GB939576A - Improvements in or relating to smoking tobacco product and method of making the same - Google Patents

Improvements in or relating to smoking tobacco product and method of making the same

Info

Publication number
GB939576A
GB939576A GB20449/62A GB2044962A GB939576A GB 939576 A GB939576 A GB 939576A GB 20449/62 A GB20449/62 A GB 20449/62A GB 2044962 A GB2044962 A GB 2044962A GB 939576 A GB939576 A GB 939576A
Authority
GB
United Kingdom
Prior art keywords
menthol
acid
ester
give
tobacco
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB20449/62A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
British American Tobacco Investments Ltd
Original Assignee
British American Tobacco Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by British American Tobacco Co Ltd filed Critical British American Tobacco Co Ltd
Publication of GB939576A publication Critical patent/GB939576A/en
Expired legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/301Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

Landscapes

  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Menthol acid polycarboxylic esters for incorporation in tobacco (see Group VI) are prepared using normal methods, by reacting maleic anhydride and menthol to give menthol acid maleate of m.p. 83-85 DEG C. or by alcoholysis of di-menthyl maleate with aqueous sodium hydroxide solution to give menthol acid maleate of m.p. 84-85 DEG C., by reacting succinic anhydride and menthol to give menthol acid succinate of m.p. 58-59 DEG C., and by reacting menthol and hemimellitic acid using p-toluene sulphonic acid as a catalyst to give menthol acid hemimellitate.ALSO:A smoking tobacco is treated by incorporating therein a mono-ester of menthol and a polycarboxylic acid or anhydride thereof. The acid may be saturated or unsaturated aliphatic or aromatic or heteroaromatic and 18 examples of suitable acids are given. Examples are given of methods for incorporating the ester in the tobacco by spraying with or dipping in a solution or suspension of the ester. The ester may also be applied to the paper or leaf wrapper of the tobacco product. Methods for the preparation of monomenthylmaleate, monomenthylsuccinate and monomenthylhemimellitate are included (see Group IV (b)).
GB20449/62A 1961-06-27 1962-05-28 Improvements in or relating to smoking tobacco product and method of making the same Expired GB939576A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US119779A US3111127A (en) 1961-06-27 1961-06-27 Smoking tobacco product and method of making the same

Publications (1)

Publication Number Publication Date
GB939576A true GB939576A (en) 1963-10-16

Family

ID=22386347

Family Applications (1)

Application Number Title Priority Date Filing Date
GB20449/62A Expired GB939576A (en) 1961-06-27 1962-05-28 Improvements in or relating to smoking tobacco product and method of making the same

Country Status (7)

Country Link
US (1) US3111127A (en)
BE (1) BE619401A (en)
CH (1) CH458169A (en)
CY (1) CY293A (en)
DK (1) DK116713B (en)
GB (1) GB939576A (en)
MY (1) MY6400103A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117089948A (en) * 2023-10-18 2023-11-21 汕头市兴裕泰纺织有限公司 Cooling factor modified nylon fiber with special-shaped cross section, preparation method and application thereof in cool sense anti-ultraviolet fabric

Families Citing this family (82)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3342186A (en) * 1964-08-07 1967-09-19 Allied Chem Aromatized tobaccos
US3704714A (en) * 1971-06-16 1972-12-05 Liggett & Myers Inc 2-isopropyl-5-methyl-2-hexenal, 2-isop-ropyl-5-methylhexanal,3-hydroxy-2-isopropyl-5-methylhexanal, and derivatives thereof as tobacco flavorants
US3762423A (en) * 1971-06-16 1973-10-02 Liggett & Myers Inc Methyl trans-2-isopropyl-5-methyl-3-hexenoate and derivatives thereof as tobacco flavorants
US3750674A (en) * 1972-08-07 1973-08-07 Reynolds Tobacco Co R Tobacco product
US4119106A (en) * 1975-10-22 1978-10-10 Philip Morris, Incorporated Flavorant-release resin compositions
US5752529A (en) * 1996-08-21 1998-05-19 V. Mane Fils S.A. Tobacco products containing coolant compositions
WO1997007771A1 (en) * 1995-08-29 1997-03-06 V. Mane Fils S.A. Refreshing compositions
US5843466A (en) * 1995-08-29 1998-12-01 V. Mane Fils S.A. Coolant compositions
WO1998011867A1 (en) * 1996-09-20 1998-03-26 Warner-Lambert Company Oral compositions containing a zinc compound
DE60215385T2 (en) * 2001-12-19 2007-10-25 Vector Tobacco Inc.(N.D.Ges.D.Staates Virginia) METHOD AND COMPOSITION FOR THE MENTHOLENREICHICHUNG OF CIGARETTES
US20040185093A1 (en) * 2003-03-18 2004-09-23 Szymczak Christopher E. Compositions containing sucralose
US7361376B2 (en) 2003-04-11 2008-04-22 International Flavors & Fragrances Inc. Alkyldienamides exhibiting taste and sensory effect in flavor compositions
US7632531B2 (en) * 2003-04-11 2009-12-15 International Flavors & Fragnances Inc. Alkyldienamides exhibiting taste and sensory effect in flavor compositions
US6884906B2 (en) * 2003-07-01 2005-04-26 International Flavors & Fragrances Inc. Menthyl half acid ester derivatives, processes for preparing same, and uses thereof for their cooling/refreshing effect in consumable materials
US7141686B2 (en) * 2003-07-10 2006-11-28 International Flavors & Fragrances Inc. E2, E4, Z8-undecatrienoic acid and ester and carboxamide derivatives thereof, organoleptic uses thereof and processes for preparing same
US7025997B2 (en) * 2003-09-24 2006-04-11 International Flavors & Fragrances Inc. Coolant plant extract compositions containing monomenthyl succinate
US8007839B2 (en) * 2003-10-03 2011-08-30 International Flavors & Fragrances Conjugated dienamides, methods of production thereof, compositions containing same and uses thereof
US7329767B2 (en) 2003-10-03 2008-02-12 International Flavors & Fragrances Inc. Conjugated dienamides, methods of production thereof, compositions containing same and uses thereof
US7541055B2 (en) * 2004-09-10 2009-06-02 International Flavors & Fragrances Inc. Saturated and unsaturated N-alkamides exhibiting taste and flavor enhancement effect in flavor compositions
US7427421B2 (en) * 2004-09-10 2008-09-23 International Flavors & Fragrances Inc. Saturated and unsaturated N-alkamides exhibiting taste and flavor enhancement effect in flavor compositions
CA2623545C (en) 2005-10-05 2013-04-09 Cadbury Adams Usa Llc Cooling compositions
US7856988B2 (en) * 2005-10-18 2010-12-28 Philip Morris Usa Inc. Method of making reconstituted tobacco with bonded flavorant
US7247743B1 (en) * 2006-02-27 2007-07-24 Millennium Specialty Chemicals, Inc. Process for making monomenthyl esters
US8356606B2 (en) 2007-06-01 2013-01-22 Philip Morris Usa Inc. Production of micronized encapsulated tobacco particles for tobacco flavor delivery from an oral pouch
US8541401B2 (en) * 2007-07-25 2013-09-24 Philip Morris Usa Inc. Flavorant ester salts of polycarboxylic acids and methods for immobilizing and delivering flavorants containing hydroxyl groups
RU2517179C2 (en) 2008-08-15 2014-05-27 Дзе Проктер Энд Гэмбл Компани Synthesis of cyclohexane derivatives used as sensates in consumer goods
WO2010019729A1 (en) * 2008-08-15 2010-02-18 The Procter & Gamble Company Solution of menthane carboxamides for use in consumer products
CN102215808B (en) 2008-11-20 2014-04-23 宝洁公司 Personal care compositions providing enhanced cooling sensation
US9155772B2 (en) 2008-12-08 2015-10-13 Philip Morris Usa Inc. Soft, chewable and orally dissolvable and/or disintegrable products
US9167835B2 (en) * 2008-12-30 2015-10-27 Philip Morris Usa Inc. Dissolvable films impregnated with encapsulated tobacco, tea, coffee, botanicals, and flavors for oral products
US9167847B2 (en) 2009-03-16 2015-10-27 Philip Morris Usa Inc. Production of coated tobacco particles suitable for usage in a smokeless tobacoo product
US7960580B2 (en) * 2009-04-22 2011-06-14 Renessenz, Llc Process for making menthyl glutarate
US9185925B2 (en) 2009-10-09 2015-11-17 Philip Morris Usa Inc. Immobilized flavorants for flavor delivery
DE102010002558A1 (en) 2009-11-20 2011-06-01 Symrise Ag Use of physiological cooling agents and agents containing such agents
US9089162B2 (en) 2010-03-26 2015-07-28 Philip Morris Usa Inc. Smoking articles containing polymers of polycarboxylic acid esters
US20120014883A1 (en) 2010-07-19 2012-01-19 Douglas Craig Scott Compositions Comprising Derivatives Of Essential Oil Compounds And Use In Personal Care Products
RU2536137C2 (en) 2010-08-18 2014-12-20 Интерконтинентал Грейт Брэндс ЛЛС Chewing gum composition moistening mouth (versions) and products containing it
JP2013534146A (en) 2010-08-18 2013-09-02 クラフト・フーズ・グローバル・ブランズ・エルエルシー Mouth moisturizing gum composition and product comprising the same
AU2011308857B2 (en) 2010-10-01 2015-11-05 The Procter & Gamble Company Oral care compositions with improved flavor
US20130042482A1 (en) 2011-08-16 2013-02-21 Valerie Jean Bradford Skin Engaging Member Comprising An Anti-Irritation Agent
PL2750656T3 (en) 2011-09-01 2018-12-31 The Procter & Gamble Company Oral care compositions with improved rheology
EP2758041B1 (en) 2011-09-20 2021-01-13 Basf Se Low-molecular modulators of the cold-menthol receptor trpm8 and use of same
EP3219303B1 (en) 2012-01-30 2019-11-06 Symrise AG Compositions
US9743685B2 (en) 2012-05-16 2017-08-29 Symrise Ag Mixtures having improved cooling effect
US20130315843A1 (en) 2012-05-25 2013-11-28 The Procter & Gamble Company Composition for reduction of trpa1 and trpv1 sensations
MX355922B (en) 2012-09-28 2018-05-03 Gillette Co Llc A skin engaging member comprising at least one thermally resilient sensate.
ES2643511T3 (en) 2012-09-28 2017-11-23 The Gillette Company Llc An auxiliary skin-shaving auxiliary member comprising at least one thermally resistant sensing agent
DE202012013357U1 (en) 2012-12-12 2016-07-29 Symrise Ag preparations
CN105025870B (en) 2012-12-12 2018-02-02 西姆莱斯股份公司 Composition
EP2801263B1 (en) 2013-05-09 2021-04-14 Symrise AG Process for the preparation of a cooling composition in the form of granules
WO2015037648A1 (en) * 2013-09-13 2015-03-19 長谷川香料株式会社 Freshness-maintaining agent having reduced off-flavor
US9884130B2 (en) 2013-11-13 2018-02-06 The Procter & Gamble Company Compositions for delivery of oral comfort sensations
US20150273711A1 (en) 2014-03-26 2015-10-01 The Gillette Company Razor Comprising A Molded Shaving Aid Composition Comprising A Thermally Resilient Sensate
US20150272847A1 (en) 2014-03-26 2015-10-01 The Gillette Company Skin Engaging Shaving Aid Comprising A Thermally Resilient Sensate And A TRPA1 Receptor Inhibitor
EP3134080A1 (en) 2014-04-23 2017-03-01 The Procter & Gamble Company Cyclohexanecarboxamide with cooling properties
EP2979751B1 (en) 2014-07-29 2020-10-28 Symrise AG Process for the manufacturing of solid cooling agents
SG11201703353RA (en) 2014-11-26 2017-06-29 Gillette Co Llc A skin engaging member comprising ethylene vinyl acetate
US9951295B2 (en) 2015-02-19 2018-04-24 The Procter & Gamble Company Compositions for deposition on biological surfaces
EP4015075A1 (en) 2015-02-19 2022-06-22 Symrise AG Standard packages with fixed cooling materials
US11696884B2 (en) 2015-03-04 2023-07-11 Symrise Ag Compositions comprising menthol compounds as smoothing agents
CN107532063B (en) 2015-03-25 2020-03-10 高砂香料工业株式会社 Methylmenthol derivative and cold-sensitive composition containing the same
EP3381453A3 (en) 2015-04-09 2018-12-12 The Procter & Gamble Company Reduction in cpc taste aversion by reducing cpc activation of trpa1 receptors, tprv1 receptors, or both
CA3000021C (en) 2015-10-22 2020-10-13 The Procter & Gamble Company Method of separating stereoisomers using supercritical fluid chromatography
MX2018004814A (en) 2015-10-22 2019-04-01 Procter & Gamble Synthesis of cyclohexane carboxamide derivatives useful as sensates in consumer products.
AU2016371908A1 (en) 2015-12-18 2018-07-05 The Procter & Gamble Company Synthesis of cyclohexane ester derivatives useful as sensates in consumer products
US10933039B2 (en) 2016-05-05 2021-03-02 Symrise Ag Coolant mixtures
CN109310595A (en) 2016-05-14 2019-02-05 西姆莱斯股份公司 Flavor formulation containing menthol
US20170334082A1 (en) 2016-05-18 2017-11-23 The Gillette Company Llc Skin Engaging Member Comprising Ethylene Vinyl Acetate
WO2018081189A1 (en) 2016-10-25 2018-05-03 The Procter & Gamble Company Fibrous structures
WO2018081190A1 (en) 2016-10-25 2018-05-03 The Procter & Gamble Company Fibrous structures
WO2018085479A1 (en) 2016-11-03 2018-05-11 The Gillette Company Llc Skin engaging member comprising ethylene vinyl acetate
EP3541476A1 (en) 2016-11-17 2019-09-25 The Gillette Company LLC Skin engaging member comprising ethylene vinyl acetate and a fragrance
MX2020002347A (en) 2017-08-31 2020-10-28 Basf Se Use of physiological cooling active ingredients, and compositions comprising such active ingredients.
EP3689324A1 (en) 2019-02-04 2020-08-05 Symrise AG New cooling agents and preparations comprising them
EP4259287A1 (en) 2020-12-09 2023-10-18 Symrise AG A method for fighting microorganisms using menthol derivatives
CN117615798A (en) 2021-06-10 2024-02-27 西姆莱斯股份公司 Composition for combating malodour
EP4387587A1 (en) 2021-08-16 2024-06-26 Symrise AG Compositions
EP4429465A1 (en) 2021-11-10 2024-09-18 Symrise AG Compositions comprising trpm8 agonistic cooling agents
WO2023147852A1 (en) 2022-02-02 2023-08-10 Symrise Ag Compositions (iii)
WO2023222213A1 (en) 2022-05-18 2023-11-23 Symrise Ag Antimicrobial mixtures
WO2022207944A2 (en) 2022-07-11 2022-10-06 Symrise Ag Novel mixtures and uses of (2e)-3-(1,3-benzodioxol-5-yl)-n-phenyl-n-(tetrahydro-3-furanyl)-2-propenamide
WO2024110023A1 (en) 2022-11-23 2024-05-30 Symrise Ag An active composition comprising retinol

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1065767B (en) * 1959-09-17 Zigarettenfabrik KOSMOS G.m. b.H., Memmingen (Allgäu) Process for mentholizing tobacco and manufacturing menthol cigarettes
GB189612736A (en) * 1896-06-10 1897-05-01 Richard Pserhofer Improvements in and connected with the Manufacture of Tobacco.
US1673216A (en) * 1927-10-27 1928-06-12 Vuccino Amedee Method of treating tobacco
US2822306A (en) * 1955-07-01 1958-02-04 Plate Gmbh Dr Aromatic and pleasant tasting de-nicotinized tobacco and method of producing same
US2936320A (en) * 1957-06-24 1960-05-10 California Research Corp Diesters of mixed aromatic dibasic acids
US2921089A (en) * 1957-11-27 1960-01-12 Eastman Kodak Co 2-propylheptanol and its esters
US2941907A (en) * 1958-05-22 1960-06-21 Dow Chemical Co Tobacco compositions

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117089948A (en) * 2023-10-18 2023-11-21 汕头市兴裕泰纺织有限公司 Cooling factor modified nylon fiber with special-shaped cross section, preparation method and application thereof in cool sense anti-ultraviolet fabric

Also Published As

Publication number Publication date
BE619401A (en) 1962-12-27
CY293A (en) 1964-06-13
CH458169A (en) 1968-06-15
DK116713B (en) 1970-02-02
MY6400103A (en) 1964-12-31
US3111127A (en) 1963-11-19

Similar Documents

Publication Publication Date Title
GB939576A (en) Improvements in or relating to smoking tobacco product and method of making the same
SE7905659L (en) MEANS FOR THE TREATMENT OF SEBORREIS CONDITIONS
GB883769A (en) 3ª-:16ª-:17ª--trihydroxy steroids
PH13267A (en) D*honoandrostant-117oc-carboxylic acid derivatives
GB1293870A (en) Preparation of cis-1-alkenyl phosphonic acids and their o-carboxyphenyl esters
GB827638A (en) Preparation of citraconic anhydride
CA544032A (en) Process for preparing esters of aromatic polycarboxylic acids
GB716077A (en) Method of stabilizing a carboxylic peracid
GB922802A (en) A process for the preparation of 4-acyloxy-and 4-hydroxy-3-keto-í¸-steroids
GB942664A (en) Improved methods of producing dimethyl ª -ketoadipate and dimethyl ª -methyl ª -ketoadipate
GB951108A (en) A-nor steroids
GB874152A (en) Process for the production of alpha-amino-beta-hydroxy-carboxylic acids
GB842523A (en) Process for preparation of isoascorbic acid
GB894134A (en) New active insecticidal esters of the pyrethrum type and a process for the production thereof
CA528127A (en) Lactones of 2,2-dihalogeno-4-hydroxyalkanoic acids
CA576507A (en) Preparation of alkyl esters of acylated 3,5-diaminopolyiodobenzoic acids
CA528234A (en) Process for treating aqueous mixture of methyl acetate, methyl alcohol and acetic acid
UA6043A1 (en) Method for producing chloroambucyl derivatives (variants)
SU1841126A1 (en) Method of producing alkanephosphonic acids 2,2,2-trinitroethyl esters
CA573956A (en) Process for the preparation of esters of carboxylic acids of low solubility
GB889407A (en) Methylated steroidal lactones
AU224760B2 (en) Improved process for the manufacture of alpha-2, 4, 5-trichlorophenoxypropionic acid alkyl esters and derivatives thereof from 2, 4, 5-trichlorophenol
GB822720A (en) Production of xanthene derivatives
GB848410A (en) Improvements in or relating to dipeptide derivatives
GB961343A (en) Tetrahydrofurfuryl 3-pyridylacetate