GB490830A - Improvements in or relating to the printing and colouring of textile and like materials and compositions suitable therefor - Google Patents

Improvements in or relating to the printing and colouring of textile and like materials and compositions suitable therefor

Info

Publication number
GB490830A
GB490830A GB31069/36A GB3106936A GB490830A GB 490830 A GB490830 A GB 490830A GB 31069/36 A GB31069/36 A GB 31069/36A GB 3106936 A GB3106936 A GB 3106936A GB 490830 A GB490830 A GB 490830A
Authority
GB
United Kingdom
Prior art keywords
azo
chloro
aminoanisole
naphthol
amino
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB31069/36A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of GB490830A publication Critical patent/GB490830A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B33/00Disazo and polyazo dyes of the types A->K<-B, A->B->K<-C, or the like, prepared by diazotising and coupling
    • C09B33/02Disazo dyes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Abstract

For dyeing or printing textile and other dyeable materials by forming azo dyes in situ, use is made of neutral or alkaline compositions containing (a) a diazotized aromatic aminestabilized against reaction with a coupling component in a neutral or alkaline medium, and (b) a coupling component containing an azo group. Component (a) is stabilized by conversion into a diazoimino compound or a nitrosamine or an azosulphonate. The compositions may be produced in the form of powders, pastes or solutions, and after they have been applied to the material to be dyed, the colour is developed by treatment with an acid. The following examples are given: (1) the diazoimino compound from diazotized 4-chloro-2-aminoanisole and piperidine-a -carboxylic acid is mixed with the azo compound from diazotized m-nitraniline and 1-amino-7-naphthol, and the mixture is pasted with the aid of caustic soda solution, monopol oil, and starch-tragacanth thickener; cotton goods are printed with the paste and then treated with steam containing acetic and formic acid vapours, brown prints being obtained; (2) the diazoimino compound from diazotized 4-chloro-2-aminoanisole and methylglucamine is mixed with the azo compound from diazotized 4-chloro-2-aminoanisole and 1-amino-7-naphthol, and the mixture is pasted and applied as in example 1, brown prints being obtained; (3) a printing paste is prepared containing the nitrosamine from 4-chloro-2-aminoanisole, the azo compound from diazotized 4 - chloro - 2 - aminoanisole and 1 - amino - 7-naphthol, leucanol, aqueous caustic soda, and starch-tragacanth thickener; cotton goods are printed with the paste, and the colour is then developed by treating the goods either with steam containing acetic acid vapour or with a bath containing acetic acid and sodium chromate, brown prints being obtained; (4) a printing paste is prepared containing the diazoimino compound from diazotized 4-chloro-2-aminoanisole and piperidine-a -carboxylic acid, benzene-azo-resorcinol, aqueous caustic soda, monopol oil, and starch-tragacanth thickener, and the paste is applied as in example 1, brown prints being obtained; (5) as in example 4, except that benzene-azo-2 : 5-dioxynaphthalene is used in place of benzene-azo-resorcinol, brown prints being again obtained. A table is given also of compositions containing ingredients selected from the following lists: (a) arylamines from which diazoimino compounds are prepared: 4 - chloro - 2 - aminotoluene, aniline, 4-chloro-2-aminoanisole, and dianisidine; (b) stabilizers used in making the diazoimino compounds: piperidine - a - carboxylic acid, sarcosine, and methylglucamine; (c) coupling components: the azo compounds from 1-amino-7-naphthol and the diazo compounds of 4-chloro-2-aminoanisole, 5-nitro-2-aminoanisole, 2 : 5-dichloraniline, aniline, 3-chloraniline, 4-nitraniline, 4 - chloro - 2 - nitraniline, 2 : 5 - dichloro - 4-nitraniline, 2 : 4-dimethyl-6-nitraniline; 2 : 5-diethoxy - 4 - nitraniline, m - aminobenzotrifluoride, 4-chloro-2-aminotoluene, 4-nitro-2-aminotoluene, 3-nitro-4-aminotoluene, 4-nitro-2-aminoanisole, 3-nitro-4-aminoanisole, a -naphthylamine, b -naphthylamine, and a -aminoanthraquinone; the compositions yield black or brown shades. Other specified diazo compounds to be used in a stabilized form are those from o-chloraniline, 4-chloro-2-aminophenetole, 4 - chloro - 2 : 5 - dimethylaniline, 4-benzoylamino - 2 : 5 - dimethoxyaniline, 1-methoxy-2-naphthylamine, 4-chloro-2-aminodiphenyl ether, o-aminoazotoluene, 4 : 41-diaminodiphenylamine, and 3-aminocarbazole. Other specified reagents for the production of diazoimino compounds are 1 - methylaminoethane-2-sulphonic acid, proline, nipecotinic acid, benzyleneimino-p-sulphonic acid, 1-naphthylamine-2 : 4 : 8-trisulphonic acid, and 2-ethylamino - 4 - sulphobenzoic acid. Other specified coupling components are p-nitrobenzene - azo - phloroglucinol, 2 : 5 - dichlorobenzene-azo-2 : 7-dioxynaphthalene, p-methylbenzene - azo - 1 : 5 - dioxynaphthalene, 3 - (p-nitrobenzene) - azo - 4 : 41 - dioxydiphenyl, benzene - azo - 1 : 5 - dioxyanthracene, benzeneazo - m - phenylenediamine, benzene - azo - 1 : 5-diaminonaphthalene, p-chlorobenzene - azo - m-aminophenol, benzene - azo - 3 : 5 - dihydroxyaniline, 2 : 5 - dichlorobenzene - azo - 2 - amino - 7 - naphthol, 2 : 5-dichlorobenzene-azo-1-amino-5-naphthol, 2 - nitro - 4 - methylbenzene - azo - 2 - amino-6-naphthol, a -naphthalene-azo-1-amino-6-naphthol, benzene-azo-1 : 3-diamino-5-naphthol, and p-nitrobenzene - azo - 4 - amino - 1 : 5-dioxynaphthalene. Other specified materials which may be treated are regenerated cellulose, cellulose esters and ethers, wool, silk and leather. Other specified components of the compositions are ethyl alcohol, ethylene glycol monoethyl ether, and ethanolamine. Reference is made also to the production of pigments by acidifying the compositions in aqueous solution or suspension.
GB31069/36A 1935-11-13 1936-11-13 Improvements in or relating to the printing and colouring of textile and like materials and compositions suitable therefor Expired GB490830A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US490830XA 1935-11-13 1935-11-13

Publications (1)

Publication Number Publication Date
GB490830A true GB490830A (en) 1938-08-16

Family

ID=21957958

Family Applications (1)

Application Number Title Priority Date Filing Date
GB31069/36A Expired GB490830A (en) 1935-11-13 1936-11-13 Improvements in or relating to the printing and colouring of textile and like materials and compositions suitable therefor

Country Status (1)

Country Link
GB (1) GB490830A (en)

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