GB921556A - Process for the production of a derivative of hypoglycine a - Google Patents
Process for the production of a derivative of hypoglycine aInfo
- Publication number
- GB921556A GB921556A GB293060A GB293060A GB921556A GB 921556 A GB921556 A GB 921556A GB 293060 A GB293060 A GB 293060A GB 293060 A GB293060 A GB 293060A GB 921556 A GB921556 A GB 921556A
- Authority
- GB
- United Kingdom
- Prior art keywords
- compound
- formula
- reacting
- hypoglycine
- derivative
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OOJZCXFXPZGUBJ-RITPCOANSA-N hypoglycin Chemical class OC(=O)[C@@H](N)C[C@H]1CC1=C OOJZCXFXPZGUBJ-RITPCOANSA-N 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 4
- -1 aralkyl ester Chemical class 0.000 abstract 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 150000008064 anhydrides Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 235000019253 formic acid Nutrition 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 150000007530 organic bases Chemical group 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07K—PEPTIDES
- C07K5/00—Peptides containing up to four amino acids in a fully defined sequence; Derivatives thereof
- C07K5/02—Peptides containing up to four amino acids in a fully defined sequence; Derivatives thereof containing at least one abnormal peptide link
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Biophysics (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Medicinal Chemistry (AREA)
- Molecular Biology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention comprises a compound of the formula <FORM:0921556/IV(a)/1> and the preparation thereof by reacting a compound of the formula <FORM:0921556/IV(a)/2> (wherein R is an alkyl group in an inert anhydrous organic solvent and in the presence of a tertiary organic base, with a halogen formic acid alkyl or aralkyl ester, reacting the solution of a mixed anhydride so obtained with an aqueous solution of an alkali metal salt of a compound of the formula <FORM:0921556/IV(a)/3> to give a compound of the formula <FORM:0921556/IV(a)/4> and hydrolysing this under alkaline conditions. All the steps in the reaction are performed at low temperatures. An example is given.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH6901059 | 1959-01-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB921556A true GB921556A (en) | 1963-03-20 |
Family
ID=4529164
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB293060A Expired GB921556A (en) | 1959-01-30 | 1960-01-27 | Process for the production of a derivative of hypoglycine a |
Country Status (2)
| Country | Link |
|---|---|
| ES (1) | ES255380A1 (en) |
| GB (1) | GB921556A (en) |
-
1960
- 1960-01-27 GB GB293060A patent/GB921556A/en not_active Expired
- 1960-01-29 ES ES0255380A patent/ES255380A1/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| ES255380A1 (en) | 1960-07-01 |
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