GB708865A - A process for the production of non-hygroscopic choline salts - Google Patents

A process for the production of non-hygroscopic choline salts

Info

Publication number
GB708865A
GB708865A GB1946/52A GB194652A GB708865A GB 708865 A GB708865 A GB 708865A GB 1946/52 A GB1946/52 A GB 1946/52A GB 194652 A GB194652 A GB 194652A GB 708865 A GB708865 A GB 708865A
Authority
GB
United Kingdom
Prior art keywords
calcium
salts
choline
magnesium
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1946/52A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Badische Anilin and Sodafabrik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE, Badische Anilin and Sodafabrik AG filed Critical BASF SE
Publication of GB708865A publication Critical patent/GB708865A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/40Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton with quaternised nitrogen atoms bound to carbon atoms of the carbon skeleton

Abstract

The invention comprises mixed polybasic acid salts of choline and calcium or magnesium. They are made by treating salts of choline and polybasic acids still containing hydrogen atoms which are replaceable by metal with calcium or magnesium oxides or hydroxides, water-soluble calcium or magnesium salts, or difficultly water-soluble or water-insoluble salts of calcium or magnesium with acids which are weaker than the acid contained in the acid choline salt and thereby converting them into the corresponding calcium- or magnesium-choline mixed salts. The acid choline salts may be converted into their sodium salts before treatment with calcium or magnesium compounds. The products are non-hygroscopic. Choline salts specified are the mono- or di-citrates and phosphates, mono-tartrate and maleinate and acid salts of butane tetracarboxylic acid. Calcium and magnesium compounds specified are the oxides, hydroxides, carbonates, bicarbonates and chlorides. Reactions may be effected in water or lower alcohols, the choline salt and calcium or magnesium compound being taken in equimolar quantities. The products may be precipitated from solution by the addition of organic solvents. In an example mono-choline citrate is treated in water with calcium hydroxide, the mixed salt being obtained on evaporation of the solution.
GB1946/52A 1951-02-01 1952-01-24 A process for the production of non-hygroscopic choline salts Expired GB708865A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE708865X 1951-02-01

Publications (1)

Publication Number Publication Date
GB708865A true GB708865A (en) 1954-05-12

Family

ID=6617718

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1946/52A Expired GB708865A (en) 1951-02-01 1952-01-24 A process for the production of non-hygroscopic choline salts

Country Status (1)

Country Link
GB (1) GB708865A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1088984B (en) * 1953-06-06 1960-09-15 Buzas Andre Process for the production of stable, quaternary ammonium hyposulfites
US3759980A (en) * 1969-05-26 1973-09-18 Stockton Chemicals Inc Salicylates
US5043168A (en) * 1990-04-26 1991-08-27 Sidmak Laboratories, Inc. Solid choline magnesium salicylate composition and method of preparing same

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1088984B (en) * 1953-06-06 1960-09-15 Buzas Andre Process for the production of stable, quaternary ammonium hyposulfites
US3759980A (en) * 1969-05-26 1973-09-18 Stockton Chemicals Inc Salicylates
US5043168A (en) * 1990-04-26 1991-08-27 Sidmak Laboratories, Inc. Solid choline magnesium salicylate composition and method of preparing same

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