GB912532A - Improvements in the treatment of dense soda ash - Google Patents

Improvements in the treatment of dense soda ash

Info

Publication number
GB912532A
GB912532A GB3791260A GB3791260A GB912532A GB 912532 A GB912532 A GB 912532A GB 3791260 A GB3791260 A GB 3791260A GB 3791260 A GB3791260 A GB 3791260A GB 912532 A GB912532 A GB 912532A
Authority
GB
United Kingdom
Prior art keywords
ash
na2co3
solution
withdrawn
dense
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3791260A
Inventor
Ned Alden Caldwell
William Charles Bauer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FMC Corp
Original Assignee
FMC Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FMC Corp filed Critical FMC Corp
Priority to GB3791260A priority Critical patent/GB912532A/en
Publication of GB912532A publication Critical patent/GB912532A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00Carbonates of sodium, potassium or alkali metals in general
    • C01D7/22Purification
    • C01D7/24Crystallisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

In a process producing dense soda ash, where trona is dissolved in a circulating aqueous solution of Na2CO3 and NaHCO3 containing a greater concentration of carbonate than bicarbonate insoluble and organic substances are removed from the loaded solution, sodium sesquicarbonate is crystallized by cooling and filtering, and the sesquicarbonate is heated to form light ash, a portion of the filtered circulating solution is withdrawn at any point in the cycle, and reacted with the light ash to form Na2CO3.H2O, which is heated to form dense ash. The withdrawn solution, containing 17,5-38 parts Na2CO3 and 1-16 parts NaHCO3/100 parts water (temperature 15 DEG -105 DEG C.) is contacted with light ash (temperature 140 DEG -265 DEG C.) to form a 1:1 molar mixture. Heating the Na2CO3.H2O to 140 DEG -210 DEG C. gives dense ash. The withdrawn liquor may be diluted with water before contacting with light ash.
GB3791260A 1960-11-04 1960-11-04 Improvements in the treatment of dense soda ash Expired GB912532A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB3791260A GB912532A (en) 1960-11-04 1960-11-04 Improvements in the treatment of dense soda ash

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3791260A GB912532A (en) 1960-11-04 1960-11-04 Improvements in the treatment of dense soda ash

Publications (1)

Publication Number Publication Date
GB912532A true GB912532A (en) 1962-12-12

Family

ID=10399882

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3791260A Expired GB912532A (en) 1960-11-04 1960-11-04 Improvements in the treatment of dense soda ash

Country Status (1)

Country Link
GB (1) GB912532A (en)

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