GB507065A - Manufacture of compounds of the anthraquinone series - Google Patents
Manufacture of compounds of the anthraquinone seriesInfo
- Publication number
- GB507065A GB507065A GB3382137A GB3382137A GB507065A GB 507065 A GB507065 A GB 507065A GB 3382137 A GB3382137 A GB 3382137A GB 3382137 A GB3382137 A GB 3382137A GB 507065 A GB507065 A GB 507065A
- Authority
- GB
- United Kingdom
- Prior art keywords
- anthraquinone
- leuco
- sulphuric acid
- ammonia
- nitrobenzene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
- C09B1/50—Amino-hydroxy-anthraquinones; Ethers and esters thereof
Abstract
507,065. Anthraquinone derivatives. OLPIN, H. C. Dec. 7, 1937, No. 33821. [Class 2 (iii)] A leuco -1-amino-4-hydroxyanthraquinone is made by acting with ammonia on a leuco-1.4- dihydroxy - anthraquinone free from amino groups, and discontinuing the reaction before any substantial proportion of the corresponding 1.4-diamino-anthraquinone has been produced. Further substituents may be hydroxy, alkoxy, sulpho- or halogen. Advantageously the ammonia is employed in excess at below 40‹ C. The reaction may be effected in presence of water or an organic liquid such as ethyl alcohol or other aliphatic alcohol. The leuco body first obtained may be oxidized by free oxygen in presence of pyridine or piperidine, with sulphuric acid with or without nitrobenzene, or with substantially anhydrous sulphuric acid according to Specification. 501,341. In an example, leucoquinizarin is treated with aqueous-alcoholic ammonia, followed by oxidation with 96 per cent sulphuric acid, with or without nitrobenzene.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB3382137A GB507065A (en) | 1937-12-07 | 1937-12-07 | Manufacture of compounds of the anthraquinone series |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB3382137A GB507065A (en) | 1937-12-07 | 1937-12-07 | Manufacture of compounds of the anthraquinone series |
Publications (1)
Publication Number | Publication Date |
---|---|
GB507065A true GB507065A (en) | 1939-06-07 |
Family
ID=10357887
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3382137A Expired GB507065A (en) | 1937-12-07 | 1937-12-07 | Manufacture of compounds of the anthraquinone series |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB507065A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0496113A1 (en) * | 1991-01-23 | 1992-07-29 | BASF Aktiengesellschaft | Process for the preparation of 1-amino-2-chloro-4-hydroxy-anthraquinone |
-
1937
- 1937-12-07 GB GB3382137A patent/GB507065A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0496113A1 (en) * | 1991-01-23 | 1992-07-29 | BASF Aktiengesellschaft | Process for the preparation of 1-amino-2-chloro-4-hydroxy-anthraquinone |
US5180841A (en) * | 1991-01-23 | 1993-01-19 | Basf Aktiengesellschaft | Preparation of 1-amino-2-chloro-4-hydroxyanthraquinone |
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