GB1421192A - Preparation of aminomethane-diphosphonic acid - Google Patents

Preparation of aminomethane-diphosphonic acid

Info

Publication number
GB1421192A
GB1421192A GB387873A GB387873A GB1421192A GB 1421192 A GB1421192 A GB 1421192A GB 387873 A GB387873 A GB 387873A GB 387873 A GB387873 A GB 387873A GB 1421192 A GB1421192 A GB 1421192A
Authority
GB
United Kingdom
Prior art keywords
diphosphonic acid
aminomethane
acid
pcl
jan
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB387873A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BK Ladenburg GmbH
Original Assignee
Benckiser Knapsack GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Benckiser Knapsack GmbH filed Critical Benckiser Knapsack GmbH
Publication of GB1421192A publication Critical patent/GB1421192A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/38Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3839Polyphosphonic acids
    • C07F9/3873Polyphosphonic acids containing nitrogen substituent, e.g. N.....H or N-hydrocarbon group which can be substituted by halogen or nitro(so), N.....O, N.....S, N.....C(=X)- (X =O, S), N.....N, N...C(=X)...N (X =O, S)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

1421192 Aminomethane diphosphonic acid BENCKISER-KNAPSACK GmbH 25 Jan 1973 [25 Jan 1972] 3878/73 Heading C2P Aminomethane diphosphonic acid is prepared by reacting HCN with a mixture of PCl 3 and H 3 PO 3 in the presence of a catalyst comprising a halide of a polyvalent metal or metalloid, without heating, and subsequently hydrolysing the resulting product. The acid obtained may be converted to a salt by reaction with an alkali or alkaline earth metal hydroxide or alternatively an alkali metal salt may be obtained directly by replacing HCN by an alkali metal cyanide. The hydrolysis may be effected with water or hydrochloric acid and the catalyst may comprise AlCl 3 , BBr 3 , BF 3 , SbCl 5 or ZnCl 2 . The PCl 3 and H 3 PO 3 are preferably used in a mole ratio of from 1 : 2 to 5 : 1.
GB387873A 1972-01-25 1973-01-25 Preparation of aminomethane-diphosphonic acid Expired GB1421192A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2203366A DE2203366C3 (en) 1972-01-25 1972-01-25 Process for the preparation of aminomethanediphosphonic acid and its salts

Publications (1)

Publication Number Publication Date
GB1421192A true GB1421192A (en) 1976-01-14

Family

ID=5833951

Family Applications (1)

Application Number Title Priority Date Filing Date
GB387873A Expired GB1421192A (en) 1972-01-25 1973-01-25 Preparation of aminomethane-diphosphonic acid

Country Status (5)

Country Link
US (1) US3903142A (en)
DE (1) DE2203366C3 (en)
FR (1) FR2169116B1 (en)
GB (1) GB1421192A (en)
IT (1) IT978466B (en)

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3565949A (en) * 1967-08-15 1971-02-23 Fmc Corp Diaminoalkanediylidenetetraphosphonic acids useful in cleaning compositions

Also Published As

Publication number Publication date
IT978466B (en) 1974-09-20
DE2203366C3 (en) 1975-04-10
DE2203366B2 (en) 1974-08-22
FR2169116B1 (en) 1976-08-27
DE2203366A1 (en) 1973-08-02
US3903142A (en) 1975-09-02
FR2169116A1 (en) 1973-09-07

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee