GB1452136A - Process for preparation of pufified phosphoric acid - Google Patents

Process for preparation of pufified phosphoric acid

Info

Publication number
GB1452136A
GB1452136A GB5459273A GB5459273A GB1452136A GB 1452136 A GB1452136 A GB 1452136A GB 5459273 A GB5459273 A GB 5459273A GB 5459273 A GB5459273 A GB 5459273A GB 1452136 A GB1452136 A GB 1452136A
Authority
GB
United Kingdom
Prior art keywords
organic
phosphoric acid
organic solvent
weight
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5459273A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mizusawa Industrial Chemicals Ltd
Original Assignee
Mizusawa Industrial Chemicals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mizusawa Industrial Chemicals Ltd filed Critical Mizusawa Industrial Chemicals Ltd
Publication of GB1452136A publication Critical patent/GB1452136A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/18Phosphoric acid
    • C01B25/22Preparation by reacting phosphate-containing material with an acid, e.g. wet process
    • C01B25/222Preparation by reacting phosphate-containing material with an acid, e.g. wet process with sulfuric acid, a mixture of acids mainly consisting of sulfuric acid or a mixture of compounds forming it in situ, e.g. a mixture of sulfur dioxide, water and oxygen
    • C01B25/232Preparation by reacting phosphate containing material with concentrated sulfuric acid and subsequently lixiviating the obtained mass, e.g. clinker process
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/18Phosphoric acid
    • C01B25/234Purification; Stabilisation; Concentration

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Saccharide Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

1452136 Phosphoric acid MIZUSAWA KAGAKU KOGYO KK 23 Nov 1973 [25 Nov 1972] 54592/73 Heading C1A Phosphoric acid is prepared by mixing phosphate rock with sulphuric acid to give a solid granular phosphate rock-sulphuric acid reaction product having a transfer index E of 0À8-2À8 and selectively extracting the phosphoric acid component from the reaction product using an organic solvent. The transfer index is defined by the relationship where (P 2 O 5 ), (CaO), (SO 3 ) and (F-fluorine) are the respective weight percentages in the reaction product and (M) is the sum of the weight percentages of Al 2 O 3 , SiO 2 , Fe 2 O 3 , MgO and alkali metal oxides, the quantity E being, for all practical purposes, the percentage of water in the composition. The organic solvent may be an aliphatic alcohol. where n is an integer of 1-3, m is 0 or 1, R<SP>1</SP> is an aliphatic hydrocarbon residue having 2 to 8 carbon atoms, whose carbon chain is optionally interrupted by an ether-type oxygen atom and R<SP>2</SP> is a H atom or an alkyl group of up to 4 carbon atoms. The preferred organic solvent is butanol and the organic solvent may contain water in an amount of at most x parts by weight where x = y-z, z is the weight of water present in the phosphate rock and y is that weight of water which if present in the rock would give a transfer index of 0À8. Other organic solvents mentioned include organic sulphoxides, organic phosphates, organic amines and quaternary organic ammonium salts.
GB5459273A 1972-11-25 1973-11-23 Process for preparation of pufified phosphoric acid Expired GB1452136A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP47118342A JPS5228117B2 (en) 1972-11-25 1972-11-25

Publications (1)

Publication Number Publication Date
GB1452136A true GB1452136A (en) 1976-10-13

Family

ID=14734293

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5459273A Expired GB1452136A (en) 1972-11-25 1973-11-23 Process for preparation of pufified phosphoric acid

Country Status (13)

Country Link
JP (1) JPS5228117B2 (en)
BE (1) BE807728A (en)
CA (1) CA1015529A (en)
DE (1) DE2358780C3 (en)
ES (1) ES420814A1 (en)
FR (1) FR2207861B1 (en)
GB (1) GB1452136A (en)
IN (1) IN140714B (en)
IT (1) IT999487B (en)
NL (1) NL7316156A (en)
NO (1) NO137543C (en)
SE (1) SE390529B (en)
SU (1) SU613710A3 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS578873Y2 (en) * 1976-07-28 1982-02-19
FR3138474B1 (en) 2022-07-29 2024-06-14 Psa Automobiles Sa SYSTEM AND METHOD FOR DETECTING CLOGGING OF A HEAVY LOAD CHECK VALVE OF A THERMAL ENGINE, VEHICLE COMPRISING SUCH A SYSTEM

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE328266B (en) * 1967-05-17 1970-09-14 Mizusawa Industrial Chem

Also Published As

Publication number Publication date
BE807728A (en) 1974-03-15
SU613710A3 (en) 1978-06-30
SE390529B (en) 1976-12-27
DE2358780B2 (en) 1979-07-12
FR2207861B1 (en) 1977-08-12
DE2358780C3 (en) 1980-03-13
IT999487B (en) 1976-02-20
NL7316156A (en) 1974-05-28
NO137543B (en) 1977-12-05
DE2358780A1 (en) 1974-06-06
ES420814A1 (en) 1976-04-01
JPS4976795A (en) 1974-07-24
IN140714B (en) 1976-12-11
FR2207861A1 (en) 1974-06-21
AU6285173A (en) 1975-05-29
JPS5228117B2 (en) 1977-07-25
CA1015529A (en) 1977-08-16
NO137543C (en) 1978-03-15

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee