HRP20230965T1 - Novi uzorak kanala prikupljanja i distribucije za simulirani postupak odvajanja pokretnog sloja upotrebom n stupaca u nizu - Google Patents

Novi uzorak kanala prikupljanja i distribucije za simulirani postupak odvajanja pokretnog sloja upotrebom n stupaca u nizu Download PDF

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Publication number
HRP20230965T1
HRP20230965T1 HRP20230965TT HRP20230965T HRP20230965T1 HR P20230965 T1 HRP20230965 T1 HR P20230965T1 HR P20230965T T HRP20230965T T HR P20230965TT HR P20230965 T HRP20230965 T HR P20230965T HR P20230965 T1 HRP20230965 T1 HR P20230965T1
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Croatia
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column
channel
fluid
collection
wall
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HRP20230965TT
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English (en)
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Frederic Augier
Aude ROYON-LEBEAUD
Damien Leinekugel Le Cocq
Alexandre VONNER
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IFP Energies Nouvelles
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Publication of HRP20230965T1 publication Critical patent/HRP20230965T1/hr

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/1842—Simulated moving beds characterized by apparatus features
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterized by the components to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/22—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the construction of the column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/085—Feeding reactive fluids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02—Monocyclic hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6004—Construction of the column end pieces
    • G01N30/6017—Fluid distributors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/24—Hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702—Hydrocarbons
    • B01D2257/7027—Aromatic hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00884—Means for supporting the bed of particles, e.g. grids, bars, perforated plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00893—Feeding means for the reactants
    • B01J2208/00902—Nozzle-type feeding elements

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Threshing Machine Elements (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Combinations Of Kitchen Furniture (AREA)
  • Invalid Beds And Related Equipment (AREA)

Claims (7)

1. Uređaj za distribuciju ili prikupljanje tekućine unutar granuliranog sloja (6) koji se nalazi u koloni namijenjenoj za provođenje odvajanja u mnoštvo komponenti u kojem: - distribucija ulaznog fluida se vrši pomoću distribucijskog kanala (3) promjenjivog poprečnog presjeka u kojem fluid struji konstantnom brzinom Vcanal između 0,1 i 5 m/s; - skupljanje izlaznog fluida vrši se sabirnim kanalom (8) promjenjivog poprečnog presjeka u kojem fluid struji konstantnom brzinom Vcanal; - pri čemu kolona je kolona s aksijalnim protokom, • visina hsup(r) distribucijskog kanala (3) definirana između granuliranog sloja (6) i stijenke (4) distribucijskog kanala (3), slijedeći radijalnu koordinatu r, prati sljedeći profil: [image] • visina hinf(r) sabirnog kanala (8) definirana od druge rešetke (7) postavljene između granuliranog sloja (6) i stijenke (9) sabirnog kanala (8), slijedeći radijalnu koordinatu r, prati sljedeći profil: [image] • gdje je VSL površinska brzina fluida u granuliranom sloju (6) definirana kao omjer brzine volumenskog protoka i poprečnog presjeka kolone, R je polumjer kolone; ili - pri čemu kolona je kolona s radijalnim protokom, • radijalni položaj rdistrib(z) stijenke (4) distribucijskog kanala (3) računajući od osi kolone, prateći aksijalnu koordinatu z, prati sljedeći profil: [image] • sabirni kanal (8) omeđen stjenkom (9) prati radijalni profil profile rcollecte(z) koji se računa od osi kolone kao funkcija aksijalne koordinate z u skladu s formulom: [image] • gdje je VSL površinska brzina fluida u granuliranom sloju (6) definirana kao omjer brzine volumenskog protoka i poprečnog presjeka kolone, Hlit je ukupna visina kolone, z je aksijalna koordinata računata od ulaz fluida u kolonu, rdistrib(0) je radijalni položaj koji se računa od osi kolone gdje je z jednako 0, i Elit je debljina sloja definirana u radijalnom smjeru.
2. Postupak simuliranog pokretnog sloja koji koristi uređaj za prikupljanje prema zahtjevu 1, naznačen time što je cirkulacija tekućine unutar sloja granulirane krutine aksijalna, a ubrizgavanje u sloj se vrši pomoću kanala (2) koji je uglavnom centriran na okomitoj osi kolone, koja opskrbljuje vodoravni distribucijski kanal (3) omeđen stjenkom (4) distribucijskog kanala (3), sloj granulirane krutine (6) se zatim dovodi iz navedenog distribucijskog kanala (3) kroz prvu rešetku (5), a fluid struju kroz granulirani sloj (6) u uglavnom okomitom smjeru, fluid se tada sakuplja ispod druge rešetke (7) iz sabirnog kanala (8) omeđenog zakrivljenom stjenkom (9) sabirnog kanala (8) putem perifernih kanala (10), a sav protok se skuplja u jednom ispusnom kanalu (11) koji je uglavnom centriran na okomitoj osi kolone.
3. Postupak simuliranog odvajanja pokretnog sloja korištenjem uređaja za prikupljanje prema zahtjevu 1, naznačen time što se cirkulacija fluida unutar sloja granulirane krutine vrši na radijalan način, te se fluid uvodi u središte kolone putem kanala (2) koji opskrbljuje distribucijski kanal (3) omeđen u središtu stjenkom (4) distribucijskog kanala (3), te zatim prolazi kroz granulirani sloj (6) od središta granularnog sloja (6) omeđenog prvom rešetkom (5) prema obodu granuliranog sloja (6) omeđenog drugom rešetkom (7) gdje se tekućina sakuplja u sabirnom kanalu (8) definiranom izvana stijenkom (9) sabirnog kanala (8), koji vraća tekućinu preko perifernih kanala (10) prema ispusnom kanalu (11) koji je uglavnom centriran na osi kolone.
4. Postupak simuliranog odvajanja pokretnog sloja korištenjem uređaja prema zahtjevu 1, naznačen time što je sirovina koja se odvaja bilo koja smjesa aromatskih spojeva koji imaju od 7 do 9 atoma ugljika.
5. Postupak simuliranog odvajanja pokretnog sloja korištenjem uređaja prema zahtjevu 1, naznačen time što je sirovina koja se odvaja smjesa normalnih i izo-parafina.
6. Postupak simuliranog odvajanja pokretnog sloja korištenjem uređaja prema zahtjevu 1, naznačen time što je sirovina koja se odvaja smjesa normalnih i izo-olefina.
7. Postupak simuliranog odvajanja pokretnog sloja korištenjem uređaja prema zahtjevu 1, naznačen time što glavni fluid koji prolazi kroz navedeni uređaj ima gustoću između 600 i 950 kg/m3 i viskoznost između 0,1 i 0,6 cPo.
HRP20230965TT 2017-04-12 2018-04-05 Novi uzorak kanala prikupljanja i distribucije za simulirani postupak odvajanja pokretnog sloja upotrebom n stupaca u nizu HRP20230965T1 (hr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1753216A FR3065173B1 (fr) 2017-04-12 2017-04-12 Nouveau dessin des canaux de collecte et de distribution pour un procede de separation en lit mobile simule utilisant n-colonnes en serie
EP18165968.1A EP3388128B1 (fr) 2017-04-12 2018-04-05 Nouveau dessin des canaux de collecte et de distribution pour un procede de separation en lit mobile simule utilisant n-colonnes en serie

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HRP20230965T1 true HRP20230965T1 (hr) 2023-12-08

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US (1) US20180296941A1 (hr)
EP (1) EP3388128B1 (hr)
JP (1) JP7117129B2 (hr)
KR (1) KR102501564B1 (hr)
CN (1) CN108686590A (hr)
ES (1) ES2954315T3 (hr)
FR (1) FR3065173B1 (hr)
HR (1) HRP20230965T1 (hr)
PL (1) PL3388128T3 (hr)
PT (1) PT3388128T (hr)

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FR3072885B1 (fr) * 2017-10-27 2019-11-15 IFP Energies Nouvelles Nouveau systeme de distribution par panneaux meridiens pour un procede de separation en lit mobile simule utilisant n-colonnes en serie
CN109432822B (zh) 2018-11-14 2023-09-29 内蒙古伊泰煤基新材料研究院有限公司 一种高效模拟移动床设备以及高效模拟移动床工艺

Family Cites Families (14)

* Cited by examiner, † Cited by third party
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JP2002504227A (ja) 1997-03-12 2002-02-05 メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフトング クロマトグラフィーカラムの末端部材
WO1999062609A1 (en) * 1998-06-01 1999-12-09 Wisconsin Alumni Research Foundation Fluid flow distributor
EP1154828A1 (en) * 1999-02-25 2001-11-21 Pall Corporation Chromatography devices and flow distributor arrangements used in chromatography devices
GB0111486D0 (en) 2001-05-11 2001-07-04 Amersham Pharm Biotech Ab Scalable inlet liquid distribution system for large scale chromatography columns
BE1015976A3 (fr) * 2004-04-14 2005-12-06 Broqueville Axel De Procede de polymerisation cataltytique dans un lit fluidifie vertical rotatif.
FR2930454B1 (fr) * 2008-04-25 2010-11-19 Inst Francais Du Petrole Systeme de distribution et de collecte des fluides dans une colonne multietagee
US20090321338A1 (en) * 2008-06-25 2009-12-31 Millipore Corporation Chromatography apparatus
FR2933000B1 (fr) * 2008-06-27 2011-03-18 Inst Francais Du Petrole Nouveau systeme de distribution et de collecte dans une colonne multi etagee permettant d'egaliser les temps de sejour sur chaque etage
FR2932999B1 (fr) * 2008-06-27 2011-03-18 Inst Francais Du Petrole Nouveau systeme de distribution et de collecte des fluides dans une colonne multi etagee comportant un brise jet
US8043578B2 (en) * 2009-02-18 2011-10-25 Uop Llc Flexible pressure containing shaped coverplate configuration
EP2583093B1 (en) * 2010-06-15 2016-05-11 GE Healthcare Bio-Sciences AB Fluid distributor unit
US20150057480A1 (en) 2013-08-22 2015-02-26 Uop Llc Radial Flow Process and Apparatus
US9302953B2 (en) * 2014-06-30 2016-04-05 Exxonmobil Chemicals Patents Inc. Process for the production of xylenes
US9611194B2 (en) 2014-08-15 2017-04-04 Uop Llc Simulated moving bed separators and methods for isolating a desired component

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Publication number Publication date
KR102501564B1 (ko) 2023-02-17
FR3065173B1 (fr) 2020-06-26
US20180296941A1 (en) 2018-10-18
ES2954315T3 (es) 2023-11-21
PT3388128T (pt) 2023-08-23
CN108686590A (zh) 2018-10-23
KR20180115232A (ko) 2018-10-22
EP3388128A1 (fr) 2018-10-17
PL3388128T3 (pl) 2023-11-13
FR3065173A1 (fr) 2018-10-19
JP2019000842A (ja) 2019-01-10
EP3388128B1 (fr) 2023-06-07
JP7117129B2 (ja) 2022-08-12

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