GB1463742A - Purification of phosophoric acid by means of organic solvents - Google Patents
Purification of phosophoric acid by means of organic solventsInfo
- Publication number
- GB1463742A GB1463742A GB2647274A GB2647274A GB1463742A GB 1463742 A GB1463742 A GB 1463742A GB 2647274 A GB2647274 A GB 2647274A GB 2647274 A GB2647274 A GB 2647274A GB 1463742 A GB1463742 A GB 1463742A
- Authority
- GB
- United Kingdom
- Prior art keywords
- solvent
- phosphoric acid
- conduit
- water
- azeotrope
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003960 organic solvent Substances 0.000 title abstract 3
- 239000002253 acid Substances 0.000 title abstract 2
- 238000000746 purification Methods 0.000 title abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 18
- 239000002904 solvent Substances 0.000 abstract 10
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 8
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 2
- 238000005201 scrubbing Methods 0.000 abstract 2
- NMRPBPVERJPACX-UHFFFAOYSA-N (3S)-octan-3-ol Natural products CCCCCC(O)CC NMRPBPVERJPACX-UHFFFAOYSA-N 0.000 abstract 1
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 abstract 1
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 abstract 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 abstract 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 abstract 1
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 abstract 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 239000008346 aqueous phase Substances 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 229910001385 heavy metal Inorganic materials 0.000 abstract 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 229940043265 methyl isobutyl ketone Drugs 0.000 abstract 1
- 239000003791 organic solvent mixture Substances 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 150000003388 sodium compounds Chemical class 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000011877 solvent mixture Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/18—Phosphoric acid
- C01B25/234—Purification; Stabilisation; Concentration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2334019A DE2334019C3 (de) | 1973-07-04 | 1973-07-04 | Verfahren zur Reinigung von verunreinigter wäßriger Phosphorsäure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1463742A true GB1463742A (en) | 1977-02-09 |
Family
ID=5885915
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2647274A Expired GB1463742A (en) | 1973-07-04 | 1974-06-14 | Purification of phosophoric acid by means of organic solvents |
Country Status (22)
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2318725C1 (ru) * | 2006-11-10 | 2008-03-10 | Открытое акционерное общество "Научно-исследовательский институт по удобрениям и инсектофунгицидам им. Я.В. Самойлова" | Способ очистки экстракционной фосфорной кислоты |
| CN108862223A (zh) * | 2018-09-07 | 2018-11-23 | 云南云天化股份有限公司 | 一种有效延长磷酸浓缩系统设备清洗周期的方法 |
| CN110316891A (zh) * | 2019-03-25 | 2019-10-11 | 华颢控股（集团）有限公司 | 一种h酸废水萃取工艺以及改性脂肪族减水剂的制备方法 |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1436113A (en) * | 1972-04-26 | 1976-05-19 | Albright & Wilson | Purification of phosphoric acid |
| DE2538720C2 (de) * | 1975-08-30 | 1982-11-18 | Giulini Chemie Gmbh, 6700 Ludwigshafen | Verfahren zur Reinigung von Naßverfahrensphosphorsäure |
| FR2447348A1 (fr) * | 1979-01-24 | 1980-08-22 | Rhone Poulenc Ind | Procede de purification d'un acide phosphorique impur |
| DE3246415A1 (de) * | 1982-12-15 | 1984-06-20 | Hoechst Ag, 6230 Frankfurt | Verfahren zur reinigung von nassverfahrenphosphorsaeure |
| JPS60155513A (ja) * | 1984-01-23 | 1985-08-15 | Mitsui Toatsu Chem Inc | 燐酸液の濃縮方法 |
| DE19703884C2 (de) | 1997-02-03 | 1999-04-29 | Bk Giulini Chem Gmbh & Co Ohg | Verfahren zur Reinigung von Naßverfahrensphosphorsäure |
| JP6143808B2 (ja) * | 2015-05-28 | 2017-06-07 | 曽田香料株式会社 | 水溶液中の溶質成分の抽出法 |
| DE102016212242B4 (de) | 2016-07-05 | 2019-02-07 | Technische Universität Bergakademie Freiberg | Verfahren zur Herstellung von Phosphorsäure aus phosphorhaltigen Primär- und Sekundärrohstoffen |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE884358C (de) * | 1951-09-20 | 1953-07-27 | Gerardo Collardin | Verfahren zur Reinigung von technischer Phosphorsaeure |
-
1973
- 1973-07-04 DE DE2334019A patent/DE2334019C3/de not_active Expired
-
1974
- 1974-05-24 NL NLAANVRAGE7407025,A patent/NL178408C/xx not_active IP Right Cessation
- 1974-05-29 ES ES426753A patent/ES426753A1/es not_active Expired
- 1974-05-30 CH CH740074A patent/CH603488A5/xx not_active IP Right Cessation
- 1974-06-11 ZA ZA00743713A patent/ZA743713B/xx unknown
- 1974-06-14 GB GB2647274A patent/GB1463742A/en not_active Expired
- 1974-06-16 IL IL45043A patent/IL45043A/en unknown
- 1974-06-20 FI FI1900/74A patent/FI190074A7/fi unknown
- 1974-06-21 SU SU742035160A patent/SU589902A3/ru active
- 1974-06-24 PH PH15977A patent/PH12113A/en unknown
- 1974-06-25 EG EG244/74A patent/EG11909A/xx active
- 1974-06-26 AT AT530074A patent/AT351492B/de not_active IP Right Cessation
- 1974-06-27 JP JP49073758A patent/JPS5239799B2/ja not_active Expired
- 1974-06-27 TR TR19869A patent/TR19869A/xx unknown
- 1974-06-27 FR FR7422510A patent/FR2235876B1/fr not_active Expired
- 1974-06-27 SE SE7408508A patent/SE397332B/xx unknown
- 1974-06-28 BE BE146016A patent/BE817018A/xx not_active IP Right Cessation
- 1974-06-28 BR BR5372/74A patent/BR7405372A/pt unknown
- 1974-06-28 DK DK350174*A patent/DK350174A/da not_active Application Discontinuation
- 1974-06-28 IT IT51807/74A patent/IT1018704B/it active
- 1974-06-28 DD DD179576A patent/DD112420A5/xx unknown
- 1974-06-28 CA CA203,698A patent/CA1020725A/en not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2318725C1 (ru) * | 2006-11-10 | 2008-03-10 | Открытое акционерное общество "Научно-исследовательский институт по удобрениям и инсектофунгицидам им. Я.В. Самойлова" | Способ очистки экстракционной фосфорной кислоты |
| CN108862223A (zh) * | 2018-09-07 | 2018-11-23 | 云南云天化股份有限公司 | 一种有效延长磷酸浓缩系统设备清洗周期的方法 |
| CN110316891A (zh) * | 2019-03-25 | 2019-10-11 | 华颢控股（集团）有限公司 | 一种h酸废水萃取工艺以及改性脂肪族减水剂的制备方法 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 19920614 |