GB1488094A - Process for the synthesis of decaborane(14) - Google Patents
Process for the synthesis of decaborane(14)Info
- Publication number
- GB1488094A GB1488094A GB3169/75A GB316975A GB1488094A GB 1488094 A GB1488094 A GB 1488094A GB 3169/75 A GB3169/75 A GB 3169/75A GB 316975 A GB316975 A GB 316975A GB 1488094 A GB1488094 A GB 1488094A
- Authority
- GB
- United Kingdom
- Prior art keywords
- decaborane
- boron trifluoride
- solvent
- mbh
- jan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 230000015572 biosynthetic process Effects 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 238000003786 synthesis reaction Methods 0.000 title 1
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 abstract 8
- 229910015900 BF3 Inorganic materials 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 239000007800 oxidant agent Substances 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- 238000002360 preparation method Methods 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- JHWIEAWILPSRMU-UHFFFAOYSA-N 2-methyl-3-pyrimidin-4-ylpropanoic acid Chemical compound OC(=O)C(C)CC1=CC=NC=N1 JHWIEAWILPSRMU-UHFFFAOYSA-N 0.000 abstract 1
- YNJSNEKCXVFDKW-UHFFFAOYSA-N 3-(5-amino-1h-indol-3-yl)-2-azaniumylpropanoate Chemical compound C1=C(N)C=C2C(CC(N)C(O)=O)=CNC2=C1 YNJSNEKCXVFDKW-UHFFFAOYSA-N 0.000 abstract 1
- 108010008488 Glycylglycine Proteins 0.000 abstract 1
- -1 alkyl ammonium ions Chemical class 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 150000002170 ethers Chemical class 0.000 abstract 1
- YMAWOPBAYDPSLA-UHFFFAOYSA-N glycylglycine Chemical compound [NH3+]CC(=O)NCC([O-])=O YMAWOPBAYDPSLA-UHFFFAOYSA-N 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 239000012286 potassium permanganate Substances 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/02—Boron; Borides
- C01B35/026—Higher boron hydrides, i.e. containing at least three boron atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US43666374A | 1974-01-25 | 1974-01-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1488094A true GB1488094A (en) | 1977-10-05 |
Family
ID=23733325
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3169/75A Expired GB1488094A (en) | 1974-01-25 | 1975-01-24 | Process for the synthesis of decaborane(14) |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5514812B2 (en:Method) |
| BE (1) | BE824771A (en:Method) |
| CA (1) | CA1040386A (en:Method) |
| DE (1) | DE2502716A1 (en:Method) |
| FR (1) | FR2259050B1 (en:Method) |
| GB (1) | GB1488094A (en:Method) |
| IT (1) | IT1027362B (en:Method) |
| SE (1) | SE7500775L (en:Method) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0007599A1 (en) * | 1978-07-21 | 1980-02-06 | Union Carbide Corporation | Synthesis of tetradecahydroundecaborate(-1) from borohydride ion |
| RU2346890C2 (ru) * | 2006-12-27 | 2009-02-20 | Федеральное государственное унитарное предприятие "Государственный ордена Трудового Красного Знамени научно-исследовательский институт химии и технологии элементоорганических соединений" (ФГУП ГНИИХТЭОС) | Способ получения декаборана |
-
1974
- 1974-12-31 CA CA217,148A patent/CA1040386A/en not_active Expired
-
1975
- 1975-01-23 DE DE19752502716 patent/DE2502716A1/de not_active Withdrawn
- 1975-01-24 SE SE7500775A patent/SE7500775L/xx not_active Application Discontinuation
- 1975-01-24 FR FR7502275A patent/FR2259050B1/fr not_active Expired
- 1975-01-24 GB GB3169/75A patent/GB1488094A/en not_active Expired
- 1975-01-24 IT IT67162/75A patent/IT1027362B/it active
- 1975-01-24 BE BE152704A patent/BE824771A/xx unknown
- 1975-01-24 JP JP993275A patent/JPS5514812B2/ja not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0007599A1 (en) * | 1978-07-21 | 1980-02-06 | Union Carbide Corporation | Synthesis of tetradecahydroundecaborate(-1) from borohydride ion |
| RU2346890C2 (ru) * | 2006-12-27 | 2009-02-20 | Федеральное государственное унитарное предприятие "Государственный ордена Трудового Красного Знамени научно-исследовательский институт химии и технологии элементоорганических соединений" (ФГУП ГНИИХТЭОС) | Способ получения декаборана |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5514812B2 (en:Method) | 1980-04-18 |
| FR2259050A1 (en:Method) | 1975-08-22 |
| FR2259050B1 (en:Method) | 1978-07-13 |
| CA1040386A (en) | 1978-10-17 |
| JPS50104800A (en:Method) | 1975-08-19 |
| IT1027362B (it) | 1978-11-20 |
| BE824771A (fr) | 1975-07-24 |
| SE7500775L (en:Method) | 1975-07-28 |
| DE2502716A1 (de) | 1975-08-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |