GB978795A - Improvements in or relating to distillation of metal solutions - Google Patents

Improvements in or relating to distillation of metal solutions

Info

Publication number
GB978795A
GB978795A GB3960562A GB3960562A GB978795A GB 978795 A GB978795 A GB 978795A GB 3960562 A GB3960562 A GB 3960562A GB 3960562 A GB3960562 A GB 3960562A GB 978795 A GB978795 A GB 978795A
Authority
GB
United Kingdom
Prior art keywords
still
calcium
solution
line
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3960562A
Inventor
Jan Zbigniew Lang
Allan Robert Gibson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Elgar Trading Ltd
UK Atomic Energy Authority
Original Assignee
Elgar Trading Ltd
UK Atomic Energy Authority
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Elgar Trading Ltd, UK Atomic Energy Authority filed Critical Elgar Trading Ltd
Priority to GB3960562A priority Critical patent/GB978795A/en
Publication of GB978795A publication Critical patent/GB978795A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00General methods of reducing to metals
    • C22B5/02Dry methods smelting of sulfides or formation of mattes
    • C22B5/16Dry methods smelting of sulfides or formation of mattes with volatilisation or condensation of the metal being produced

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

<PICT:0978795/C6-C7/1> In a process for recovering a light metal (e.g. calcium, sodium or cadmium) from a liquid solution containing the light metal and a heavy metal (e.g. copper, lead, uranium or thorium) by distillation in a still 5, maintained under vacuum by line 10, the solution is drawn up into the still via line 4 owing to the difference in pressure between the supply vessel and the still; the light metal evaporates from the solution and condenses on condenser 6, and the depleted solution flows out of the still via line 3 owing to the difference in pressure between the still and the receiver. In an example, calcium sulphide is electrolysed in cell 1 using molten copper-calcium alloy as cathode, whereby the calcium, produced by electrolysis, dissolves in the molten alloy to form a solution of calcium in copper which is drawn up line 4 into still 5. The still is heated, preferably electrically, to a temperature of 800-850 DEG C. When the cell 1 is at atmospheric pressure and the still is operated at a pressure of 5-0.1 mm. Hg., pipes 3 and 4 are 3 metres and 3.5 metres long, respectively. Condenser 6 is cooled by gas, introduced through line 7. When a sufficient quantity of calcium has collected on the condenser, the vacuum in the still is broken by admitting argon via valve 12, so that all the solution in the still drops down pipes 3 and 4 into cell 1.
GB3960562A 1961-10-25 1961-10-25 Improvements in or relating to distillation of metal solutions Expired GB978795A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB3960562A GB978795A (en) 1961-10-25 1961-10-25 Improvements in or relating to distillation of metal solutions

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3960562A GB978795A (en) 1961-10-25 1961-10-25 Improvements in or relating to distillation of metal solutions

Publications (1)

Publication Number Publication Date
GB978795A true GB978795A (en) 1964-12-23

Family

ID=10410473

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3960562A Expired GB978795A (en) 1961-10-25 1961-10-25 Improvements in or relating to distillation of metal solutions

Country Status (1)

Country Link
GB (1) GB978795A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112875960A (en) * 2021-01-25 2021-06-01 吕梁学院 Industrial waste water heavy metal extraction element

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112875960A (en) * 2021-01-25 2021-06-01 吕梁学院 Industrial waste water heavy metal extraction element
CN112875960B (en) * 2021-01-25 2022-12-02 吕梁学院 Industrial waste water heavy metal extraction element

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