GB717930A - Improvements in or relating to the extraction of titanium from its halides - Google Patents
Improvements in or relating to the extraction of titanium from its halidesInfo
- Publication number
 - GB717930A GB717930A GB25566/51A GB2556651A GB717930A GB 717930 A GB717930 A GB 717930A GB 25566/51 A GB25566/51 A GB 25566/51A GB 2556651 A GB2556651 A GB 2556651A GB 717930 A GB717930 A GB 717930A
 - Authority
 - GB
 - United Kingdom
 - Prior art keywords
 - titanium
 - pipe
 - argon
 - reaction products
 - sodium
 - Prior art date
 - Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
 - Expired
 
Links
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title abstract 5
 - 229910052719 titanium Inorganic materials 0.000 title abstract 5
 - 239000010936 titanium Substances 0.000 title abstract 5
 - 238000000605 extraction Methods 0.000 title 1
 - 150000004820 halides Chemical class 0.000 title 1
 - XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical group [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract 8
 - FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 6
 - 229910052786 argon Inorganic materials 0.000 abstract 4
 - 239000007795 chemical reaction product Substances 0.000 abstract 4
 - DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 3
 - 229910052708 sodium Inorganic materials 0.000 abstract 3
 - 239000011734 sodium Substances 0.000 abstract 3
 - 239000011780 sodium chloride Substances 0.000 abstract 3
 - XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract 3
 - IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
 - 238000002844 melting Methods 0.000 abstract 2
 - 230000008018 melting Effects 0.000 abstract 2
 - UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
 - 229910000831 Steel Inorganic materials 0.000 abstract 1
 - QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
 - 230000001464 adherent effect Effects 0.000 abstract 1
 - 239000007864 aqueous solution Substances 0.000 abstract 1
 - QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
 - 238000001816 cooling Methods 0.000 abstract 1
 - 239000000428 dust Substances 0.000 abstract 1
 - 239000007789 gas Substances 0.000 abstract 1
 - 238000010438 heat treatment Methods 0.000 abstract 1
 - 239000001257 hydrogen Substances 0.000 abstract 1
 - 229910052739 hydrogen Inorganic materials 0.000 abstract 1
 - 239000007788 liquid Substances 0.000 abstract 1
 - 230000004048 modification Effects 0.000 abstract 1
 - 238000012986 modification Methods 0.000 abstract 1
 - 229910052757 nitrogen Inorganic materials 0.000 abstract 1
 - 239000001301 oxygen Substances 0.000 abstract 1
 - 229910052760 oxygen Inorganic materials 0.000 abstract 1
 - 239000000047 product Substances 0.000 abstract 1
 - 239000010959 steel Substances 0.000 abstract 1
 - 238000003756 stirring Methods 0.000 abstract 1
 - 239000000126 substance Substances 0.000 abstract 1
 - 235000011149 sulphuric acid Nutrition 0.000 abstract 1
 - 239000001117 sulphuric acid Substances 0.000 abstract 1
 - XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
 
Classifications
- 
        
- C—CHEMISTRY; METALLURGY
 - C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
 - C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
 - C22B1/00—Preliminary treatment of ores or scrap
 - C22B1/02—Roasting processes
 - C22B1/10—Roasting processes in fluidised form
 
 - 
        
- C—CHEMISTRY; METALLURGY
 - C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
 - C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
 - C22B1/00—Preliminary treatment of ores or scrap
 - C22B1/02—Roasting processes
 - C22B1/08—Chloridising roasting
 
 - 
        
- C—CHEMISTRY; METALLURGY
 - C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
 - C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
 - C22B34/00—Obtaining refractory metals
 - C22B34/10—Obtaining titanium, zirconium or hafnium
 - C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
 - C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
 - C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
 - C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
 
 
Landscapes
- Chemical & Material Sciences (AREA)
 - Engineering & Computer Science (AREA)
 - Environmental & Geological Engineering (AREA)
 - General Life Sciences & Earth Sciences (AREA)
 - Life Sciences & Earth Sciences (AREA)
 - Geology (AREA)
 - Mechanical Engineering (AREA)
 - Manufacturing & Machinery (AREA)
 - Materials Engineering (AREA)
 - Metallurgy (AREA)
 - Organic Chemistry (AREA)
 - Geochemistry & Mineralogy (AREA)
 - Manufacture And Refinement Of Metals (AREA)
 
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title | 
|---|---|---|---|
| LU31781D LU31781A1 (en:Method) | 1951-11-01 | ||
| BE515246D BE515246A (en:Method) | 1951-11-01 | ||
| NL77870D NL77870C (en:Method) | 1951-11-01 | ||
| NLAANVRAGE7605575,B NL173516B (nl) | 1951-11-01 | Werkwijze voor het selectief hydrogeneren van meervoudig onverzadigde verbindingen. | |
| GB25566/51A GB717930A (en) | 1951-11-01 | 1951-11-01 | Improvements in or relating to the extraction of titanium from its halides | 
| FR1069706D FR1069706A (fr) | 1951-11-01 | 1952-10-31 | Perfectionnements relatifs à la fabrication des métaux | 
| US317855A US2827371A (en) | 1951-11-01 | 1952-10-31 | Method of producing titanium in an agitated solids bed | 
| DEI6530A DE1027881B (de) | 1951-11-01 | 1952-10-31 | Verfahren zur Herstellung von Titan | 
| CH308890D CH308890A (de) | 1951-11-01 | 1952-11-01 | Verfahren zur Herstellung von Titan durch Reduktion von Titantetrachlorid. | 
| CH328601D CH328601A (fr) | 1951-11-01 | 1953-06-08 | Procédé de préparation d'uraciles | 
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title | 
|---|---|---|---|
| GB25566/51A GB717930A (en) | 1951-11-01 | 1951-11-01 | Improvements in or relating to the extraction of titanium from its halides | 
| GB1469152 | 1952-06-11 | 
Publications (1)
| Publication Number | Publication Date | 
|---|---|
| GB717930A true GB717930A (en) | 1954-11-03 | 
Family
ID=29217381
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date | 
|---|---|---|---|
| GB25566/51A Expired GB717930A (en) | 1951-11-01 | 1951-11-01 | Improvements in or relating to the extraction of titanium from its halides | 
Country Status (8)
| Country | Link | 
|---|---|
| US (1) | US2827371A (en:Method) | 
| BE (1) | BE515246A (en:Method) | 
| CH (1) | CH308890A (en:Method) | 
| DE (1) | DE1027881B (en:Method) | 
| FR (1) | FR1069706A (en:Method) | 
| GB (1) | GB717930A (en:Method) | 
| LU (1) | LU31781A1 (en:Method) | 
| NL (2) | NL77870C (en:Method) | 
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| US2830888A (en) * | 1955-09-21 | 1958-04-15 | Nat Distillers Chem Corp | Process for the preparation of titanium and zirconium subchlorides | 
| US2835568A (en) * | 1952-11-20 | 1958-05-20 | Nat Lead Co | Method of producing titanium | 
| US2865738A (en) * | 1955-08-17 | 1958-12-23 | Nat Distillers Chem Corp | Process of preparation of titanium | 
| US2882144A (en) * | 1955-08-22 | 1959-04-14 | Allied Chem | Method of producing titanium | 
| US2890953A (en) * | 1954-11-16 | 1959-06-16 | Peter Spence & Sons Ltd | Continuous process for the manufacture of titanium metal | 
| US2910357A (en) * | 1956-02-09 | 1959-10-27 | Nat Distillers Chem Corp | Method of reducing metal halides | 
| US2916374A (en) * | 1957-03-13 | 1959-12-08 | Nat Distillers Chem Corp | Method of producing multivalent metal | 
| US2922710A (en) * | 1957-02-19 | 1960-01-26 | Du Pont | Production of refractory metals | 
| US2944887A (en) * | 1955-02-07 | 1960-07-12 | Ici Ltd | Manufacture of metals | 
| US2944888A (en) * | 1956-01-17 | 1960-07-12 | Ici Ltd | Manufacture of titanium | 
| US2950963A (en) * | 1957-05-02 | 1960-08-30 | Nat Distillers Chem Corp | Production of metals | 
| US2962346A (en) * | 1957-06-18 | 1960-11-29 | Columbia Southern Chem Corp | Process for preparing alkali metal zirconate from zircon | 
| US2962347A (en) * | 1957-06-18 | 1960-11-29 | Columbia Southern Chem Corp | Method of recovering zirconium values from zircon | 
| US2963362A (en) * | 1956-02-27 | 1960-12-06 | Nat Distillers Chem Corp | Process for reducing higher halides | 
| DE1094465B (de) * | 1956-01-27 | 1960-12-08 | Ici Ltd | Verfahren zur Herstellung von Titan | 
| DE1106503B (de) * | 1955-09-21 | 1961-05-10 | Nat Distillers Chem Corp | Verfahren zur Herstellung von Titan | 
| DE1160188B (de) * | 1959-04-06 | 1963-12-27 | Allied Chem | Zweistufiges Verfahren zur Herstellung von Titan | 
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| US2835567A (en) * | 1954-11-22 | 1958-05-20 | Du Pont | Method of producing granular refractory metal | 
| US2958574A (en) * | 1955-12-02 | 1960-11-01 | Nat Distillers Chem Corp | Purification of titanium tetrachloride | 
| US3078082A (en) * | 1957-05-06 | 1963-02-19 | Nat Res Corp | Apparatus for reducing vaporizable refractory metal compounds | 
| US2986462A (en) * | 1957-10-10 | 1961-05-30 | Cons Mining & Smelting Co | Process for the production of metals | 
| US2994603A (en) * | 1958-06-20 | 1961-08-01 | Nat Distillers Chem Corp | Process of preparing columbium and tantalum | 
| US3012878A (en) * | 1958-09-16 | 1961-12-12 | Nat Distillers Chem Corp | Titanium metal production process | 
| US3004848A (en) * | 1958-10-02 | 1961-10-17 | Nat Distillers Chem Corp | Method of making titanium and zirconium alloys | 
| US3043679A (en) * | 1958-10-20 | 1962-07-10 | Diamond Alkali Co | Method of producing chromium | 
| US3086847A (en) * | 1958-12-17 | 1963-04-23 | Nat Distillers Chem Corp | Boron production | 
| US3022159A (en) * | 1959-09-24 | 1962-02-20 | Allied Chem | Production of titanium metal | 
| US3022158A (en) * | 1959-09-24 | 1962-02-20 | Allied Chem | Manufacture of metallic titanium | 
| US3053648A (en) * | 1959-10-08 | 1962-09-11 | Battelle Memorial Institute | Reduction of iron ore | 
| US3012876A (en) * | 1960-10-07 | 1961-12-12 | Du Pont | Metal production | 
| US3234015A (en) * | 1961-05-01 | 1966-02-08 | Dougles E Jones | Heavy duty, wear resistant machine element | 
| US3520656A (en) * | 1966-03-30 | 1970-07-14 | Du Pont | Silicon carbide compositions | 
| GB1202581A (en) * | 1967-01-16 | 1970-08-19 | British Titan Products Ltd | Apparatus for admitting gas into a reactor | 
| JPS6415334A (en) * | 1987-07-09 | 1989-01-19 | Toho Titanium Co Ltd | Production of metal from metal halide | 
| CN1076759C (zh) * | 1994-08-01 | 2001-12-26 | 国际钛金属粉末公司 | 制备金属和其它元素的方法 | 
| JP2005538252A (ja) * | 2002-09-07 | 2005-12-15 | インターナショナル・タイテイニアム・パウダー・リミテッド・ライアビリティ・カンパニー | TiスラリーからTiを分離する方法 | 
| US20050284824A1 (en) * | 2002-09-07 | 2005-12-29 | International Titanium Powder, Llc | Filter cake treatment apparatus and method | 
| UA79310C2 (en) * | 2002-09-07 | 2007-06-11 | Int Titanium Powder Llc | Methods for production of alloys or ceramics with the use of armstrong method and device for their realization | 
| US20060107790A1 (en) * | 2002-10-07 | 2006-05-25 | International Titanium Powder, Llc | System and method of producing metals and alloys | 
| AU2003263082A1 (en) * | 2002-10-07 | 2004-05-04 | International Titanium Powder, Llc. | System and method of producing metals and alloys | 
| US20070180951A1 (en) * | 2003-09-03 | 2007-08-09 | Armstrong Donn R | Separation system, method and apparatus | 
| CN100554447C (zh) * | 2004-07-30 | 2009-10-28 | 联邦科学和工业研究组织 | 由相应的金属卤化物制备金属的方法 | 
| US20070017319A1 (en) * | 2005-07-21 | 2007-01-25 | International Titanium Powder, Llc. | Titanium alloy | 
| WO2007044635A2 (en) | 2005-10-06 | 2007-04-19 | International Titanium Powder, Llc | Titanium or titanium alloy with titanium boride dispersion | 
| US20080031766A1 (en) * | 2006-06-16 | 2008-02-07 | International Titanium Powder, Llc | Attrited titanium powder | 
| US7753989B2 (en) * | 2006-12-22 | 2010-07-13 | Cristal Us, Inc. | Direct passivation of metal powder | 
| US9127333B2 (en) * | 2007-04-25 | 2015-09-08 | Lance Jacobsen | Liquid injection of VCL4 into superheated TiCL4 for the production of Ti-V alloy powder | 
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| DE296867C (en:Method) * | ||||
| GB386621A (en) * | 1930-04-17 | 1933-01-19 | Walther Kangro | Improved process for alloying or combining metals of any kind | 
| US2148345A (en) * | 1936-09-10 | 1939-02-21 | Degussa | Preparation of metallic titanium | 
| DE658995C (de) * | 1936-09-11 | 1938-04-21 | Degussa | Verfahren zur Herstellung von metallischem Titan | 
| DE674625C (de) * | 1937-07-11 | 1939-04-18 | Wilhelm Kroll Dr Ing | Verfahren zur Gewinnung von reinem Titan | 
| US2462661A (en) * | 1946-03-27 | 1949-02-22 | Standard Oil Dev Co | Fluidization process for producing aluminum | 
| US2478912A (en) * | 1947-03-13 | 1949-08-16 | American Metal Co Ltd | Fluidizing process for zinc recovery | 
| US2560175A (en) * | 1948-05-12 | 1951-07-10 | American Metal Co Ltd | Fluidizing reduction of zinc compounds with stagewise feeding of solids | 
| US2618549A (en) * | 1949-05-02 | 1952-11-18 | Kennecott Copper Corp | Method for the production of titanium | 
| US2621121A (en) * | 1949-09-27 | 1952-12-09 | Du Pont | Production of titanium metal | 
| US2596072A (en) * | 1951-03-28 | 1952-05-06 | Henry L Crowley & Co Inc | Process of selectively reducing ferrous chloride in the vapor phase from a gaseous mixture of manganese and ferrous chloride | 
| US2618550A (en) * | 1952-01-04 | 1952-11-18 | Kennecott Copper Corp | Method for the production of titanium | 
- 
        0
        
- LU LU31781D patent/LU31781A1/xx unknown
 - NL NLAANVRAGE7605575,B patent/NL173516B/xx unknown
 - NL NL77870D patent/NL77870C/xx active
 - BE BE515246D patent/BE515246A/xx unknown
 
 - 
        1951
        
- 1951-11-01 GB GB25566/51A patent/GB717930A/en not_active Expired
 
 - 
        1952
        
- 1952-10-31 US US317855A patent/US2827371A/en not_active Expired - Lifetime
 - 1952-10-31 DE DEI6530A patent/DE1027881B/de active Pending
 - 1952-10-31 FR FR1069706D patent/FR1069706A/fr not_active Expired
 - 1952-11-01 CH CH308890D patent/CH308890A/de unknown
 
 
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| US2835568A (en) * | 1952-11-20 | 1958-05-20 | Nat Lead Co | Method of producing titanium | 
| US2890953A (en) * | 1954-11-16 | 1959-06-16 | Peter Spence & Sons Ltd | Continuous process for the manufacture of titanium metal | 
| US2944887A (en) * | 1955-02-07 | 1960-07-12 | Ici Ltd | Manufacture of metals | 
| US2865738A (en) * | 1955-08-17 | 1958-12-23 | Nat Distillers Chem Corp | Process of preparation of titanium | 
| US2882144A (en) * | 1955-08-22 | 1959-04-14 | Allied Chem | Method of producing titanium | 
| US2830888A (en) * | 1955-09-21 | 1958-04-15 | Nat Distillers Chem Corp | Process for the preparation of titanium and zirconium subchlorides | 
| DE1106503B (de) * | 1955-09-21 | 1961-05-10 | Nat Distillers Chem Corp | Verfahren zur Herstellung von Titan | 
| US2944888A (en) * | 1956-01-17 | 1960-07-12 | Ici Ltd | Manufacture of titanium | 
| DE1094465B (de) * | 1956-01-27 | 1960-12-08 | Ici Ltd | Verfahren zur Herstellung von Titan | 
| US2910357A (en) * | 1956-02-09 | 1959-10-27 | Nat Distillers Chem Corp | Method of reducing metal halides | 
| US2963362A (en) * | 1956-02-27 | 1960-12-06 | Nat Distillers Chem Corp | Process for reducing higher halides | 
| US2922710A (en) * | 1957-02-19 | 1960-01-26 | Du Pont | Production of refractory metals | 
| US2916374A (en) * | 1957-03-13 | 1959-12-08 | Nat Distillers Chem Corp | Method of producing multivalent metal | 
| US2950963A (en) * | 1957-05-02 | 1960-08-30 | Nat Distillers Chem Corp | Production of metals | 
| US2962347A (en) * | 1957-06-18 | 1960-11-29 | Columbia Southern Chem Corp | Method of recovering zirconium values from zircon | 
| US2962346A (en) * | 1957-06-18 | 1960-11-29 | Columbia Southern Chem Corp | Process for preparing alkali metal zirconate from zircon | 
| DE1160188B (de) * | 1959-04-06 | 1963-12-27 | Allied Chem | Zweistufiges Verfahren zur Herstellung von Titan | 
Also Published As
| Publication number | Publication date | 
|---|---|
| CH308890A (de) | 1955-08-15 | 
| NL173516B (nl) | |
| NL77870C (en:Method) | |
| FR1069706A (fr) | 1954-07-12 | 
| BE515246A (en:Method) | |
| LU31781A1 (en:Method) | |
| DE1027881B (de) | 1958-04-10 | 
| US2827371A (en) | 1958-03-18 | 
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