GB736890A - Improvements in or relating to lubricating greases and method of making same - Google Patents
Improvements in or relating to lubricating greases and method of making sameInfo
- Publication number
- GB736890A GB736890A GB7323/53A GB732353A GB736890A GB 736890 A GB736890 A GB 736890A GB 7323/53 A GB7323/53 A GB 7323/53A GB 732353 A GB732353 A GB 732353A GB 736890 A GB736890 A GB 736890A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acids
- acid
- oils
- lubricating
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M5/00—Solid or semi-solid compositions containing as the essential lubricating ingredient mineral lubricating oils or fatty oils and their use
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
- C10M2207/122—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms monocarboxylic
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
- C10M2207/124—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms containing hydroxy groups; Ethers thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/129—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of thirty or more carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
- C10M2207/404—Fatty vegetable or animal oils obtained from genetically modified species
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
- C10M2215/065—Phenyl-Naphthyl amines
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/08—Amides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/08—Amides
- C10M2215/082—Amides containing hydroxyl groups; Alkoxylated derivatives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/086—Imides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/14—Containing carbon-to-nitrogen double bounds, e.g. guanidines, hydrazones, semicarbazones
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/28—Amides; Imides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2010/00—Metal present as such or in compounds
- C10N2010/02—Groups 1 or 11
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/08—Resistance to extreme temperature
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/02—Bearings
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/12—Gas-turbines
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/12—Gas-turbines
- C10N2040/13—Aircraft turbines
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/10—Semi-solids; greasy
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2070/00—Specific manufacturing methods for lubricant compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
Lubricating greases of high dropping point and soft consistency over a wide temperature range are prepared by saponifying, in a lubricating oil, a saponifiable material consisting of saturated or hydrogenated glyceride fats and oils, or unsaturated fats and oils other than rapeseed oil, or mixtures of glycerine and C12-C30 saturated or unsaturated fatty acids, the saponification being effected with an excess of alkali, heating the mixture after saponification until gas is evolved, maintaining the temperature until gas evolution ceases, and then cooling the mixture. Suitable lubricating oils are mineral oils or unsaponifiable synthetic oils, but when the reaction mixture has been cooled to a temperature below 300 DEG F., following gas evolution, further lubricating oil may be added and this may be of any type, including ester lubricating oils. The preferred alkali p used for saponifying is caustic soda. Saponifiable materials mentioned are tallow, hog-fat and mixtures of glycerides with fatty acids and glycerine. Lauric, myristic, palmitic, stearic and behenic acids are examples of saturated fatty acids which may be employed. The preferred unsaturated fatty acids are C18 to about C22 acids, but those acids containing conjugated bonds such as the acids of oiticica, tung and similar drying oils should be used, if at all, only in small quantities. The lubricating greases may contain additional ingredients such as antioxidants (especially amines), dispersants, and sulphur-containing extreme pressure agents, while an oil-soluble petroleum sulphonic acid or alkali metal salt thereof may be present during saponification to increase the soft consistency and the stability of the greases. After the gas evolution, at least a portion of the free alkali in the grease may be neutralized by the addition of a fat or an organic acid, particularly a fatty acid, and sufficient acid may be added to ensure the presence of free acid in the final grease. If the acid is added after the grease has been cooled to a temperature below the transition temperature where it becomes a short-fibred unctuous mass (about 325-375 DEG F.), to produce a slight excess of free acidity in the finished grease, the cooling time may be reduced to about 1-10 hours, slow cooling being necessary otherwise. Suitable acids for neutralization of excess alkalinity are C2-C11 saturated aliphatic monocarboxylic acids such as acetic, propionic, butyric and valeric acids; C12-C30 saturated or unsaturated fatty acids such as palmitic, stearic, behenic, oleic and erucic acids; acrylic acid or hydroxy-substituted acids such as lactic, hydroxy-stearic and dihydroxy-stearic acids; and the acid employed may be the same as those employed in the initial saponification. It is believed that the evolution of gas mentioned above is caused by the dehydration of glycerine to acrolein and the reaction of the latter with alkali to form the alkali metal salt of acrylic acid and hydrogen. In the examples, lubricating greases are prepared according to the process of the invention from mineral oil, caustic soda and (1) hydrogenated tallow, further hydrogenated tallow being added after gas evolution to partially neutralize alkalinity; (2) oleic acid, with or without "Hydrofol A.B." acids, glycerine, sodium petroleum sulphonates, phenyl alpha-naphthylamine and condensation product of salicylal and ethylene diamine; and (3) hydrogenated tallow and sodium petroleum sulphonates, with the addition of hydrogenated fish oil acids and phenyl alpha-naphthylamine after gas evolution to produce a final grease containing free acids. The preparation of various rapeseed oil greases is also described for comparison purposes.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US289897A US2790769A (en) | 1952-05-24 | 1952-05-24 | Greases prepared by alkali fusion of fatty materials |
Publications (1)
Publication Number | Publication Date |
---|---|
GB736890A true GB736890A (en) | 1955-09-14 |
Family
ID=23113608
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB7323/53A Expired GB736890A (en) | 1952-05-24 | 1953-03-17 | Improvements in or relating to lubricating greases and method of making same |
Country Status (5)
Country | Link |
---|---|
US (1) | US2790769A (en) |
DE (1) | DE1012017B (en) |
FR (1) | FR1078726A (en) |
GB (1) | GB736890A (en) |
NL (1) | NL95544C (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2462209B1 (en) | 2009-08-05 | 2018-10-10 | Skf Bv | A grease composition and methods for manufacturing the grease composition |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2265791A (en) * | 1939-04-06 | 1941-12-09 | Standard Oil Dev Co | Grease composition and method for making same |
US2360631A (en) * | 1942-12-09 | 1944-10-17 | Standard Oil Dev Co | Lubricant |
US2413121A (en) * | 1944-03-20 | 1946-12-24 | Standard Oil Co | Greases |
US2445935A (en) * | 1945-10-31 | 1948-07-27 | Shell Dev | Production of greases |
US2495651A (en) * | 1947-03-20 | 1950-01-24 | Socony Vacuum Oil Co Inc | High-temperature ball-bearing grease |
US2449312A (en) * | 1947-05-07 | 1948-09-14 | Socony Vacuum Oil Co Inc | Block greases |
US2468099A (en) * | 1947-10-01 | 1949-04-26 | Standard Oil Dev Co | High-temperature grease |
US2487081A (en) * | 1947-11-28 | 1949-11-08 | Standard Oil Co | Grease |
US2487080A (en) * | 1947-11-28 | 1949-11-08 | Standard Oil Co | Grease |
US2514286A (en) * | 1947-12-31 | 1950-07-04 | Standard Oil Dev Co | Lubricating grease and method of preparing same |
US2468098A (en) * | 1948-02-18 | 1949-04-26 | Standard Oil Dev Co | Grease composition |
US2503969A (en) * | 1948-03-30 | 1950-04-11 | Standard Oil Dev Co | High-temperature lubricating grease |
US2514330A (en) * | 1948-06-05 | 1950-07-04 | Standard Oil Dev Co | Mixed base lubricating greases |
US2545126A (en) * | 1948-06-07 | 1951-03-13 | Phillips Petroleum Co | Processing of fatty acids and making grease therefrom |
DE807703C (en) * | 1948-10-02 | 1951-07-02 | Basf Ag | Lubricating greases |
DE800423C (en) * | 1948-10-02 | 1950-11-06 | Basf Ag | Process for the production of lubricating greases |
DE817183C (en) * | 1948-10-02 | 1951-10-15 | Basf Ag | Process for the production of lubricating greases |
DE833538C (en) * | 1948-10-02 | 1952-03-10 | Basf Ag | Process for the production of lubricating greases |
US2583435A (en) * | 1949-06-23 | 1952-01-22 | Standard Oil Dev Co | High-temperature grease |
US2595161A (en) * | 1950-05-24 | 1952-04-29 | Standard Oil Dev Co | Lubricating composition |
NL130887C (en) * | 1959-10-06 |
-
0
- NL NL95544D patent/NL95544C/xx active
-
1952
- 1952-05-24 US US289897A patent/US2790769A/en not_active Expired - Lifetime
-
1953
- 1953-03-17 GB GB7323/53A patent/GB736890A/en not_active Expired
- 1953-04-25 FR FR1078726D patent/FR1078726A/en not_active Expired
- 1953-05-23 DE DEST6459A patent/DE1012017B/en active Pending
Also Published As
Publication number | Publication date |
---|---|
US2790769A (en) | 1957-04-30 |
FR1078726A (en) | 1954-11-23 |
DE1012017B (en) | 1957-07-11 |
NL95544C (en) |
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