GB1471490A - Method for the preparation of 1-amino-anthraquinone - Google Patents
Method for the preparation of 1-amino-anthraquinoneInfo
- Publication number
- GB1471490A GB1471490A GB5426374A GB5426374A GB1471490A GB 1471490 A GB1471490 A GB 1471490A GB 5426374 A GB5426374 A GB 5426374A GB 5426374 A GB5426374 A GB 5426374A GB 1471490 A GB1471490 A GB 1471490A
- Authority
- GB
- United Kingdom
- Prior art keywords
- product
- catalyst
- aminoanthraquinone
- dec
- glycol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
1471490 Preparing 1-aminoanthraquinone MITSUI TOATSU CHEMICALS Inc 16 Dec 1974 [21 Dec 1973] 54263/74 Heading C4P 1-Aminoanthraquinone is prepared by catalytically hydrogenating 1-nitroanthraquinone in an aqueous reaction medium in presence of a hydrogenation catalyst. The aqueous reaction medium may contain up to 10% by weight of a water-miscible solvent, e.g. methanol, ethanol, propanol, ethylene glycol, propylene glycol, glycerine, dioxane, 1,2-dimethoxyethane, 1,2- diethoxyethane, diethylene glycol or dipropylene glycol and the reaction which proceeds at 10-160‹ C. under pressure is facilitated by presence of a surface active agent. The catalysts used include palladium, platinum, ruthenium, rhodium, nickel, cobalt, copper and copperchromium. A carrier, e.g. carbon, alumina or diatomaceous earth may be used. The product is obtained by separating the product and catalyst, e.g. by filtration, from the aqueous liquor, dissolving the product in a solvent to remove the catalyst and then diluting or cooling the solution to precipitate the product.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14249473A JPS56421B2 (en) | 1973-12-21 | 1973-12-21 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1471490A true GB1471490A (en) | 1977-04-27 |
Family
ID=15316620
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB5426374A Expired GB1471490A (en) | 1973-12-21 | 1974-12-16 | Method for the preparation of 1-amino-anthraquinone |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS56421B2 (en) |
| BE (1) | BE823534A (en) |
| CH (1) | CH603747A5 (en) |
| FR (1) | FR2255291B1 (en) |
| GB (1) | GB1471490A (en) |
| IT (1) | IT1027922B (en) |
| NL (1) | NL170729C (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102658129A (en) * | 2012-05-07 | 2012-09-12 | 南京工业大学 | Catalyst for preparing 1-aminoanthraquinone through hydrogenization, and preparation method and application of catalyst |
| CN113769747A (en) * | 2021-08-31 | 2021-12-10 | 浙江工业大学 | Application of carbon material coated nickel nanoparticle catalyst in 1-nitroanthraquinone hydrogenation synthesis of 1-aminoanthraquinone |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5446767A (en) * | 1977-09-22 | 1979-04-12 | Mitsui Toatsu Chem Inc | Preparation of high-purity 1-aminoanthraquinone |
| JPH0644984U (en) * | 1992-11-13 | 1994-06-14 | 武盛 豊永 | Simple solarium |
| CN108295850B (en) * | 2018-01-22 | 2020-10-02 | 江苏欣诺科催化剂有限公司 | Catalyst for preparing aminoanthraquinone and catalytic method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5717897B2 (en) * | 1973-09-25 | 1982-04-13 |
-
1973
- 1973-12-21 JP JP14249473A patent/JPS56421B2/ja not_active Expired
-
1974
- 1974-12-16 GB GB5426374A patent/GB1471490A/en not_active Expired
- 1974-12-18 BE BE151662A patent/BE823534A/en not_active IP Right Cessation
- 1974-12-20 IT IT3086974A patent/IT1027922B/en active
- 1974-12-20 CH CH1714674A patent/CH603747A5/xx not_active IP Right Cessation
- 1974-12-20 NL NL7416714A patent/NL170729C/en not_active IP Right Cessation
- 1974-12-23 FR FR7442543A patent/FR2255291B1/fr not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102658129A (en) * | 2012-05-07 | 2012-09-12 | 南京工业大学 | Catalyst for preparing 1-aminoanthraquinone through hydrogenization, and preparation method and application of catalyst |
| CN102658129B (en) * | 2012-05-07 | 2014-06-25 | 南京工业大学 | Catalyst for preparing 1-aminoanthraquinone through hydrogenization, and preparation method and application of catalyst |
| CN113769747A (en) * | 2021-08-31 | 2021-12-10 | 浙江工业大学 | Application of carbon material coated nickel nanoparticle catalyst in 1-nitroanthraquinone hydrogenation synthesis of 1-aminoanthraquinone |
Also Published As
| Publication number | Publication date |
|---|---|
| NL170729C (en) | 1982-12-16 |
| BE823534A (en) | 1975-04-16 |
| IT1027922B (en) | 1978-12-20 |
| NL170729B (en) | 1982-07-16 |
| NL7416714A (en) | 1975-06-24 |
| DE2460687B2 (en) | 1977-03-31 |
| DE2460687A1 (en) | 1975-07-03 |
| FR2255291A1 (en) | 1975-07-18 |
| JPS56421B2 (en) | 1981-01-08 |
| JPS5093959A (en) | 1975-07-26 |
| FR2255291B1 (en) | 1979-06-01 |
| CH603747A5 (en) | 1978-08-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 19921216 |