IL40777A - Process for the preparation of 4-chloro-2,5-dimethoxy-aniline - Google Patents
Process for the preparation of 4-chloro-2,5-dimethoxy-anilineInfo
- Publication number
- IL40777A IL40777A IL40777A IL4077772A IL40777A IL 40777 A IL40777 A IL 40777A IL 40777 A IL40777 A IL 40777A IL 4077772 A IL4077772 A IL 4077772A IL 40777 A IL40777 A IL 40777A
- Authority
- IL
- Israel
- Prior art keywords
- chloro
- mol
- dimethoxy
- platinum
- catalyst
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract 14
- YGUFQYGSBVXPMC-UHFFFAOYSA-N 4-chloro-2,5-dimethoxyaniline Chemical compound COC1=CC(Cl)=C(OC)C=C1N YGUFQYGSBVXPMC-UHFFFAOYSA-N 0.000 title abstract 3
- 239000003054 catalyst Substances 0.000 claims abstract 7
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims abstract 6
- 150000002828 nitro derivatives Chemical class 0.000 claims abstract 5
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims abstract 3
- ORLPGMKKCAEWOW-UHFFFAOYSA-N 1-chloro-2,5-dimethoxy-4-nitrobenzene Chemical compound COC1=CC([N+]([O-])=O)=C(OC)C=C1Cl ORLPGMKKCAEWOW-UHFFFAOYSA-N 0.000 claims abstract 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims abstract 2
- 239000004280 Sodium formate Substances 0.000 claims abstract 2
- GOBGCUAZYIPRTM-UHFFFAOYSA-N [Na+].[Na+].OB(O)OB([O-])[O-] Chemical compound [Na+].[Na+].OB(O)OB([O-])[O-] GOBGCUAZYIPRTM-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000007864 aqueous solution Substances 0.000 claims abstract 2
- 229910021538 borax Inorganic materials 0.000 claims abstract 2
- 239000003795 chemical substances by application Substances 0.000 claims abstract 2
- 238000004519 manufacturing process Methods 0.000 claims abstract 2
- 229910052697 platinum Inorganic materials 0.000 claims abstract 2
- 239000001632 sodium acetate Substances 0.000 claims abstract 2
- 235000017281 sodium acetate Nutrition 0.000 claims abstract 2
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 claims abstract 2
- 235000019254 sodium formate Nutrition 0.000 claims abstract 2
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 229910052799 carbon Inorganic materials 0.000 claims 1
- AJFXNBUVIBKWBT-UHFFFAOYSA-N disodium;boric acid;hydrogen borate Chemical compound [Na+].[Na+].OB(O)O.OB(O)O.OB(O)O.OB([O-])[O-] AJFXNBUVIBKWBT-UHFFFAOYSA-N 0.000 claims 1
- 238000005984 hydrogenation reaction Methods 0.000 claims 1
- FSUMZUVANZAHBW-UHFFFAOYSA-N n,n-dimethoxyaniline Chemical compound CON(OC)C1=CC=CC=C1 FSUMZUVANZAHBW-UHFFFAOYSA-N 0.000 claims 1
- 238000009738 saturating Methods 0.000 claims 1
- 239000012928 buffer substance Substances 0.000 abstract 2
- 239000012431 aqueous reaction media Substances 0.000 abstract 1
- 239000003849 aromatic solvent Substances 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 abstract 1
- 239000004328 sodium tetraborate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/42—Platinum
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/18—Carbon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/20—Sulfiding
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2156051A DE2156051C3 (de) | 1971-11-11 | 1971-11-11 | Verfahren zur Herstellung von 4-Chlor-2,5-dimethoxy-anilin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL40777A0 IL40777A0 (en) | 1973-01-30 |
| IL40777A true IL40777A (en) | 1976-04-30 |
Family
ID=5824830
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL40777A IL40777A (en) | 1971-11-11 | 1972-11-08 | Process for the preparation of 4-chloro-2,5-dimethoxy-aniline |
Country Status (20)
| Country | Link |
|---|---|
| JP (1) | JPS5644060B2 (OSRAM) |
| AT (1) | AT331210B (OSRAM) |
| AU (1) | AU474209B2 (OSRAM) |
| BE (1) | BE791300A (OSRAM) |
| CA (1) | CA995248A (OSRAM) |
| CH (1) | CH575377A5 (OSRAM) |
| CS (1) | CS173610B2 (OSRAM) |
| DD (1) | DD99356A5 (OSRAM) |
| DE (1) | DE2156051C3 (OSRAM) |
| ES (1) | ES408273A1 (OSRAM) |
| FR (1) | FR2160166A5 (OSRAM) |
| GB (1) | GB1393428A (OSRAM) |
| HU (1) | HU165205B (OSRAM) |
| IL (1) | IL40777A (OSRAM) |
| IT (1) | IT970356B (OSRAM) |
| NL (1) | NL7214964A (OSRAM) |
| PL (1) | PL85137B1 (OSRAM) |
| RO (1) | RO62342A (OSRAM) |
| SU (1) | SU474135A3 (OSRAM) |
| ZA (1) | ZA727738B (OSRAM) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2455704C3 (de) * | 1974-11-25 | 1978-06-08 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von 4-Chlor-23-dimethoxy anilin |
| CA1148562A (en) * | 1979-02-22 | 1983-06-21 | Alfred J. Bird | Catalyst for the hydrogenation of halogen substituted aromatic nitro compounds |
| JPS58159957U (ja) * | 1982-04-19 | 1983-10-25 | 日本発条株式会社 | ヘツドレスト上，下調節機構 |
| DE3821013A1 (de) * | 1988-06-22 | 1989-12-28 | Hoechst Ag | Verfahren zur herstellung von 4-chlor-2,5-dimethoxyanilin |
-
0
- BE BE791300D patent/BE791300A/xx not_active IP Right Cessation
-
1971
- 1971-11-11 DE DE2156051A patent/DE2156051C3/de not_active Expired
-
1972
- 1972-10-18 DD DD166310A patent/DD99356A5/xx unknown
- 1972-11-01 ZA ZA727738A patent/ZA727738B/xx unknown
- 1972-11-02 RO RO72709A patent/RO62342A/ro unknown
- 1972-11-04 ES ES408273A patent/ES408273A1/es not_active Expired
- 1972-11-06 NL NL7214964A patent/NL7214964A/xx not_active Application Discontinuation
- 1972-11-07 CS CS7507A patent/CS173610B2/cs unknown
- 1972-11-07 AU AU48583/72A patent/AU474209B2/en not_active Expired
- 1972-11-08 IL IL40777A patent/IL40777A/en unknown
- 1972-11-08 GB GB5151772A patent/GB1393428A/en not_active Expired
- 1972-11-09 AT AT952372A patent/AT331210B/de not_active IP Right Cessation
- 1972-11-09 HU HUHO1523A patent/HU165205B/hu unknown
- 1972-11-09 SU SU1843993A patent/SU474135A3/ru active
- 1972-11-09 IT IT31481/72A patent/IT970356B/it active
- 1972-11-09 CH CH1630472A patent/CH575377A5/xx not_active IP Right Cessation
- 1972-11-10 CA CA156,152A patent/CA995248A/en not_active Expired
- 1972-11-10 PL PL1972158797A patent/PL85137B1/pl unknown
- 1972-11-10 FR FR7239905A patent/FR2160166A5/fr not_active Expired
- 1972-11-10 JP JP11219772A patent/JPS5644060B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2156051A1 (de) | 1973-05-17 |
| AU4858372A (en) | 1974-05-09 |
| AU474209B2 (en) | 1976-07-15 |
| ES408273A1 (es) | 1975-11-16 |
| GB1393428A (en) | 1975-05-07 |
| JPS4857938A (OSRAM) | 1973-08-14 |
| DE2156051C3 (de) | 1974-10-31 |
| IT970356B (it) | 1974-04-10 |
| FR2160166A5 (OSRAM) | 1973-06-22 |
| IL40777A0 (en) | 1973-01-30 |
| BE791300A (fr) | 1973-05-14 |
| CS173610B2 (OSRAM) | 1977-02-28 |
| AT331210B (de) | 1976-08-10 |
| CH575377A5 (OSRAM) | 1976-05-14 |
| RO62342A (OSRAM) | 1977-08-15 |
| SU474135A3 (ru) | 1975-06-14 |
| JPS5644060B2 (OSRAM) | 1981-10-16 |
| DE2156051B2 (de) | 1974-03-28 |
| HU165205B (OSRAM) | 1974-07-27 |
| DD99356A5 (OSRAM) | 1973-08-05 |
| ATA952372A (de) | 1975-11-15 |
| CA995248A (en) | 1976-08-17 |
| NL7214964A (OSRAM) | 1973-05-15 |
| ZA727738B (en) | 1973-09-26 |
| PL85137B1 (OSRAM) | 1976-04-30 |
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