GB932300A - Process for the preparation of surface-active esters of inorganic polybasic acids - Google Patents

Process for the preparation of surface-active esters of inorganic polybasic acids

Info

Publication number
GB932300A
GB932300A GB9751/61A GB975161A GB932300A GB 932300 A GB932300 A GB 932300A GB 9751/61 A GB9751/61 A GB 9751/61A GB 975161 A GB975161 A GB 975161A GB 932300 A GB932300 A GB 932300A
Authority
GB
United Kingdom
Prior art keywords
oil
acid
carbon atoms
chains
alcohols
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB9751/61A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Boehme Fettchemie GmbH
Original Assignee
Boehme Fettchemie GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Boehme Fettchemie GmbH filed Critical Boehme Fettchemie GmbH
Publication of GB932300A publication Critical patent/GB932300A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/24—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfuric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic System
    • C07F5/02—Boron compounds
    • C07F5/04—Esters of boric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C07F9/09—Esters of phosphoric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G99/00—Subject matter not provided for in other groups of this subclass
    • C07G99/002—Compounds of unknown constitution containing sulfur
    • C—CHEMISTRY; METALLURGY
    • C14—SKINS; HIDES; PELTS; LEATHER
    • C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
    • C14C3/00—Tanning; Compositions for tanning
    • C14C3/02—Chemical tanning
    • C14C3/08—Chemical tanning by organic agents
    • C14C3/14—Fat tanning; Oil tanning
    • C—CHEMISTRY; METALLURGY
    • C14—SKINS; HIDES; PELTS; LEATHER
    • C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
    • C14C9/00—Impregnating leather for preserving, waterproofing, making resistant to heat or similar purposes
    • C14C9/02—Impregnating leather for preserving, waterproofing, making resistant to heat or similar purposes using fatty or oily materials, e.g. fat liquoring
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
    • D06P1/613—Polyethers without nitrogen
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
    • D06P1/613—Polyethers without nitrogen
    • D06P1/6136—Condensation products of esters, acids, oils, oxyacids with oxiranes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/02—Water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/042—Sulfate esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/46—Textile oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10—Semi-solids; greasy

Abstract

Surface active esters are prepared by reacting, at 10 DEG to 40 DEG C., epoxidised products of higher molecular weight unsaturated compounds having an epoxy oxygen content up to 3% by weight and at least one carbon chain which has from 10 to 26 carbon atoms, with a polybasic inorganic acid or anhydride, and, if desired, neutralisation of the reaction product. The carbon chains are uninterrupted straight or branched chains of carbon atoms which may be in the form of, or form part of, a ring system. Preferred chains are those containing 12-24 carbon atoms. Chains of 10 to 14 carbon atoms provide products with wetting action and those of 12 to 20 carbon atoms yield products with washing and cleaning action. The higher molecular weight unsaturated compounds include hydrocarbons such as dodecene, octadecene and squalene; alcohols such as oleyl, and other mono or poly unsaturated alcohols, acids such as monoor poly-basic unsaturated carboxylic acids and esters and amides thereof, especially naturally occurring glycerides such as soya bean oil, cotton seed oil, rape seed oil, linseed oil, castor oil, sunflower seed oil, olive oil, neat's foot oil, sperm oil, herring oil, cod oil, shark liver oil, whale oil or the interesterification products thereof, in addition esters of mono or polyhydric alcohols of the aliphatic, cycloaliphatic, aromatic or heterocyclic series, such as n-butyl, t-amyl, 2 ethylhexyl, octadecyl, cyclohexyl, methylcyclohexyl, naphthyl and benzyl alcohols, also with ethylene glycol, 1,2 propylene glycol, butanediol-1,4, dodecanediol-1,12, pentaerythritol and polyalkylene glycols, the amides may be based on fatty acid amides derived from ammonia, dimethylamine, dodecylamine, oleylamine, ethylenediamine, cyclohexylamine or benzylamine. Preferred starting epoxides have an epoxide oxygen content of 0.5 to 3%. The reaction may be carried out in an inert diluent at a preferred temperature range of 15-35 DEG C. using as the polybasic inorganic acid boric acid, sulphuric acid, sulphur trioxide, pyridinesulphuric acid adducts, oleum, phosphoric acid, phosphorus pentoxide, or anhydrous phosphoric acids. Examples illustrate the reaction of various epoxidised oils and epoxidised decyl oleate, with sulphuric and phosphoric acids. The epoxidation (partial) of some of the starting materials with hydrogen peroxide and acetic acid is described.
GB9751/61A 1960-05-04 1961-03-17 Process for the preparation of surface-active esters of inorganic polybasic acids Expired GB932300A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE1960B0057714 DE1198815C2 (en) 1960-05-04 1960-05-04 PROCESS FOR THE PRODUCTION OF SURFACE-ACTIVE SULFUR ACID ESTERS AND THEIR SALT
DE1418650A DE1418650B2 (en) 1960-05-04 1960-12-24 Process for the production of surface-active sulfuric acid esters or their salts

Publications (1)

Publication Number Publication Date
GB932300A true GB932300A (en) 1963-07-24

Family

ID=25965640

Family Applications (2)

Application Number Title Priority Date Filing Date
GB9751/61A Expired GB932300A (en) 1960-05-04 1961-03-17 Process for the preparation of surface-active esters of inorganic polybasic acids
GB35022/61A Expired GB949249A (en) 1960-05-04 1961-09-29 Sulphonation products of epoxidised higher molecular weight compounds

Family Applications After (1)

Application Number Title Priority Date Filing Date
GB35022/61A Expired GB949249A (en) 1960-05-04 1961-09-29 Sulphonation products of epoxidised higher molecular weight compounds

Country Status (6)

Country Link
CH (2) CH388935A (en)
DE (2) DE1198815C2 (en)
GB (2) GB932300A (en)
IT (1) IT649680A (en)
NL (1) NL271858A (en)
SE (1) SE310361B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116103451A (en) * 2023-03-30 2023-05-12 精艺裘皮制品股份有限公司 Multi-working-procedure effective synergistic beach sheepskin harmless tanning method

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3617657C2 (en) * 1986-05-26 1994-08-18 Stockhausen Chem Fab Gmbh Room temperature liquid derivatives of natural fats or oils, process for their preparation, and their use
DE4231073A1 (en) * 1992-09-17 1994-03-24 Rhein Chemie Rheinau Gmbh Phosphorylation of epoxides
CN110055754B (en) * 2019-05-07 2021-08-10 四川丝玛帛科技有限公司 Soft lubricating grafted modified silk, preparation method thereof and grease emulsion

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE969930C (en) * 1954-05-06 1958-07-31 Henkel & Cie Gmbh Process for the production of higher molecular weight compounds

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116103451A (en) * 2023-03-30 2023-05-12 精艺裘皮制品股份有限公司 Multi-working-procedure effective synergistic beach sheepskin harmless tanning method

Also Published As

Publication number Publication date
IT649680A (en)
CH388935A (en) 1965-03-15
DE1418650A1 (en) 1969-10-09
SE310361B (en) 1969-04-28
DE1198815C2 (en) 1975-12-04
DE1198815B (en) 1965-08-19
NL271858A (en)
GB949249A (en) 1964-02-12
DE1418650B2 (en) 1978-05-03
CH412865A (en) 1966-05-15

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