GB885692A - Improvements in or relating to the production of urea - Google Patents
Improvements in or relating to the production of ureaInfo
- Publication number
- GB885692A GB885692A GB4310659A GB4310659A GB885692A GB 885692 A GB885692 A GB 885692A GB 4310659 A GB4310659 A GB 4310659A GB 4310659 A GB4310659 A GB 4310659A GB 885692 A GB885692 A GB 885692A
- Authority
- GB
- United Kingdom
- Prior art keywords
- urea
- biuret
- synthesis
- autoclave
- stage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/14—Separation; Purification; Stabilisation; Use of additives
- C07C273/16—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Biuret-enriched urea mother liquor, obtained after separation of a biuret-impoverished urea by crystallization from a urea synthesis product comprising an aqueous solution of urea and biuret, is recycled to a stage in the urea synthesis which favours the conversion of biuret to urea. Such a stage is preferably characterized by pressures of 5 to 300 atmospheres, temperatures of between 100 DEG C. and 200 DEG C. and the presence of free ammonia. Such conditions may be provided in the autoclave during the synthesis of urea from ammonia and carbon dioxide or in high pressure distillation or scrubbing towers leading from the synthesis autoclave. The biuret-containing mother liquor may be used to absorb unreacted carbon dioxide or other reactants before returning it to the synthesis autoclave. Specification 885,691 is referred to.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR812587A FR1253254A (en) | 1959-12-09 | 1959-12-09 | Production process for low biuret urea |
GB4310659A GB885692A (en) | 1959-12-18 | 1959-12-18 | Improvements in or relating to the production of urea |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB4310659A GB885692A (en) | 1959-12-18 | 1959-12-18 | Improvements in or relating to the production of urea |
Publications (1)
Publication Number | Publication Date |
---|---|
GB885692A true GB885692A (en) | 1961-12-28 |
Family
ID=10427347
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB4310659A Expired GB885692A (en) | 1959-12-09 | 1959-12-18 | Improvements in or relating to the production of urea |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB885692A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3317601A (en) * | 1962-08-08 | 1967-05-02 | Toyo Koatsu Ind Inc | Synthesizing urea |
-
1959
- 1959-12-18 GB GB4310659A patent/GB885692A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3317601A (en) * | 1962-08-08 | 1967-05-02 | Toyo Koatsu Ind Inc | Synthesizing urea |
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