GB825185A - Improvements in or relating to the purification of electrolytic fluorine - Google Patents
Improvements in or relating to the purification of electrolytic fluorineInfo
- Publication number
- GB825185A GB825185A GB1731357A GB1731357A GB825185A GB 825185 A GB825185 A GB 825185A GB 1731357 A GB1731357 A GB 1731357A GB 1731357 A GB1731357 A GB 1731357A GB 825185 A GB825185 A GB 825185A
- Authority
- GB
- United Kingdom
- Prior art keywords
- regeneration
- trays
- naf
- purification
- relating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/20—Fluorine
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/245—Fluorine; Compounds thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Treating Waste Gases (AREA)
- Gas Separation By Absorption (AREA)
Abstract
HF-contaminated electrolytic fluorine is contacted with sodium fluoride powder at between 0 DEG and 85 DEG C. and the absorbent containing absorbed HF is subsequently regenerated by heating, and the steps of removing HF contaminant in F2 by regenerated absorbent at the specified temperatures and regenerating are repeated. Regeneration may be at 200-400 DEG C. in situ, in a stream of inert gas, e.g. N2 or air. The NaF powder may be in shallow beds in trays disposed in a series of superimposed horizontal shelves, which may be heated for regeneration by a grid of electric cable below each layer of trays or by a cable buried in the bed. Residual HF may be removed by passing the F2 through a further tower packed with NaF pellets.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DENDAT1073453D DE1073453B (en) | 1957-05-31 | Process for removing hydrogen fluoride from electrolytically produced fluorine | |
GB1731357A GB825185A (en) | 1957-05-31 | 1957-05-31 | Improvements in or relating to the purification of electrolytic fluorine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1731357A GB825185A (en) | 1957-05-31 | 1957-05-31 | Improvements in or relating to the purification of electrolytic fluorine |
Publications (1)
Publication Number | Publication Date |
---|---|
GB825185A true GB825185A (en) | 1959-12-09 |
Family
ID=10092988
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1731357A Expired GB825185A (en) | 1957-05-31 | 1957-05-31 | Improvements in or relating to the purification of electrolytic fluorine |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE1073453B (en) |
GB (1) | GB825185A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3989808A (en) * | 1975-07-28 | 1976-11-02 | The United States Of America As Represented By The United States Energy Research And Development Administration | Method of preparing pure fluorine gas |
EP1455918A2 (en) * | 2001-11-26 | 2004-09-15 | Fluorine on Call, Ltd. | Generation, distribution, and use of molecular fluorine within a fabrication facility |
JP2011017077A (en) * | 2009-06-12 | 2011-01-27 | Central Glass Co Ltd | Fluorine gas generating device |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5336832A (en) * | 1992-11-06 | 1994-08-09 | Conoco Inc. | Recovery of HF from hydrocarbon streams |
-
0
- DE DENDAT1073453D patent/DE1073453B/en active Pending
-
1957
- 1957-05-31 GB GB1731357A patent/GB825185A/en not_active Expired
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3989808A (en) * | 1975-07-28 | 1976-11-02 | The United States Of America As Represented By The United States Energy Research And Development Administration | Method of preparing pure fluorine gas |
EP1455918A2 (en) * | 2001-11-26 | 2004-09-15 | Fluorine on Call, Ltd. | Generation, distribution, and use of molecular fluorine within a fabrication facility |
EP1455918A4 (en) * | 2001-11-26 | 2004-12-15 | Fluorine On Call Ltd | Generation, distribution, and use of molecular fluorine within a fabrication facility |
JP2011017077A (en) * | 2009-06-12 | 2011-01-27 | Central Glass Co Ltd | Fluorine gas generating device |
EP2423354A1 (en) * | 2009-06-12 | 2012-02-29 | Central Glass Company, Limited | Fluorine gas generating device |
EP2423354A4 (en) * | 2009-06-12 | 2012-09-12 | Central Glass Co Ltd | Fluorine gas generating device |
Also Published As
Publication number | Publication date |
---|---|
DE1073453B (en) | 1960-01-21 |
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