GB233840A - Process for the manufacture of active absorbing carbon and phosphoric acid and its compounds - Google Patents

Process for the manufacture of active absorbing carbon and phosphoric acid and its compounds

Info

Publication number
GB233840A
GB233840A GB8048/24A GB804824A GB233840A GB 233840 A GB233840 A GB 233840A GB 8048/24 A GB8048/24 A GB 8048/24A GB 804824 A GB804824 A GB 804824A GB 233840 A GB233840 A GB 233840A
Authority
GB
United Kingdom
Prior art keywords
phosphoric acid
treated
calcium
magnesium
bone char
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB8048/24A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JOHN OUTRAM CUTTER
ROGER DUNCALFE
Original Assignee
JOHN OUTRAM CUTTER
ROGER DUNCALFE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JOHN OUTRAM CUTTER, ROGER DUNCALFE filed Critical JOHN OUTRAM CUTTER
Priority to GB8048/24A priority Critical patent/GB233840A/en
Publication of GB233840A publication Critical patent/GB233840A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00Purification of sugar juices
    • C13B20/12Purification of sugar juices using adsorption agents, e.g. active carbon
    • C13B20/123Inorganic agents, e.g. active carbon
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
    • C01B32/312Preparation
    • C01B32/342Preparation characterised by non-gaseous activating agents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Water Treatment By Sorption (AREA)
  • Removal Of Specific Substances (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

Bone char or bone char dust is leached with a dilute solution of phosphoric acid in order to obtain activated carbon and phosphoric acid. The bone char, which may receive a preliminary re-calcination, is washed with water after leaching and dried and the combined washing water and leaching liquor is treated with sulphuric acid in amount considerably less than the equivalent of the calcium and magnesium present in solution. On evaporation, di-calcium-hydrogen phosphate is precipitated which may be removed and regarded as the finished product or may be decomposed with sulphuric acid to give calcium sulphate and phosphoric acid for re-use. The filtrate from the di-calcium hydrogen phosphate is treated with sulphuric acid in quantity sufficient to precipitate most of the calcium and magnesium as sulphates. The latter are separated and the mother-liquor containing phosphoric acid is treated for the removal of the salts of magnesium and the alkalies which are present. Waste liquors which are too dilute to warrant evaporation may be treated with lime to recover their content of phosphate.ALSO:Bone char or bone char dust is leached with a dilute solution of phosphoric acid in order to obtain activated carbon and phosphoric acid. The bone char which may receive a preliminary re-calcination is washed with water after leaching and dried and the combined washing water and leaching liquor is treated with sulphuric acid in amount considerably less than the equivalent of the calcium and magnesium present in solution. On evaporation dicalcium-hydrogen phosphate is precipitated, which may be removed and regarded as the finished product, or may be decomposed with sulphuric acid to give calcium sulphate and phosphoric acid for re-use. The filtrate from the dicalcium hydrogen phosphate is treated with sulphuric acid in quantity sufficient to precipitate most of the calcium and magnesium as sulphates. The latter are separated and the mother-liquor containing phosphoric acid is treated for the removal of the salts of magnesium and the alkalies which are present. Waste liquors which are too dilute to warrant evaporation may be treated with lime to recover their content of phosphate.
GB8048/24A 1924-03-29 1924-03-29 Process for the manufacture of active absorbing carbon and phosphoric acid and its compounds Expired GB233840A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB8048/24A GB233840A (en) 1924-03-29 1924-03-29 Process for the manufacture of active absorbing carbon and phosphoric acid and its compounds

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB8048/24A GB233840A (en) 1924-03-29 1924-03-29 Process for the manufacture of active absorbing carbon and phosphoric acid and its compounds

Publications (1)

Publication Number Publication Date
GB233840A true GB233840A (en) 1925-05-21

Family

ID=9844773

Family Applications (1)

Application Number Title Priority Date Filing Date
GB8048/24A Expired GB233840A (en) 1924-03-29 1924-03-29 Process for the manufacture of active absorbing carbon and phosphoric acid and its compounds

Country Status (1)

Country Link
GB (1) GB233840A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2712494A (en) * 1951-01-16 1955-07-05 Saint Gobain Preparation of phosphorus oxychloride
GB2399343A (en) * 2003-01-16 2004-09-15 Rodney Bruce Gilmour Disposal of animal waste

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2712494A (en) * 1951-01-16 1955-07-05 Saint Gobain Preparation of phosphorus oxychloride
GB2399343A (en) * 2003-01-16 2004-09-15 Rodney Bruce Gilmour Disposal of animal waste

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