2014-08-12 |
EP2895427A4 (en) | 2016-05-04 |
CN104755426B (zh) | 2017-05-31 |
EP2895427A1 (en) | 2015-07-22 |
CA2883806A1 (en) | 2014-03-20 |
WO2014043118A1 (en) | 2014-03-20 |
US20140072507A1 (en) | 2014-03-13 |
CA2883806C (en) | 2018-04-10 |
CN104755426A (zh) | 2015-07-01 |
US20140334995A1 (en) | 2014-11-13 |
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