GB1490350A - Manufacture of hydroxynaphthaldehydes - Google Patents
Manufacture of hydroxynaphthaldehydesInfo
- Publication number
- GB1490350A GB1490350A GB2483874A GB2483874A GB1490350A GB 1490350 A GB1490350 A GB 1490350A GB 2483874 A GB2483874 A GB 2483874A GB 2483874 A GB2483874 A GB 2483874A GB 1490350 A GB1490350 A GB 1490350A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydroxynaphthaldehydes
- aqueous phase
- phase transfer
- formula
- phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/008—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with tri- or tetrahalomethyl compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
1490350 2-Hydroxynaphthaldehydes IMPERIAL CHEMICAL INDUSTRIES Ltd 30 April 1975 [5 June 1974] 24838/74 Heading C2C 2-Hydroxynaphthaldehydes are prepared by reacting chloroform with an aqueous solution of a 2-naphthol alkali metal salt solution in the presence of a phase transfer catalyst. The phase transfer catalyst is a substance which transfers a reactant from aqueous phase to non-aqueous phase where it undergoes reaction thus releasing the catalyst back into the aqueous phase, preferred phase transfer catalysts are quaternary ammonium salts of the formula where R 1 , R 2 , R 3 and R 4 are each alkyl, aralkyl, and cycloalkyl, or two together may form a ring with 5 to 7 carbon atoms and X is halogen, bisulphate or hydroxyl, and the equivalent quaternary phosphonium salts. The 2-naphthol starting material preferably has the formula wherein R 1 and R 3 are hydrogen atoms or sulphonic acid groups, and R 3 is a carboxyl or sulphonic acid group or hydrogen.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2483874A GB1490350A (en) | 1975-04-30 | 1975-04-30 | Manufacture of hydroxynaphthaldehydes |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2483874A GB1490350A (en) | 1975-04-30 | 1975-04-30 | Manufacture of hydroxynaphthaldehydes |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1490350A true GB1490350A (en) | 1977-11-02 |
Family
ID=10218041
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2483874A Expired GB1490350A (en) | 1975-04-30 | 1975-04-30 | Manufacture of hydroxynaphthaldehydes |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1490350A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5841834A (en) * | 1981-09-07 | 1983-03-11 | Sumitomo Chem Co Ltd | Preparation of hydroxybenzaldehyde |
-
1975
- 1975-04-30 GB GB2483874A patent/GB1490350A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5841834A (en) * | 1981-09-07 | 1983-03-11 | Sumitomo Chem Co Ltd | Preparation of hydroxybenzaldehyde |
EP0074272A1 (en) * | 1981-09-07 | 1983-03-16 | Sumitomo Chemical Company, Limited | Process for the preparation of hydroxybenzaldehydes |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |