GB896786A - Catalyst feeding - Google Patents

Catalyst feeding

Info

Publication number
GB896786A
GB896786A GB32894/58A GB3289458A GB896786A GB 896786 A GB896786 A GB 896786A GB 32894/58 A GB32894/58 A GB 32894/58A GB 3289458 A GB3289458 A GB 3289458A GB 896786 A GB896786 A GB 896786A
Authority
GB
United Kingdom
Prior art keywords
liquid
catalyst
reactor
zone
discharge opening
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB32894/58A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Celanese Corp
Original Assignee
Celanese Corp
Celanese Corp of America
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Celanese Corp, Celanese Corp of America filed Critical Celanese Corp
Publication of GB896786A publication Critical patent/GB896786A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/0045Feeding of the particles in the reactor; Evacuation of the particles out of the reactor by means of a rotary device in the flow channel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/003Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/0061Controlling the level
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743Feeding or discharging of solids
    • B01J2208/00752Feeding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00191Control algorithm
    • B01J2219/00193Sensing a parameter
    • B01J2219/00207Sensing a parameter other than of the reactor heat exchange system
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00191Control algorithm
    • B01J2219/00211Control algorithm comparing a sensed parameter with a pre-set value
    • B01J2219/00213Fixed parameter value
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00191Control algorithm
    • B01J2219/00222Control algorithm taking actions
    • B01J2219/00227Control algorithm taking actions modifying the operating conditions
    • B01J2219/0024Control algorithm taking actions modifying the operating conditions other than of the reactor or heat exchange system

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

A method of feeding powdered solid catalyst into a reactor comprises continuously feeding the catalyst at a controlled rate into a zone provided with a discharge opening communicating with the reactor and continuously feeding a liquid at an independently controlled rate into the zone, the liquid passing through said discharge opening and carrying catalyst therewith as a slurry of controlled solids content into the reactor, a body of said liquid being maintained in said zone and fresh liquid being supplied thereto at such a rate as to maintain the volume of liquid therein between predetermined limits. The invention also consists of an apparatus comprising said reactor, zone (a vessel) and discharge opening; means for continuously supplying at independent rates the catalyst and liquid, and means for maintaining within predetermined limits a head of liquid in the vessel. The catalyst may be introduced by way of a pipe below the liquid level; preferably within the pipe is a screw conveyer adapted to forward the catalyst through the pipe at a lower rate near the outlet than at the inlet so as to cause the catalyst to form a plug sealing the outlet against ingress of liquid. Specification 790,195 is referred to.ALSO:Polymerization of olefines, particularly ethylene, is effected in a solvent with solid catalyst (e.g. thermally activated chromia-silica-alumina) slurried therein, the catalyst being supplied by continuously feeding it at a controlled rate into a zone provided with a discharge opening communicating with the reactor and continuously feeding a liquid at an independently controlled rate into the zone, the liquid passing through said discharge opening and carrying catalyst therewith as a slurry of controlled solids content into the reactor, a body of said liquid being maintained in said zone and fresh liquid being supplied thereto at such a rate as to maintain the volume of liquid therein between predetermined limits; the contents of the reactor are withdrawn in a measure as olefine and fresh catalyst slurry are supplied thereto. Other monomers listed are propylene, 1- and 2- butene, -pentene, -hexene and -octene; 2-and 3-methyl-1-butene; isobutylene, 1-dodecene, 4-methyl-1-pentene, 2-methyl-2-butene, cyclohexene, 4-vinylcyclohexene, butadiene and isoprene; mixtures of these specified monomers, and unspecified methyl, ethyl or chloro-substituted conjugated diolefins. The usual hydrocarbon solvents are mentioned, cyclohexane being particularly preferred. Specification 790,195 is referred to.
GB32894/58A 1957-11-25 1958-10-15 Catalyst feeding Expired GB896786A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US896786XA 1957-11-25 1957-11-25

Publications (1)

Publication Number Publication Date
GB896786A true GB896786A (en) 1962-05-16

Family

ID=22218994

Family Applications (1)

Application Number Title Priority Date Filing Date
GB32894/58A Expired GB896786A (en) 1957-11-25 1958-10-15 Catalyst feeding

Country Status (2)

Country Link
GB (1) GB896786A (en)
IT (1) IT599042A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002062462A1 (en) * 2001-02-02 2002-08-15 Basell Polyolefine Gmbh Method for dosing catalysts
WO2004054700A1 (en) * 2002-12-13 2004-07-01 Solvay Polyolefins Europe - Belgium (S.A.) Particulate flow control process
WO2006094766A1 (en) 2005-03-08 2006-09-14 Basf Aktiengesellschaft Method for filling a reactor
WO2007014103A1 (en) * 2005-07-22 2007-02-01 Kemya Pressure control system
WO2009088428A1 (en) * 2008-01-07 2009-07-16 Univation Technologies, Llc Catalyst feed systems and methods for using the same
EP2197573A1 (en) * 2007-09-11 2010-06-23 Rentech, Inc. System and method for catalyst loading/mixing
US7927555B2 (en) 2005-03-08 2011-04-19 Basf Aktiengesellschaft Charging of a reactor
CN112390902A (en) * 2020-07-22 2021-02-23 北京锦吾新材科技有限公司 Olefin polymerization process and application

Cited By (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002062462A1 (en) * 2001-02-02 2002-08-15 Basell Polyolefine Gmbh Method for dosing catalysts
US7527175B2 (en) 2001-02-02 2009-05-05 Basell Polyolefine Gmbh Metering of catalysts
WO2004054700A1 (en) * 2002-12-13 2004-07-01 Solvay Polyolefins Europe - Belgium (S.A.) Particulate flow control process
US8202485B2 (en) 2002-12-13 2012-06-19 Ineos Manufacturing Belgium Nv Particulate flow control process
US7713490B2 (en) 2002-12-13 2010-05-11 Ineos Manufacturing Belgium Nv Particulate flow control process
JP2008535646A (en) * 2005-03-08 2008-09-04 ビーエーエスエフ ソシエタス・ヨーロピア How to charge the reactor
CN101137431B (en) * 2005-03-08 2011-06-29 巴斯福股份公司 Method for filling a reactor
WO2006094766A1 (en) 2005-03-08 2006-09-14 Basf Aktiengesellschaft Method for filling a reactor
US7927555B2 (en) 2005-03-08 2011-04-19 Basf Aktiengesellschaft Charging of a reactor
EP1749567A1 (en) * 2005-07-22 2007-02-07 Kemya Al-Jubail Petrochemical Company Pressure control system
WO2007014103A1 (en) * 2005-07-22 2007-02-01 Kemya Pressure control system
JP2009502454A (en) * 2005-07-22 2009-01-29 ケムヤ Pressure control system
US8075846B2 (en) 2005-07-22 2011-12-13 Jubail Petrochemical Co. “Kemya” Pressure control system
EP2197573A1 (en) * 2007-09-11 2010-06-23 Rentech, Inc. System and method for catalyst loading/mixing
EP2197573A4 (en) * 2007-09-11 2011-01-05 Rentech Inc System and method for catalyst loading/mixing
US9073025B2 (en) 2007-09-11 2015-07-07 Res Usa, Llc System and method for catalyst loading/mixing
US10010842B2 (en) 2007-09-11 2018-07-03 Res Usa, Llc System and method for catalyst loading/mixing
WO2009088428A1 (en) * 2008-01-07 2009-07-16 Univation Technologies, Llc Catalyst feed systems and methods for using the same
US8206654B2 (en) 2008-01-07 2012-06-26 Univation Technologies, Llc Catalyst feed systems and methods for using the same
RU2486952C2 (en) * 2008-01-07 2013-07-10 Юнивейшн Текнолоджиз, Ллк Catalyst feed systems and methods of their application
US8496882B2 (en) 2008-01-07 2013-07-30 Univation Technologies, Llc Catalyst feed systems and methods for using the same
CN112390902A (en) * 2020-07-22 2021-02-23 北京锦吾新材科技有限公司 Olefin polymerization process and application

Also Published As

Publication number Publication date
IT599042A (en)

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