GB778917A - Manufacture of stable solid diazonium compounds - Google Patents
Manufacture of stable solid diazonium compoundsInfo
- Publication number
- GB778917A GB778917A GB20498/54A GB2049854A GB778917A GB 778917 A GB778917 A GB 778917A GB 20498/54 A GB20498/54 A GB 20498/54A GB 2049854 A GB2049854 A GB 2049854A GB 778917 A GB778917 A GB 778917A
- Authority
- GB
- United Kingdom
- Prior art keywords
- diazonium
- oxalic acid
- solution
- oxalate
- chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007787 solid Substances 0.000 title abstract 6
- 150000001989 diazonium salts Chemical class 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract 15
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 10
- 239000012954 diazonium Substances 0.000 abstract 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-O diazynium Chemical compound [NH+]#N IJGRMHOSHXDMSA-UHFFFAOYSA-O 0.000 abstract 9
- 239000000243 solution Substances 0.000 abstract 6
- 235000006408 oxalic acid Nutrition 0.000 abstract 5
- 239000011780 sodium chloride Substances 0.000 abstract 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 4
- 150000001875 compounds Chemical class 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 3
- NIFHFRBCEUSGEE-UHFFFAOYSA-N oxalic acid Chemical compound OC(=O)C(O)=O.OC(=O)C(O)=O NIFHFRBCEUSGEE-UHFFFAOYSA-N 0.000 abstract 3
- 239000000975 dye Substances 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- TYMLOMAKGOJONV-UHFFFAOYSA-N 4-nitroaniline Chemical compound NC1=CC=C([N+]([O-])=O)C=C1 TYMLOMAKGOJONV-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 abstract 1
- -1 aminoazo compound Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- IRXRGVFLQOSHOH-UHFFFAOYSA-L dipotassium;oxalate Chemical compound [K+].[K+].[O-]C(=O)C([O-])=O IRXRGVFLQOSHOH-UHFFFAOYSA-L 0.000 abstract 1
- 150000002790 naphthalenes Chemical class 0.000 abstract 1
- VMPITZXILSNTON-UHFFFAOYSA-N o-anisidine Chemical compound COC1=CC=CC=C1N VMPITZXILSNTON-UHFFFAOYSA-N 0.000 abstract 1
- 235000011118 potassium hydroxide Nutrition 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000005185 salting out Methods 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- ZPEJZWGMHAKWNL-UHFFFAOYSA-L zinc;oxalate Chemical compound [Zn+2].[O-]C(=O)C([O-])=O ZPEJZWGMHAKWNL-UHFFFAOYSA-L 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B43/00—Preparation of azo dyes from other azo compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/02—Ethers
- C07C43/257—Ethers having an ether-oxygen atom bound to carbon atoms both belonging to six-membered aromatic rings
- C07C43/29—Ethers having an ether-oxygen atom bound to carbon atoms both belonging to six-membered aromatic rings containing halogen
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/06—Monoazo dyes prepared by diazotising and coupling from coupling components containing amino as the only directing group
- C09B29/08—Amino benzenes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE328081X | 1953-07-13 | ||
| DEF15407A DE954422C (de) | 1953-07-13 | 1954-08-08 | Verfahren zur Herstellung einer festen, haltbaren Diazoniumverbindung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB778917A true GB778917A (en) | 1957-07-17 |
Family
ID=25807313
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB20498/54A Expired GB778917A (en) | 1953-07-13 | 1954-07-13 | Manufacture of stable solid diazonium compounds |
| GB22678/55A Expired GB779389A (en) | 1953-07-13 | 1955-08-05 | A stable solid diazonium compound and process for making it |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB22678/55A Expired GB779389A (en) | 1953-07-13 | 1955-08-05 | A stable solid diazonium compound and process for making it |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US2744103A (en:Method) |
| BE (2) | BE530351A (en:Method) |
| CH (2) | CH328081A (en:Method) |
| DE (1) | DE954422C (en:Method) |
| FR (2) | FR1104617A (en:Method) |
| GB (2) | GB778917A (en:Method) |
| NL (3) | NL86069C (en:Method) |
Families Citing this family (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL87093C (en:Method) * | 1953-07-13 | |||
| NL97423C (en:Method) * | 1956-05-09 | 1900-01-01 | ||
| US3539345A (en) * | 1967-02-01 | 1970-11-10 | Gaf Corp | Thermal diazotype papers |
| US6017471A (en) * | 1993-08-05 | 2000-01-25 | Kimberly-Clark Worldwide, Inc. | Colorants and colorant modifiers |
| US5645964A (en) * | 1993-08-05 | 1997-07-08 | Kimberly-Clark Corporation | Digital information recording media and method of using same |
| US5643356A (en) * | 1993-08-05 | 1997-07-01 | Kimberly-Clark Corporation | Ink for ink jet printers |
| US5865471A (en) * | 1993-08-05 | 1999-02-02 | Kimberly-Clark Worldwide, Inc. | Photo-erasable data processing forms |
| US5773182A (en) * | 1993-08-05 | 1998-06-30 | Kimberly-Clark Worldwide, Inc. | Method of light stabilizing a colorant |
| US5700850A (en) * | 1993-08-05 | 1997-12-23 | Kimberly-Clark Worldwide | Colorant compositions and colorant stabilizers |
| US5721287A (en) * | 1993-08-05 | 1998-02-24 | Kimberly-Clark Worldwide, Inc. | Method of mutating a colorant by irradiation |
| US6211383B1 (en) | 1993-08-05 | 2001-04-03 | Kimberly-Clark Worldwide, Inc. | Nohr-McDonald elimination reaction |
| US5681380A (en) | 1995-06-05 | 1997-10-28 | Kimberly-Clark Worldwide, Inc. | Ink for ink jet printers |
| CA2120838A1 (en) * | 1993-08-05 | 1995-02-06 | Ronald Sinclair Nohr | Solid colored composition mutable by ultraviolet radiation |
| US6017661A (en) * | 1994-11-09 | 2000-01-25 | Kimberly-Clark Corporation | Temporary marking using photoerasable colorants |
| US5733693A (en) * | 1993-08-05 | 1998-03-31 | Kimberly-Clark Worldwide, Inc. | Method for improving the readability of data processing forms |
| US6242057B1 (en) | 1994-06-30 | 2001-06-05 | Kimberly-Clark Worldwide, Inc. | Photoreactor composition and applications therefor |
| US5739175A (en) * | 1995-06-05 | 1998-04-14 | Kimberly-Clark Worldwide, Inc. | Photoreactor composition containing an arylketoalkene wavelength-specific sensitizer |
| US6071979A (en) * | 1994-06-30 | 2000-06-06 | Kimberly-Clark Worldwide, Inc. | Photoreactor composition method of generating a reactive species and applications therefor |
| US5685754A (en) * | 1994-06-30 | 1997-11-11 | Kimberly-Clark Corporation | Method of generating a reactive species and polymer coating applications therefor |
| US6008268A (en) * | 1994-10-21 | 1999-12-28 | Kimberly-Clark Worldwide, Inc. | Photoreactor composition, method of generating a reactive species, and applications therefor |
| US5747550A (en) * | 1995-06-05 | 1998-05-05 | Kimberly-Clark Worldwide, Inc. | Method of generating a reactive species and polymerizing an unsaturated polymerizable material |
| ES2148776T3 (es) * | 1995-06-05 | 2000-10-16 | Kimberly Clark Co | Pre-colorantes y compuestos que los contienen. |
| US5849411A (en) * | 1995-06-05 | 1998-12-15 | Kimberly-Clark Worldwide, Inc. | Polymer film, nonwoven web and fibers containing a photoreactor composition |
| US5798015A (en) * | 1995-06-05 | 1998-08-25 | Kimberly-Clark Worldwide, Inc. | Method of laminating a structure with adhesive containing a photoreactor composition |
| US5811199A (en) * | 1995-06-05 | 1998-09-22 | Kimberly-Clark Worldwide, Inc. | Adhesive compositions containing a photoreactor composition |
| US5786132A (en) * | 1995-06-05 | 1998-07-28 | Kimberly-Clark Corporation | Pre-dyes, mutable dye compositions, and methods of developing a color |
| BR9609295A (pt) | 1995-06-28 | 1999-05-18 | Kimberly Clark Co | Novas substâncias corantes e modificadores de substância corante |
| US5782963A (en) * | 1996-03-29 | 1998-07-21 | Kimberly-Clark Worldwide, Inc. | Colorant stabilizers |
| US5855655A (en) | 1996-03-29 | 1999-01-05 | Kimberly-Clark Worldwide, Inc. | Colorant stabilizers |
| US6099628A (en) * | 1996-03-29 | 2000-08-08 | Kimberly-Clark Worldwide, Inc. | Colorant stabilizers |
| EP0854896B1 (en) * | 1995-11-28 | 2002-04-03 | Kimberly-Clark Worldwide, Inc. | Light-stabilized dyestuff compositions |
| US5891229A (en) * | 1996-03-29 | 1999-04-06 | Kimberly-Clark Worldwide, Inc. | Colorant stabilizers |
| US6524379B2 (en) | 1997-08-15 | 2003-02-25 | Kimberly-Clark Worldwide, Inc. | Colorants, colorant stabilizers, ink compositions, and improved methods of making the same |
| JP2002517523A (ja) | 1998-06-03 | 2002-06-18 | キンバリー クラーク ワールドワイド インコーポレイテッド | 新規な光開始剤およびその利用 |
| EP1062285A2 (en) | 1998-06-03 | 2000-12-27 | Kimberly-Clark Worldwide, Inc. | Neonanoplasts and microemulsion technology for inks and ink jet printing |
| AU5219299A (en) | 1998-07-20 | 2000-02-07 | Kimberly-Clark Worldwide, Inc. | Improved ink jet ink compositions |
| US6265458B1 (en) | 1998-09-28 | 2001-07-24 | Kimberly-Clark Worldwide, Inc. | Photoinitiators and applications therefor |
| ATE238393T1 (de) | 1999-01-19 | 2003-05-15 | Kimberly Clark Co | Farbstoffe, farbstoffstabilisatoren, tintenzusammensetzungen und verfahren zu deren herstellung |
| US6331056B1 (en) | 1999-02-25 | 2001-12-18 | Kimberly-Clark Worldwide, Inc. | Printing apparatus and applications therefor |
| US6294698B1 (en) * | 1999-04-16 | 2001-09-25 | Kimberly-Clark Worldwide, Inc. | Photoinitiators and applications therefor |
| US6368395B1 (en) | 1999-05-24 | 2002-04-09 | Kimberly-Clark Worldwide, Inc. | Subphthalocyanine colorants, ink compositions, and method of making the same |
| ATE333471T1 (de) | 2000-06-19 | 2006-08-15 | Kimberly Clark Co | Neue photoinitiatoren |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB317355A (en:Method) * | ||||
| US1846150A (en) * | 1926-10-05 | 1932-02-23 | Gen Aniline Works Inc | Solid diazoazocompounds |
| CH150001A (de) * | 1930-05-21 | 1931-10-15 | Chem Ind Basel | Verfahren zur Herstellung eines festen Diazopräparates. |
| NL37079C (en:Method) * | 1933-04-12 | |||
| NL44928C (en:Method) * | 1936-03-10 | |||
| DE865451C (de) * | 1940-07-14 | 1953-02-02 | Naphtol Chemie Offenbach | Verfahren zur Herstellung von Diazoloesungen und leichtloeslicher Diazosalzpraeparate aus festen Diazoniumchlorid-Metallchlorid-Doppelsalzen |
| US2319265A (en) * | 1940-09-25 | 1943-05-18 | Du Pont | Azo dyestuffs |
| NL87093C (en:Method) * | 1953-07-13 |
-
0
- NL NL87093D patent/NL87093C/xx active
- BE BE540426D patent/BE540426A/xx unknown
- NL NL189059D patent/NL189059A/xx unknown
- NL NL86069D patent/NL86069C/xx active
- BE BE530351D patent/BE530351A/xx unknown
-
1954
- 1954-07-01 US US440839A patent/US2744103A/en not_active Expired - Lifetime
- 1954-07-12 CH CH328081D patent/CH328081A/de unknown
- 1954-07-13 FR FR1104617D patent/FR1104617A/fr not_active Expired
- 1954-07-13 GB GB20498/54A patent/GB778917A/en not_active Expired
- 1954-08-08 DE DEF15407A patent/DE954422C/de not_active Expired
-
1955
- 1955-07-26 US US524583A patent/US2897187A/en not_active Expired - Lifetime
- 1955-08-05 CH CH337546D patent/CH337546A/de unknown
- 1955-08-05 GB GB22678/55A patent/GB779389A/en not_active Expired
- 1955-08-08 FR FR68178D patent/FR68178E/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| NL86069C (en:Method) | |
| US2744103A (en) | 1956-05-01 |
| GB779389A (en) | 1957-07-17 |
| CH337546A (de) | 1959-04-15 |
| FR1104617A (fr) | 1955-11-22 |
| NL189059A (en:Method) | |
| CH328081A (de) | 1958-02-28 |
| BE540426A (en:Method) | |
| DE954422C (de) | 1956-12-20 |
| US2897187A (en) | 1959-07-28 |
| BE530351A (en:Method) | |
| FR68178E (fr) | 1958-04-09 |
| NL87093C (en:Method) |
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