HRP931057A2 - Process and apparatus for dynamic-flow production of ductile, highly tear-resistant fiber mats - Google Patents
Process and apparatus for dynamic-flow production of ductile, highly tear-resistant fiber mats Download PDFInfo
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- HRP931057A2 HRP931057A2 HR931057A HRP931057A HRP931057A2 HR P931057 A2 HRP931057 A2 HR P931057A2 HR 931057 A HR931057 A HR 931057A HR P931057 A HRP931057 A HR P931057A HR P931057 A2 HRP931057 A2 HR P931057A2
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- 239000000835 fiber Substances 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 238000003825 pressing Methods 0.000 claims abstract description 13
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 10
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract description 10
- 229920003043 Cellulose fiber Polymers 0.000 claims abstract description 9
- 239000011230 binding agent Substances 0.000 claims abstract description 7
- 238000005520 cutting process Methods 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 5
- 238000009826 distribution Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 230000005520 electrodynamics Effects 0.000 claims 1
- 230000001105 regulatory effect Effects 0.000 claims 1
- 235000013311 vegetables Nutrition 0.000 abstract description 2
- 241000196324 Embryophyta Species 0.000 description 10
- 238000005259 measurement Methods 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 240000000491 Corchorus aestuans Species 0.000 description 1
- 235000011777 Corchorus aestuans Nutrition 0.000 description 1
- 235000010862 Corchorus capsularis Nutrition 0.000 description 1
- 229920000965 Duroplast Polymers 0.000 description 1
- 239000004638 Duroplast Substances 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 229920002522 Wood fibre Polymers 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 210000002808 connective tissue Anatomy 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002025 wood fiber Substances 0.000 description 1
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- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
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- D04H1/72—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
- D04H1/732—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by fluid current, e.g. air-lay
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- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
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- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
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- D04H1/4209—Inorganic fibres
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- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4326—Condensation or reaction polymers
- D04H1/4334—Polyamides
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- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
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- D04H1/4326—Condensation or reaction polymers
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- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
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- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
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- D04H1/645—Impregnation followed by a solidification process
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- D04H18/00—Needling machines
- D04H18/02—Needling machines with needles
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Nonwoven Fabrics (AREA)
- Inorganic Fibers (AREA)
- Preliminary Treatment Of Fibers (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Dry Formation Of Fiberboard And The Like (AREA)
- Folding Of Thin Sheet-Like Materials, Special Discharging Devices, And Others (AREA)
- Laminated Bodies (AREA)
- Paper (AREA)
Description
Izum se odnosi na postupak strujno dinamičke proizvodnje vlaknastih hasura promjenjivog oblika, visoke čvrstoće trganja iz vlaknastog runa, koje se sastoji i, sa veznim sredstvom impregniranih vlakana celuloze i termoplastičnih vlakana i/ili prirodnih vlakana biljnog porijekla pri čemu se grumen od vlaknastog runa miješa u bačvastom spremniku i iz te mješavine se formira vlaknasto runo, koje se sa igličastim strojem učvršćuje u vlaknastu hasuru. Izum se odnosi dalje na primjeru ovim postupkom proizvedene hasure kao i postrojenja za provedbu ovoga postupka.
Postupak spomenute vrste poznat je iz AT-PS 387.798. Prema prednostima ovog poznatog postupka miješa se vlaknasto runo u bačvastom spremniku i iz te mješavine stvaraju se npr. sljedeća runa na jednom bubnju za polaganje runa. kod toga se pokazalo, da transport razvlaknjene vlaknaste mase proizlazi besciljno od valjka bačvastog spremnika od bubnja za polaganje runa, pri čemu dolazi do nepravilnosti vlaknastog grumena na bubnju za polaganje runa kao što su nepravilno raspoređivanje površinske težine po širini vlaknastog runa. Dalje se kod toga uočava, da kod drvenih vlakana impregniranih sa umjetnom smolama uglavnom dolazi radi njihove velike težine do nalijeganja donje strane runa koje se polaže, dok se istovremeno termoplastična i/ili neimpregnirana prirodna vlakna biljnog porijekla raspoređuju u gornjim slojevima runa koje se polaže. Ova različita slojevitost vodi s time do problema kod daljnje obrade ovih hasura, budući da je donja strana hasura radi njenog previsokog dijela veznih sredstava ljepljiva, dok gornja strana gotovo uopće nije zalijepljena.
Postavljeni zadatak u ovom izumu se sastoji međutim od toga, da jedna hasura promjenjivog oblika visoke čvrstoće trganja treba posjedovati ravnomjernu težinsku raspoređenost po njenoj širini kao i po njenim slojevima, koja se sastoji iz ravnomjerno izmiješanih vlakana impregnirane i neimpregnirane vrste.
Ovaj zadatak se rješava postupkom prema izumu na taj način, da se runski grume 2,2’ dovodi bačvastom spremniku 6,6’ u kojem se grumen od vlaknastog runa razvlakni i da se na taj način nastala vlaknasta masa 14,14’ miješa strujom zraka čiji profil nastrujavanja se uspostavlja kroz jedan zračni kanal 10,10’ i u njemu primijenjene elemente za regulaciju 25, 26 kao i preko jedne u smjeru strujanja priključene venturi poluge 7,7’, pri čemu se stvara runo 18,18’ sa jednim ravnomjernim rasporedom površinske težine, koja se nakon izvršenog igličanja dovodi tlačnoj napravi 21,21’ pri čemu se proizvode hasure promjenjivog oblika i visoke čvrstoće trganja 23,23’.
Postupa u svezi sa izumom je nadalje naznačen time, da se elementi za regulaciju sastoje iz više, preko širine zračnog kanala 10 raspoređenih klapni 25 i iz više prema zračnoj struji konveksno zakrivljenih dijelova za regulaciju 26 čija se zaobljenost može namještati.
Izum se odnosi nadalje na prednosti primjene hasure proizvedenih prema izumu, koje je naznačeno time, da se primjenjuju jedna ili više hasura 23,23’ primjenjuju za proizvodnju određenih oblika prešanjem pod povišenim tlakom i temperaturom.
Izum se odnosi također na jedno postrojenje sa prednostima za strujno dinamičku proizvodnju hasura promjenjivog oblika i visoke čvrstoće trganja iz vlaknastog runa, koje se sastoji iz, sa vezivnim sredstvom impregniranih celuloznih vlakana i termoplastičnih vlakana i/ili prirodnih vlakana biljnog porijekla, koje je naznačeno time, da se postrojenje sastoji, prema protoku materijala jedan a drugim poredanih od stroja za polaganje runa 1, para valjaka za prešanje 3, 4, para valjaka za uvlačenje 5, bačvastog spremnika 6, zračnog kanala 10, koji se napaja ventilatorima 12 i u kojemu su pridodani jedan ili više dijelova za regulaciju 25 u obliku jedne ili više klapni za regulaciju, venturi poluge 7, difuzora 13, bubnja za polaganje runa 15, valjaka za transport 16, 17, mjerne naprave za izmjeru površinske težine 19, igličastog stroja 20, preše 21, stroja za rezanje 22, i naprave za odlaganje 24.
Nadalje se izum odnosi na jedno postrojenje sa prednostima za strujno dinamičku proizvodnju hasura promjenjivog oblika, visoke čvrstoće trganja iz vlaknastog runa koje se sastoji iz, sa veznim sredstvom impregniranih vlakana celuloze i termoplastičnih vlakana i/ili prirodnih vlakana biljnog porijekla pri čemu je postrojenje naznačeno time da se ono sastoji, prema protoku materijala jedan za drugim poredanih, od stroja za polaganje runa 1’, para valjaka za prešanje 3’, 4’, para valjaka za uvlačenje 5’, bačvastog spremnika 6’, kanala za zrak 10’, koji se napaja ventilatorima 12’ u kojima su postavljeni jedan ili više elemenata za regulaciju 26, koji su prema struji zraka konveksno zakrivljeni i čija se zakrivljenost može namještati, venturi poluge 7’, difuzora 13’, bubnja za polaganje runa 15’, valjaka za transport 16’, 17’, mjerne naprave za izmjeru površinske težine 19’, igličastog stroja 20’, preše 21’, stroja za rezanje 22’ i naprave za odlaganje 24’.
Slika 1 prikazuje izvedbu postupka prema izumu s pomoću postrojenja koje sadrži dijelove za regulaciju u obliku pomičnih klapni.
Slika 2 pokazuje izvedbu postupka prema izumu s pomoću postrojenja naznačenog crtkano na odgovarajućem crtežu, koja sadrži konveksno savinute dijelove za regulaciju u zračnoj struji.
Slike 3 i 4 pokazuju u perspektivi principijelni prikaz venturi poluge sa shematskim protokom zračne struje postavljene kao dio za regulaciju u postupku.
Strojem za proizvodnju runa (1,1’) se iz jedne smjese koja se sastoji iz npr. sa veznim tkivom poput duroplasta, termoplasta ili elastomera ili mješavina iz toga impregniranih i nakon toga osušenih vlakana celuloze, i termoplastičnih vlakana npr. poliester-, poliolefin-, poliamid-, poliakril- EVA- i/ili prirodna vlakna kao lanena-, kudeljina- i celulozna vlakna, stvara runski grumen (2,2’). Ovaj se nadalje zgušnjava preko valjaka za prešanje (3,3’, 3,3’) i s pomoću jednog para valjaka za uvlačenje (5,5’), se dovodi bačvastom spremniku (6,6’), čije površina je obložena sa iglama ili reznim zupčanicima koji razvlaknjuju runasti grumen. Prema broju preko iste osovine zagonjenih ventilatora 12,12’ se u kanalu zrak 10,10’ stvara zračna struja, čija brzina strujanja se uspostavlja kroz više raspoređenih dijelova za regulaciju 25, 26 (vidi sliku 2) preko širine kanala za zrak u obliku klapni za namještanje. Dijelovi za regulaciju 25 (vidi sliku 1) su prema struji zraka konveksno zakrivljeni i njihova se zakrivljenost može namještati.
Miješanje vlakana u struji zraka je nadalje ovisno o brzini strujanja. Ovo miješanje se pojačava zakretanjem venturi poluge 7,7’ za približno + 30° oko njene osi, koja po njenoj širini ukazuje varirajuće prepreke 8,8’. U međuprostorima 9,9’ (vidi sliku 3 i 4) između prepreka 8,8’ povećava se prema veličini međuprostora brzina strujanja smjese zrak-vlakna, čime slijedi dodatno miješanje vlakana u priključenom difuzoru 13,13’. Nadalje takova brzina strujanja proizvodi jedan učinak lopatica koji omogućuje pravilno rasprostranjivanje runa vlakana 14,14’ na bubanj za proizvodnju runa 15,15’. Na takav način novostvoreno runo 18,18’ se dovodi preko valjaka za transport 16,16’ i 17,17’ napravi za mjerenje površinske težine 19,19’. Ove izmjere ukazuju na pravilnu raspodjelu površinske težine kao i rezultat mjerenja, koji se može potiči poznatim postupkom stvaranja runa. Bude li usprkos toga raspored površinske težine nedovoljno dobar, moguće ga je promjenom brzine strujanja namještanjem jednog ili više dijelova za regulaciju 25, 26 promijeniti. Nadalje je preko mogućnosti namještanja venturi poluge 7,7’ dana daljnja mogućnost optimiranja strujnih odnosa.
U igličastoj mašini 20,20’ koja slijedi u aparaturi, isprepleće se runo 18,18’ sa jednim drugim runom 27,27’, npr. koje se sastoji iz poliester-, poliamid-, staklasta vlakna ili jute, čime se stvara jedna hasura 28,28’ dovoljno dobrog promjenjivog oblika. Da bi se postigla još bolja promjenjivost oblika ove hasure kod daljnje prerade u prešama za formiranje, ona se vodi kroz napravu za prešanje 21,21’, koja može biti npr. roljača ili trakasta preša. Između valjaka roljače se predzgušnjava hasura na temperaturi od 25°C do 150°C i specifičnom tlaku od 5 do 50 kp/cm2 pri čemu se drvena vlakna impregnirana sa umjetnim smolama još jače vežu na dodatna vlakna. Na taj način može hasura kod daljnje obrade npr. kod prešanja u forme preuzeti još veće vlačne sile i stoga je manje podložna stvaranju riseva.
Dodatno se pretzgušnjena hasura 24,24’ odlaže nakon prolaza stroja za rezanje 22,22’ na napravu za odlaganje 23,23’.
Claims (6)
1. Postupak za strujno dinamičku proizvodnju hasura promjenjivog oblika visoke čvrstoće trganja iz vlaknastoga runa, koje se sastoji iz sa veznim sredstvom impregniranih vlakna celuloze i termoplastičkih vlakna i/ili prirodnih vlakna biljnog porijekla pri čemu se grumen od vlaknastog runa miješa u jednom bačvastom spremniku i iz te mješavine se formira vlaknasto runo, koje se na igličastom stroju učvršćuje u hasuru, naznačen time, da se grumen od vlaknastog runa 2,2' dovodi bačvastom spremniku 6,6' u kome se grumen od vlaknastog runa razvlakni, i da se na taj način nastala vlaknasta masa 14,14' miješa jednom zračnom strujom čiji strujni profil se postavlja regulacionim elementima 25, 26 umetnutim u zračnom kanalu 10,10' kao i preko dodatne venturi šipke 7,7* u smjeru strujanja, pri čemu se stvara runo 18,18' sa ravnomjernim rasporedom površinske težine, koje se dovodi nakon izvršenog propikavanja na napravu za prešanje 21,21' pri čemu se stvara hasura promjenjivog oblika i visoke čvrstoće trganja 23,23'.
2. Postupak prema zahtjevu 1, naznačen time, da se elementi za regulaciju sastoje iz više klapni 25 za namještanje raspoređenih preko širine kanala za zrak 10.
3. Postupak prema zahtjevu 1, naznačen time, da se elementi za regulaciju sastoje iz više dijelova za regulaciju koji su konveksno zakrivljeni prema struji zraka, a sastoje se iz dijelova za regulaciju 26, koji se mogu namještati u zavojima.
4. Primjena prema zahtjevu 1 načinjene hasure promjenjivog oblika i visoke čvrstoće trganja, naznačena time, da se jedna ili više hasura 23,23'primjenjuju za proizvodnju određenih oblika prešanjem pod povišenim tlakom i povišenom temperaturom.
5. Postrojenje za strujno dinamičko dobivanje hasura promjenjivog oblika visoke čvrstoće trganja iz vlaknastog runa, koje se sastoji iz, sa veznim sredstvom impregniranih vlakna celuloze i termoplastičnih vlakana i/ili prirodnih vlakna biljnog porijekla, naznačen time, da se postrojenje sastoji glede protoka materijala jedan za drugim položenih iz stroja za proizvodnju runa 1, para valjaka za prešanje 3,4, para valjaka za uvlačenje 5, bačvastoga spremnika 6, zračnog kanala 10, koji se puni ventilatorima 12 i u kojem se nalaze jedan ili više dijelova za regulaciju 25 u formi jedne ili više klapa za namještanje, venturi poluge 7, difuzora 13, bubnja za proizvodnju runa 15, valjaka za transport 16, 17, mjerne opreme za mjerenje površinske težine 19, igličastog stroja 20, naprave za prešanje 21, stroja za rezanje 22 i naprave za odlaganje 24.
6. Postrojenje za strujno dinamičku proizvodnju hasura promjenjivog oblika visoke čvrstoće trganja iz vlaknastog runa koje se sastoji iz, sa veznim sredstvom impregniranih vlakna celuloze i termoplastičnih vlakna ili prirodnih vlakna biljnog porijekla, naznačen time, da se postrojenje sastoji iz, s obzirom na smjer protoka materijala jedan za drugim poredanih, stroja za proizvodnju runa I1, para valjaka za prešanje 31, 41, para valjaka za uvlačenje 5', bačvastog spremnika 6', zračnog kanala 10', koji se puni ventilatorima 12', u kojima su smješteni jedan ili više elemenata za regulaciju 26 sa konveksno prema struji zraka zakrivljenom formom i promjenjivom zakrivljenošću zavoja, venturi poluge 7, difuzora 13', bubnja za proizvodnju runa 15', valjaka za transport 16', 17, mjerne opreme za mjerenje površinske težine 19', igličastog stroja 20', naprave za prešanje 21', stroja za rezanje 22' i naprave za odlaganje 24'.
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AT0147092A AT398438B (de) | 1992-07-17 | 1992-07-17 | Verfahren zur strömungsdynamischen herstellung von verformbaren fasermatten hoher reissfestigkeit sowie vorrichtung zu deren herstellung |
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HRP931057A2 true HRP931057A2 (en) | 1995-10-31 |
HRP931057B1 HRP931057B1 (en) | 1999-04-30 |
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HRA1470/92A HRP931057B1 (en) | 1992-07-17 | 1993-07-16 | Process and apparatus for dynamic-flow production of ductile, highly tear-resistant fiber mats |
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EP (1) | EP0605687B1 (hr) |
JP (1) | JP3178840B2 (hr) |
KR (1) | KR100296021B1 (hr) |
AT (2) | AT398438B (hr) |
CZ (1) | CZ283384B6 (hr) |
DE (1) | DE59303438D1 (hr) |
ES (1) | ES2092315T3 (hr) |
HR (1) | HRP931057B1 (hr) |
HU (1) | HU216949B (hr) |
MX (1) | MX9304337A (hr) |
SI (1) | SI9300389A (hr) |
WO (1) | WO1994002673A1 (hr) |
ZA (1) | ZA935095B (hr) |
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US5778494A (en) * | 1995-12-08 | 1998-07-14 | E. I. Du Pont De Nemours And Company | Method and apparatus for improving the air flow through an air duct in a dry fiber web forming system |
DE10038405C1 (de) * | 2000-08-07 | 2002-05-02 | Moeller Plast Gmbh | Verfahren zum Herstellen von thermoplastisch gebundenem Naturfasermaterial |
JP4515196B2 (ja) * | 2004-08-25 | 2010-07-28 | 株式会社リブドゥコーポレーション | パルプ粉砕装置 |
AT502643B1 (de) * | 2005-11-02 | 2007-05-15 | Angleitner Helmut Dipl Ing | Einrichtung zum ablagern von in einem gasstrom transportierbaren fasern |
GB2452235A (en) * | 2007-03-05 | 2009-03-04 | Eco Mats Ltd | Plant fibre mat and method of making a plant fibre mat |
KR102327955B1 (ko) * | 2011-09-30 | 2021-11-17 | 오웬스 코닝 인텔렉츄얼 캐피탈 엘엘씨 | 섬유질 재료들로부터 웹을 형성하는 방법 |
JP6421316B2 (ja) * | 2014-03-11 | 2018-11-14 | セイコーエプソン株式会社 | シート製造装置、シート製造方法及びこれらに用いる粉体 |
DE102016009679A1 (de) * | 2016-08-10 | 2018-02-15 | Hubert Hergeth | Vliesbildemaschine |
CN108754875A (zh) * | 2018-08-28 | 2018-11-06 | 仪征市佳禾机械有限公司 | 广谱气流成网机 |
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FR1399062A (fr) * | 1964-06-11 | 1965-05-14 | Feutres non tissés avec charges minérales incorporées et leur procédé de fabrication | |
US3768119A (en) * | 1970-12-31 | 1973-10-30 | Curlator Corp | Machine for forming random fiber webs |
SE7406956L (hr) * | 1973-06-15 | 1974-12-16 | Morrison Machine Co | |
US3918126A (en) * | 1974-07-12 | 1975-11-11 | Rando Machine Corp | Method and machine for forming random fiber webs |
ES2034957T3 (es) * | 1985-12-10 | 1993-04-16 | Kimberly-Clark Corporation | Aparato y metodo para la conformacion de generos laminares fibrosos. |
AT387798B (de) * | 1987-12-11 | 1989-03-10 | Kuehnsdorfer Gmbh | Verfahren zur herstellung einer lagerfaehigen, handhabbaren fasermatte und nach dem verfahren hergestellte fasermatte |
DE3901313A1 (de) * | 1989-01-18 | 1990-07-19 | Hollingsworth Gmbh | Vlieskrempel |
DE3903946A1 (de) * | 1989-02-10 | 1990-08-16 | Vepa Ag | Verfahren und vorrichtung zur herstellung eines vlieses aus stapelfasern und zellulose |
IT1232802B (it) * | 1989-04-06 | 1992-03-05 | Claudio Governale | Dispositivo per la formazione di strutture fibrose nontessute. |
CH681990A5 (hr) * | 1989-04-14 | 1993-06-30 | Matec Holding | |
JPH0715333B2 (ja) * | 1989-05-25 | 1995-02-22 | 株式会社朝日工業社 | 風量制御装置 |
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1992
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- 1993-07-15 WO PCT/AT1993/000120 patent/WO1994002673A1/de active IP Right Grant
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Also Published As
Publication number | Publication date |
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ATE141346T1 (de) | 1996-08-15 |
HUT68090A (en) | 1995-05-29 |
WO1994002673A1 (de) | 1994-02-03 |
ATA147092A (de) | 1994-04-15 |
EP0605687A1 (de) | 1994-07-13 |
CZ283384B6 (cs) | 1998-04-15 |
HRP931057B1 (en) | 1999-04-30 |
SI9300389A (en) | 1994-03-31 |
CZ62694A3 (en) | 1994-06-15 |
KR940702236A (ko) | 1994-07-28 |
HU9400763D0 (en) | 1994-06-28 |
ES2092315T3 (es) | 1996-11-16 |
HU216949B (hu) | 1999-10-28 |
JP3178840B2 (ja) | 2001-06-25 |
EP0605687B1 (de) | 1996-08-14 |
ZA935095B (en) | 1994-06-01 |
DE59303438D1 (de) | 1996-09-19 |
JPH06511294A (ja) | 1994-12-15 |
MX9304337A (es) | 1994-04-29 |
KR100296021B1 (ko) | 2001-10-24 |
AT398438B (de) | 1994-12-27 |
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